The invention relates to a preparation method of an environmental protection coating of a SiCf/SiC composite material guider blade. The preparation method comprises the following steps: preheating a SiCf/SiC composite material guider blade matrix, and performing PS-PVD (Plasma Spraying-Physical Vapor Deposition) to prepare a Si adhesive layer, a mullite transitional layer, a Yb2SiO5 environmental barrier layer and a La2Zr2O7 heat resistant layer in sequence, wherein the environmental protection coating can be applied to a gas environment at 1,400 to 1,700 DEG C. Preparation of the Si adhesive layer, the mullite transitional layer, the Yb2SiO5 environmental barrier layer and the La2Zr2O7 heat resistant layer of the environmental protection coating is completed on the same equipment; the temperature of the matrix is effectively controlled through heating of a PS-PVD spraying gun, so as to prevent amorphous reaction in a deposition process of the mullite transitional layer; the added heat resistant layer enables the environmental protection coating to adapt to the gas environment at 1,400 to 1,700 DEG C; therefore, the preparation method is applicable to preparation of the environmental protection coating of a high-performance guider blade. The preparation method has the advantages that the preparation process is simple, easy to operate, high in stability, wide in applicable temperature range and wide in application range.