The invention discloses a
production line for synthesizing
silicon nitride micropowder by using
crystal silicon slice waste
mortar. The
production line comprises a
filter press, a filtrate clarification tank, a vacuum dryer, a rotary vibration
sieve, a
silicon powder tank, a vector
fluidization seat, an atomization ejector, an atomization synthesizer, a
plasma spray gun, a
plasma control cabinet, a circulating water high-level tank, a circulating water tank, a circulating water pump, a spray head, a
nitrogen source device, a
liquid nitrogen gasifier and a pressure regulating valve group, the
system is composed of a flow control valve
bank, a
nitrogen recovery tank, a vacuum
packaging machine, corresponding process pipelines and an
automatic control system. The method comprises the following steps: preparing high-purity silicon
powder by using
crystalline silicon slice waste
mortar, carrying out heat exchange and heating on fresh
nitrogen and a
reaction product, preheating fluidized silicon
powder, atomizing, spraying into a synthesizer, reacting under specific
process conditions to generate
silicon nitride, introducing excess reaction nitrogen and the generated product into a quench cooler, carrying out heat exchange with the fresh nitrogen, and
quenching to below 150 DEG C; fixing the
crystal form and
granularity of the
silicon nitride structure, entering a gas-
solid separator to complete the separation of Si3N4 and N2, entering the Si3N4 into a packaging inlet of a
packaging machine to be sold, and emptying and discharging N2; the cooling
water circulation system exchanges heat and cools the equipment, and the control cabinet detects and controls the operation condition of the process unit.