The invention discloses an electrostatic spinning instrument with VOCs treatment in the spinning process and adjustable temperature and humidity, including a device casing, a motor, a spinning rod, a wire, a power supply, a first exhaust port, a conversion box, and a Murphy dropper , a burette, a first conduit, a first connecting pipe, a second exhaust port and an electrode rod, a motor is fixed on the bottom side of the inner wall of the device shell by screws, one end of the motor is provided with a spinning rod, and the inner wall of the device shell is The other side of the bottom is fixed with a power supply by screws, the top of the power supply is sleeved with a wire, and an electrode rod is provided at one end of the wire. The electrospinning instrument with VOCs treatment and adjustable temperature and humidity during the spinning process has a simple structure and is easy to operate. The temperature and humidity can be adjusted by adjusting the spinning raw materials inside the conversion box, and the inside of the material box is equipped with chemical treatment drugs to collect and dispose of the volatile VOCs in the spinning process, and the waste after treatment is discharged into the waste box, which greatly reduces pollution and effectively Conducive to protecting the environment.