The invention discloses a preparation method of a
tungsten carbide embedment sample. The preparation method comprises the following steps of respectively weighing an appropriate amount of
tungsten carbide powder and an appropriate amount of
copper powder, and uniformly mixing the
tungsten carbide powder and the
copper powder; preparing a formation agent solution comprising 5-10wt% of water, 5-10wt% of
polyethylene glycol and 80-90wt% of ethyl
alcohol; adding the formation agent solution into a mixed material, and performing uniform stirring to obtain a formation material; performing
compression molding on the formation material to obtain a press blank sample strip; performing anaerobic
sintering on the press blank sample strip in a
sintering furnace; and performing gold-phase
sample preparation, sample
grinding and
polishing on the sintered sample strip to obtain the
tungsten carbide embedment sample. According to the preparation method of the
tungsten carbide embedment sample, the
copper powder and the
tungsten carbide powder are mixed and sintered, the tungsten carbide powder is shaped, thus, the
cutting difficulty of tungsten carbide is reduced, and single-
crystal grain is favorably detected; copper is not fused with tungsten carbide during
sintering, the performance reliability of the single-
crystal grain is ensured; and the tungsten carbide is embedded and fixed by cooledcopper, poly-
crystal grain is difficult to fall off during
grinding and
polishing, and effective proceeding of tungsten carbide detection operation is ensured.