The invention provides organic solvent dehydration equipment of a pervaporation membrane. The equipment comprises a feedstock pump, a preheater, an evaporator, a tail pump, a gas-liquid separator, a superheater, a dehydration device, a penetrating fluid receiving tank, a vacuum unit, a finished product condenser and a finished product tank. According to the equipment, as a dehydration system of a comprehensive membrane is adopted, the quality requirements which cannot be achieved by the traditional method are overcome, and the comprehensive utilization benefit is improved; the tail pump can be used for continuously and quantitatively discharge pollution; the gas-liquid separator can achieve the reduction of entrainment of the evaporator; the heat loss of airflow is compensated by the superheater, so that the temperature of feedstock is guaranteed; the preheater can achieve the reduction of energy consumption by utilizing heat exchange between product steam and feedstock; a membrane component adopts a jacket structure, so that materials are prevented from being liquefied; the feedstock is provided with an online monitor, so that the physical property of a membrane feeding material is ensured to be qualified; produced penetrating fluid is recycled to a distillation column again, and residues are recycled, so that energy is saved, emission is reduced, and the equipment is beneficial to environmental protection.