The present invention discloses a method for preparing flaky silver
powder for low-temperature curing
silver paste, and relates to the technical field of
metal powder metallurgy. In the present invention, a dispersant is added when preparing a
silver nitrate solution, and the speed at which the
silver nitrate solution is dripped into a
reducing agent solution is controlled. After the reaction is completed, a surfactant is added, and spherical silver
powder is obtained after washing and
drying. The spherical silver powder is then ground together with
zirconium oxide grinding balls, and sieving is performed after the
grinding is completed to obtain flaky silver powder. The present invention prepares spherical silver powder of different particle sizes and good particle size uniformity by regulating the
reaction conditions, and adds a surfactant after synthesis to make the silver powder particles in a monodisperse state, and dry-ball mills the silver powder after
drying. The
surfactant free between the silver powder particles can be used as a
grinding aid in the dry ball milling process to prevent the flake powder from sticking together. At the same time, a secondary
coating is performed on the newly exposed surface of the flake powder to make the modification and
coating of the silver flake powder more uniform.