3results about How to "Short residence time" patented technology

This invention belongs to the field of polymer synthesis and microchemical technology, and discloses a method for synthesizing hydroxyl-terminated polybutadiene in a continuous flow microchannel reactor. The preparation method includes mixing butadiene, anhydrous ethanol, 30% hydrogen peroxide, and an antioxidant under nitrogen protection to obtain a raw material liquid, which is then pumped into the microchannel reactor via a high-pressure metering pump. The mixture undergoes preheating initiation and polymerization reactions sequentially, with viscosity monitored by an online viscometer. After the reaction, the product is obtained through gas-liquid separation, sedimentation and stratification, washing, vacuum solvent removal, and filtration. This invention utilizes a microchannel reactor, which provides precise temperature control and stable pressure. Segmented temperature control and online viscosity adjustment prevent reactor blockage, resulting in high product conversion and yield, and uniform molecular weight distribution. By adding auxiliary devices to optimize the process, continuous and stable production is achieved, making it more efficient, environmentally friendly, and controllable.

This utility model discloses a stamping die for rapid demolding, including a fixed die base, a punch base, and a demolding assembly. Through a precisely designed rotating mechanism and abutment teeth, the scrap sheet is smoothly ejected. A drive motor is installed in the die to drive the rotating ring assembly and the core-removing ring seat to generate relative motion, effectively demolding through meshing and lifting actions. A spring device is installed on the bottom surface of the fixed die base to push the punching ring downwards, assisting in the ejection of the scrap sheet. This die reduces the adhesion of scrap to the die surface, improves production efficiency, and extends the die's service life. The overall structure is simple, operation is easy, and it is widely applicable to metal stamping, plastic processing, and other fields.

The application relates to the technical field of plastics, in particular to a preparation method and application of low-temperature-resistant degradable plastics. The low-temperature-resistant degradable plastics contain, in parts by weight, carboxylated polycaprolactone C-PCL: 80-90 parts, modified lignin: 15-20 parts, nano-cellulose: 5-10 parts, crosslinking agent: 2-3 parts, and antioxidant: 0.3-0.5 parts. The modified lignin is prepared by grafting epoxy groups after the alkaline lignin is protected by p-benzene dicarboxaldehyde and hydroxylated; the crosslinking agent is prepared by condensation reaction of vanillin and hexanediamine, and the imine bond contained in the crosslinking agent endows the material with a good degradation rate under acidic conditions. The low-temperature-resistant degradable plastics prepared by the application have good low-temperature mechanical properties and excellent degradation speed under acidic conditions in the case of guaranteeing a certain service life, and are suitable for application to agricultural mulching films in cold environments.