The invention provides an innovative measurement characterization method which integrates X-
ray computed tomography (X-CT) and low-field
nuclear magnetic resonance (NMR) technologies and aims at comprehensively and accurately analyzing the pore structure of the
cement paste. According to the method, nano-crystalline
cellulose (CNF) is introduced into a
cement-based material in multiple dispersion
modes, after standard curing is conducted for 7 days,
nondestructive testing is conducted through the X-
CT technology, two-dimensional and three-dimensional distribution of pores is qualitatively shown, meanwhile, key parameters of micron-sized pores are accurately measured, and a support is provided for macroscopic understanding of the pore structure. Furthermore, in combination with a low-field
nuclear magnetic resonance technology, quantitative evaluation of a nanoscale pore structure is realized, volume information and pore size distribution characteristics of nanoscale pores are accurately acquired, the defect of X-CT in nanoscale detection is overcome, and accurate testing in a full-pore-size range from a gel pore to a non-capillary pore is realized. The
combination method not only covers comprehensive analysis from microcosmic scale to
macroscopic scale, but also realizes accurate
visualization, and provides a new
view angle and methodology for scientific research of the pore structure of the
cement-based material. The method is expected to promote the development of the field of cement-based material pore structures, and provides powerful
technical support and a new research direction for deep research in the field.