The application discloses an in-situ optical-Raman-
mass spectrum combined characterization
system and method, and belongs to the technical field of in-situ characterization. The
system mainly comprises a gas inlet unit, an in-situ electrochemical reaction
cell (in-situ
cell) and a gas outlet unit. In the in-situ
cell device, from top to bottom, there are an optical window, an
electrode one, a diaphragm rich in
electrolyte, an
electrode two and a gas inlet and outlet pipeline. According to different test purposes, the positions of the
working electrode and the counter
electrode (
reference electrode) can be flexibly exchanged, and the
working electrode can be close to the optical window or away from the optical window. The device is in a closed environment, can be tested under
atmosphere control conditions, and can collect and analyze products in time. The application can realize in-situ
optical microscope imaging, Raman and
mass spectrum characterization, can simultaneously capture electrochemical signals-
optical microscope imaging signals, electrochemical signals-Raman signals and electrochemical signals-
mass spectrum signals, and has potential application value in the fields of energy and
catalysis.