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185results about How to "Restrict growth" patented technology

Preparation method of ultrafine grain rare earth magnesium alloy

The invention provides a preparation method of an ultrafine grain rare earth magnesium alloy. The method comprises the following steps of: firstly performing solution treatment on a rare earth magnesium alloy cast ingot to obtain the rare earth magnesium alloy after the solution treatment; then performing heat deformation processing on the obtained rare earth magnesium alloy after the solution treatment to obtain a heat-deformed rare earth magnesium alloy plate, wherein the heat deformation processing temperature is 350 DEG C-450 DEG C; and finally performing accumulative roll bonding with the single-pass rolling reduction of 50% on the obtained heat-deformed rare earth magnesium alloy plate, and annealing to obtain the ultrafine grain rare earth magnesium alloy. According to the preparation method provided by the invention, a heat deformation processing-accumulative roll bonding compound process is firstly adopted to successfully prepare the ultrafine grain rare earth magnesium alloy, and the problem of deterioration of mechanical properties, which is caused by non-uniform distribution of thick and big LPSO (long period stacking ordered) phases in the alloy is effectively solved; and furthermore, the preparation method provided by the invention has the advantages of simple process flow and low equipment cost, and is favorable for further large-scale industrial production.
Owner:XINJIANG TENGXIANG MAGNESIUM PROD CO LTD

Nitrogen-fixing microorganism compound fertilizer and preparation method

The invention belongs to the technical field of agricultural fertilizers, and particularly discloses a nitrogen-fixing microorganism compound fertilizer and a preparation method. The nitrogen-fixing microorganism compound fertilizer comprises polypeptide urea, a phosphatic fertilizer, polypeptide chelating potassium, a compound microorganism agent, a polypeptide compound, a soil conditioner, a medium trace element compound and a nutrition agent; the compound microorganism agent contains nitrogen-fixing bacteria, phosphate solubilizing and potassium solubilizing bacteria, photosynthetic bacteria, probiotics and adsorbate. The preparation method disclosed by the invention comprises the steps of preparing compound microorganism agent fermentation liquor, mixing the fermentation liquor with the adsorbate uniformly and preparing the compound microorganism agent and a microorganism envelope complex agent successively; mixing the microorganism envelope complex agent, a humic acid envelope organic fertilizer and a polypeptide envelope inorganic fertilizer uniformly, under the action of an electric field and a magnetic field, adding medium trace elements, spraying bone glue, and preparing nitrogen-fixing microorganism compound fertilizer particles. The compound fertilizer disclosed by the invention has the effects of adjusting nutrients, stimulating crop growth, improving the agricultural product quality, increasing yield and efficiency, preventing insect diseases, increasing soil fertility, loosening and improving soil quality and the like.
Owner:山东象力丰生物科技有限公司

Method for preparing lithium iron phosphate/carbon composite material by using aniline

The invention discloses a method for preparing a lithium iron phosphate/carbon composite material by using aniline. The method comprises the steps that: trivalent iron salt and a phosphorus-containing compound are respectively dissolved in a certain amount of deionized water, such that solutions are prepared; a proper amount of aniline is dropped into the phosphorus-containing compound solution, and the mixture is stirred, such that the mixture is uniformly dispersed; the trivalent iron salt solution is slowly dropped into the water-soluble phosphorus-containing compound solution comprising aniline; the mixture is stirred for 3-5h under room temperature, such that a FePO4/PANI precursor is synthesized. During the process, when Fe<3+> enters the water solution comprising PO4<3-> and aniline, FePO4 precipitate is first precipitated; simultaneously, Fe<3+> serves as a catalyst for promoting an oxidative polymerization reaction of aniline on the surface of FePO4 particles, such that polyaniline is produced and coated on the surface of FePO4. Therefore, FePO4 particle growth is effectively limited, and the FePO4/PANI precursor with relatively small particle size is obtained. Lithium intercalation is carried out upon the FePO4/PANI precursor, such that lithium iron phosphate/carbon is obtained. With the method, prepared lithium iron phosphate/carbon has the advantages of small particles and excellent electrochemical properties.
Owner:OPTIMUM BATTERY CO LTD

Mineral function fertilizer and preparation method

InactiveCN106673914APrevention and treatment of infectious diseasesRestrict growthCalcareous fertilisersMagnesium fertilisersRare-earth elementHumic acid
The invention belongs to the technical field of agricultural fertilizers, and particularly discloses a mineral function fertilizer and a preparation method. The mineral function fertilizer comprises non-monomer immunoglobulin, photosynthetic bacteria, bacillus, probiotics, rare earth elements, amino acid, vitamins, mineral elements, medium and medium microelements, a nano-carrier and a plant growth regulator. The preparation method comprises the steps of firstly preparing the nano-carrier containing a traditional Chinese medicinal extract, mixing a composite bacterial liquid containing the photosynthetic bacteria, bacillus and probiotics and the nano-carrier evenly, drying, and adding the amino acid and vitamins; adding the rare earth elements, mineral elements and medium and medium microelements under the effects of an electric field and a magnetic field; adding the immunoglobulin and plant growth regulator and mixing evenly; and spraying and pelletizing by using metasilicic acid mineral water, drying and sieving, and spraying a humic acid water solution on an outer layer to prepare the mineral function fertilizer. According to the mineral function fertilizer, the quality of the soil is improved, the fertility of the foil is enhanced, plant diseases and insect pests are effectively avoided, the growth of crops is promoted, and the yield and quality of the crops are improved.
Owner:山东象力丰生物科技有限公司

Process for producing carbon source for processing wastewater

The invention relates to a preparation method of carbon resource for treating wastewater, which belongs to the technical fields of environmental protection, the wastewater and sludge treatment.The invention is characterized in that the acidic fermentation preparation process is used for treating the carbon source of mine wastewater with sulfate and hydrochloric acid, which makes the sludge acidic fermentation products contain 42 percent-85 percent of propionic acid, 5 percent-18 percent of acetic acid and 10 percent-40 percent of butyrate, so the short chain fatty acid is unnecessary to be extracted from supernatant of acidic fermentation reactor; the supernatant of the acidic fermentation reactor is used as the carbon source of sulfate reducing bacteria and directly added into the mine wastewater with the sulfate and the hydrochloric acid and the obtained; the invention solves the key difficult problem that a biological method is used for treating the acidic mine wastewater. The sludge acidic fermentation process has simple operation and the fermentation products, propionic acid, acetic acid and butyrate, can be used as low cost carbon sources for treating acidic mine wastewater biologically; at the same time, the process achieves the quantity reduction, resource utilization and stabilization of the sludge.
Owner:TAIYUAN UNIV OF TECH

Method for producing nano-silver composite antibacterial agent through spray drying

The present invention relates to a method for industrial production of a nano-silver composite antibacterial agent. In the prior art, a particle size of nano-silver is large and is not easily adjusted, nano-silver is unstable and is easily agglomerated, and a particle size of nano-silver composite particles is non-uniform. A purpose of the present invention is mainly to solve problems in the prior art. According to the present invention, the method for producing the nano-silver composite antibacterial agent is provided, wherein the method comprises the following steps: a) mixing silane having an amine functional group, alkoxy silane, silver nitrate or silver acetate, and water to form a mixing liquid; b) pumping the mixing liquid into a rotation disc at a high-speed rotation state in a dryer, carrying out centrifugal atomization to obtain tiny liquid droplets, and carrying out cyclone drying with hot air to obtain dried particle powder; c) separating the particle powder with a cyclone separator, and then collecting to obtain the nano-silver composite antibacterial agent with a uniform particle size. With the present invention, problems in the prior art are solved, and the technical scheme of the present invention can be used in production of antibacterial materials with characteristics of long acting and broad spectrum.
Owner:CHANGZHOU YINGZHONG NANO TECH

Preparation method of micro-mesoporous ZSM-5 zeolite molecular sieve

The invention discloses a preparation method of a micro-mesoporous ZSM-5 zeolite molecular sieve. According to the method, sodium metaaluminate serves as an aluminum source, ethyl orthosilicate serves as a silicon source, single-end quaternary ammonium surfactants and tetrapropyl ammonium hydroxide serve as template agents, and the mesoporous zeolite molecular sieve with a ZSM-5 microporous structure is subjected to hydro-thermal synthesis in an alkaline environment. The single-end quaternary ammonium surfactants can form ZSM-5 micropores in an oriented manner, hydrophobic tail chains of the single-end quaternary ammonium surfactants can limit micro-crystal growth, mesopore formation is promoted, mesoporous uniformity is improved by introducing second template agents, specific surface area is increased, and the finally obtained ZSM-5 zeolite molecular sieve has the advantages of good hydrothermal stability, high acid catalysis activity and the like of a conventional zeolite molecular sieve, is quite beneficial to reaction with macromolecules and effectively solves the problem of mass transfer limitation of a single-pore zeolite molecular sieve. The application value of the zeolite molecular sieve in the field of catalysis, adsorption separation and the like is greatly improved.
Owner:SOUTH CHINA UNIV OF TECH

MOFs/water hyacinth derivative material, preparation method thereof and degradation method of organic pollutants

The invention belongs to the technical field of composite materials. The invention provides an MOFs/water hyacinth derivative material, a preparation method thereof and a degradation method of organic pollutants. The MOFs/water hyacinth derivative material is composed of water hyacinth biochar and a cobalt-based zeolite imidazate framework embedded in the water hyacinth biochar. The water hyacinth biochar is used as a carrier of the MOFs material, and the prepared MOFs/water hyacinth derivative material has excellent stability, conductivity and specific surface area, and is more beneficial to charge transfer and mass transfer processes between cobalt active sites and pollutants; and due to the pore limiting effect of the water hyacinth biochar, crystal growth of the MOFs derivative metal oxide in the thermal decomposition process can be effectively limited. The MOFs/water hyacinth derivative material disclosed by the invention has strong capability of activating persulfate to generate free sulfate radicals, so that the MOFs/water hyacinth derivative material has efficient and lasting capability of catalytically oxidizing organic matters, and the defects that a catalyst is easy to agglomerate, the activation time of persulfate is long and the like are effectively overcome.
Owner:GUANGDONG UNIV OF TECH

Quantum-dot-doped aluminium phosphate mesoporous glass nanometer compound and preparation method thereof

The invention discloses a novel near-infrared quantum-dot-doped aluminium phosphate mesoporous glass nanometer compound and a preparation method thereof. The PbS-quantum-dot AlPO4 mesoporous glass nanometer compound is AlPO4 mesooprous glass doped with PbS quantum dots with different dimensions. The preparation method of the quantum-dot-doped aluminium phosphate mesoporous glass nanometer compound comprises the following steps: step 1, preparing a PbS quantum dot solution with two kinds of luminescence peak-value wavelength and a mixed solution with fresh quantum dots and ripened quantum dots; step 2, immersing AlPO4 mesoporous glass prepared by employing a sol-gel method in the quantum dot solution of the step 1 for one time or for independently two times; and step 3, taking the immersed mesoporous glass out from the solution, and performing moistening washing and drying to obtain the PbS-quantum-dot AlPO4 mesoporous glass nanometer compound. Tests prove that under pumping of near infrared, the PbS-quantum-dot AlPO4 mesoporous glass nanometer compound is capable of generating broadly tunable luminescence or double-peak luminescence at near infrared wave band, and has important application to the field of broadband optical transmission, multiband response optical communication materials and devices.
Owner:SHANGHAI INST OF OPTICS & FINE MECHANICS CHINESE ACAD OF SCI

Preparation method of mesoporous-microporous dual pore ZSM-5 zeolite nano sheet

The invention discloses a preparation method of a mesoporous-microporous dual pore ZSM-5 zeolite nano sheet. According to the method, sodium meta-aluminate is taken as the aluminum source, ethyl n-silicate is taken as the silicon source, a Bola type amphiphilic molecule with dual quaternary ammonium heads is taken as the template; and the mesoporous-microporous dual pore ZSM-5 zeolite nano sheet is synthesized through a hydrothermal method under an alkaline condition. The Bola type dual head quaternary ammonium surfactant can form ZSM-5 micro pores, moreover, the hydrophobic tail chains of thesurfactant can inhibit the growth of microcrystal, and thus uniform and sequenced mesopores are formed. The nano sheet has a 90 degree intersected intergrowth structure and has a card house shape. The repeatability is good, and the synthesized ZSM-5 zeolite nano sheet has the advantages of a common zeolite molecular sieve such as good hydrothermal stability, high acid catalytic activity, and thelike. Moreover, the nano sheet is beneficial for the reactions that macro molecules participate in. The mass transfer limitation of a single-channel zeolite molecular sieve is broken through, and theapplication value of zeolite molecular sieves in fields such as catalysis, adsorption separation, and the like, is greatly increased.
Owner:SOUTH CHINA UNIV OF TECH

Knapsack traveling automatic fertilizer spreader

The invention provides a knapsack traveling automatic fertilizer spreader, relating to a machine for spreading fertilizer. A charging basket opening is provided with a basket cover, the bottom part of the charging basket is provided with an underpot internally provided with an upper end part of a feeding pipe which is fixed by a flexible fixator, the feeding pipe is in an L-shaped, and the corner is an arc transition. In addition, related facilities can be added on the fertilizer spreader as follows: the feeding pipe is arranged with a guy ring and a locking ring matched with the guy ring so as to control the switch of the fertilizer spreading; a trough matched with the feeding pipe is arranged below the front part of the charging basket; a filter screen is arranged in the charging basket; the lower end part of the feeding pipe is connected with a manifold; the branch pipe of the manifold is connected with a spray pipe, etc. The design principle of the invention is that granular fertilizer has certain fluidity, and the fertilizer can flow outwards to form a spreading effect under the vibration effect when a person carries the charging bucket on the back. The invention has the beneficial effects of directly spreading on crops, saving power, labor and fertilizer, having good fertilizing effect, simple construction and low cost, and being favor of protecting human bodies; and compared with spreading the fertilizer manually, the invention improves the working efficiency by 3-4 times.
Owner:胡建波

Preparation method of hollow ferric oxide cathode material in porous structure

The invention discloses a preparation method of a hollow iron oxide cathode material in a porous structure. The preparation method comprises the steps of weighing an organic ligand compound and iron salt at a mole ratio of 1:(1-10), adding a solvent, performing uniform stirring and dispersion, allowing a mass ratio of a solute to the solvent to be 1:(100-800), preparing a high polymer coordinationpolymer by a hydrothermal/solvothermal method under conditions of a pH (potential of hydrogen) value of 3-11, the temperature of 100-200 DEG C and reaction time of 10-72h, roasting the prepared polymer at a 200-800 DEG C oxygen-containing atmosphere, and obtaining the hollow iron oxide cathode material in a multilevel structure. A hollow ferric oxide particle in the porous structure is obtained by a hydrothermal/solvothermal - high-temperature burning two-step method; the method has the advantages that ferric ions are arrayed orderly in a long range in a lattice; an organic framework supporting the ferric ion can limit growth of the ferric oxide particle in a three-dimensional direction via aerobic burning; the obtained ferric oxide particle is good in particle size uniformity and dispersity; and the increase and improvement of a multiplying factor and cycle performance of a material are facilitated.
Owner:HEFEI GUOXUAN HIGH TECH POWER ENERGY
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