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348 results about "X-ray photoelectron spectroscopy" patented technology

X-ray photoelectron spectroscopy (XPS) is a surface-sensitive quantitative spectroscopic technique that measures the elemental composition at the parts per thousand range, empirical formula, chemical state and electronic state of the elements that exist within a material. Put more simply, XPS is a useful measurement technique because it not only shows what elements are within a film but also what other elements they are bonded to. This means if you have a metal oxide and you want to know if the metal is in a +1 or +2 state, using XPS will allow you to find that ratio. However at most the instrument will only probe 20nm into a sample.

Magnetic toner, process for production thereof, and image forming method, apparatus and process cartridge using the toner

A magnetic toner includes: magnetic toner particles each comprising at least a binder resin and magnetic toner, and inorganic fine powder. The magnetic toner has an average circularity of at least 0.970, and a magnetization of 10-50 Am2 / kg at a magnetic field of 79.6 kA / m. The magnetic powder comprises at least magnetic iron oxide. The magnetic toner particles retain carbon in an amount of A and iron in an amount of B at surfaces thereof as measured by X-ray photoelectron spectroscopy, satisfying: B / A<0.001. The binder resin comprises a resin formed by polymerization of a monomer comprising at least styrene monomer. The magnetic toner has a residual styrene monomer content of less than 300 ppm, and contains at least 50% by number of toner particles satisfying a relationship of: D / C<=0.02, wherein C represents a volume-average particle size of the magnetic toner, and D represents a minimum distance between the surface of a magnetic toner particle and magnetic powder particles contained in the magnetic toner particle. Owing to the above features, the magnetic toner can exhibit good electrohotographic performances, including excellent chargeability and little transfer-residual toner, even in a cleanerless-mode image forming system.
Owner:CANON KK

Method for direct recovery and restoration of lithium ion battery positive electrode material

The invention discloses a method for direct recovery and restoration of a lithium ion battery positive electrode material, and belongs to the field of resource recycling. According to the method, waste positive electrode pieces of lithium cobaltate or lithium nickel manganese cobalt multi-element layered oxide or a positive electrode piece leftover material and defective products are used as a positive electrode material; the materials are classified according to the type of binder by component analysis, the binder is directly damaged, cleaning and separation of the positive electrode material and a current collector are realized; by use of a heavy liquid separation principle, the positive electrode and a conductive agent are separated; the positive electrode failure mechanism is studied by use of SEM (scanning electron microscope), XRD (X-ray diffraction), STEM (scanning transmission electron microscope), XPS (X-ray photoelectron spectroscopy) and other analysis means; chemical components of the positive electrode material with the layered structure not damaged can be repaired by high temperature roasting, the layered structure of the positive electrode material with disordered and defective crystal lattice can be repaired by dissolving with a hydrothermal reaction and then precipitation, and the positive electrode material with good charge discharge performances can be again obtained. The method avoids the dissolving leaching process, reduces waste liquid generation, and simplifies the technological process.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI
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