188 results about "Stannous ion" patented technology

During the preparation of ordered nano structure metal material, correponding colloid crystal template is first prepared via capillary abstraction self-assembling method. Spacer is set between two parallel plates to form micro passage in the same thickness as the spacer, one end of the micro passage is soaked into microsphere emulsion so that the emulsion is driven by capillary effect to the micro passage to form ordered arrangement. The bottom of the micro passage is then soaked into sensitizing stannous ion solution, so that the surface of the microsphere has one layer of sensitizing stannous ion adsorbed and is sensitized. The present invention features the surface seed growing method and colloidal crystal of polystyrene microsphere as template. When the template is set inside chemical plating solution, some interval is formed between microspheres owing to electrostatic repulsion, and the interval permits forming metal shell in the outer surface of the medium microsphere.

Disclosed are oral compositions comprising a stannous ion source, a fluoride ion source, and a polymeric mineral surface active agent that binds stannous, said compositions providing adequate therapeutic efficacy with minimal side effects of tooth staining and astringency. The composition simultaneously provides reduction and control of supragingival calculus. The present oral care compositions may be formulated as single phase or dual phase compositions. The present invention also provides a method for effective delivery of stannous-containing compositions with minimal side effects of tooth staining or astringency and with effective tartar control by administering to a subject a stable dentifrice composition comprising a clinically effective amount of stannous fluoride and / or other stannous salts in combination with a fluoride ion source and a polymeric mineral surface active agent, preferably a phosphate- or phosphonate-containing polymer.

An oral care composition containing a source of stannous ions, a source of fluoride ions and an insoluble source of zinc ions, such as zinc oxide. The composition contains an amount of citric acid sufficient to increase the level of soluble zinc ions.

The present invention relates to oral care compositions comprising stannous ions, a mint-type flavor oil, a protectant component that prevents generation of off odor and off taste in the composition, and orally acceptable carriers. The mint-type oils include peppermint, spearmint and corn mint. Suitable protectant components include copper salts and carbonyl compounds such as ascorbic acid; cis-jasmone; 2,5-dimethyl-4-hydroxy-3(2H)-furanone; 5-ethyl-3-hydroxy-4-methyl-2(5H)-furanone; vanillin; ethyl vanillin; anisaldehyde; 3,4-methylenedioxybenzaldehyde; 3,4-dimethoxybenzaldehyde; 4-hydroxybenzaldehyde; 2-methyoxybenzaldehyde; 4-methoxybenzaldehyde; benzaldehyde; cinnamaldehyde (3-phenyl-2-propenal); hexyl cinnamaldehyde; α-methyl cinnamaldehyde; ortho-methoxy cinnamaldehyde; α-amyl cinnamaldehyde; and combinations thereof. The oral care composition may be a dentifrice.

Oral care composition for preventing and / or reducing calories, including: at least about 0.005%, of metal ions wherein the composition comprises at least about 0.005% of zinc ions and optionally comprises from about 0.001% to about 3%, of stannous ions; at least about 100 ppm of fluoride ions; from about 0.03% to about 10% of a mineral surface active agent selected from homopolymers of itaconic acid, homopolymers of acrylic acid, copolymers of maleic acid and acrylic acid, copolymers of maleic anhydride or acid with methyl vinyl ether, and mixtures thereof; at least 5% of water; less than 10% fused silica, calcium based abrasives, and mixtures thereof; less than 5% of polyphosphates having n+3 or higher; and wherein the weight ratio of metal ion to the mineral surface active agent is equal to or less than about 0.5.

The present invention relates to flavor oils including mint-, fruit- and spice-type flavors that are specially processed to substantially eliminate low-molecular weight sulfur compounds, in particular dimethyl sulfoxide (DMSO), which has been found to be the main precursor of malodorous species such as dimethyl sulfide and methyl mercaptan. These malodorous species are produced via oxidation-reduction reactions involving such sulfur-containing compounds present in flavor oils. A preferred processing method is an aqueous-washing process, which has advantages of being simple, inexpensive and easy to implement while importantly avoiding the problems of typical processes including non-selective removal of desirable components and subjecting the flavor oils to extreme conditions that may destroy other components and result in undesirable changes in flavor or odor character. Other processing methods to selectively remove non-desired components include (1) distillation to remove polar low boiling point components, (2) filtration through adsorbents selective for sulfur compounds, (3) countercurrent extraction and (4) column chromatography. The processing methods may optionally be followed by reengineering to add back desired components that may have been removed or altered during the processing. The specially processed flavor oils are particularly useful in oral care compositions comprising components with chemical reducing capability such as stannous ions, which react with the sulfur-containing compounds to produce malodorous products.

The present invention relates to oral care compositions comprising stannous ions, a mint-type flavor oil, a protectant component that prevents generation of off odor and off taste in the composition, and orally acceptable carriers. The mint-type oils include peppermint, spearmint and corn mint. Suitable protectant components include copper salts and carbonyl compounds such as ascorbic acid; cis-jasmone; 2,5-dimethyl-4-hydroxy-3(2H)-furanone; 5-ethyl-3-hydroxy-4-methyl-2(5H)-furanone; vanillin; ethyl vanillin; anisaldehyde; 3,4-methylenedioxybenzaldehyde; 3,4-dimethoxybenzaldehyde; 4-hydroxybenzaldehyde; 2-methyoxybenzaldehyde; 4-methoxybenzaldehyde; benzaldehyde; cinnamaldehyde (3-phenyl-2-propenal); hexyl cinnamaldehyde; α-methyl cinnamaldehyde; ortho-methoxy cinnamaldehyde; α-amyl cinnamaldehyde; and combinations thereof. The oral care composition may be a dentifrice.

Oral care compositions having improved efficacy for preventing and / or reducing caries, containing: from about 0.001% to about 5%, of metal ions wherein the composition comprises at least about 0.001%, of stannous ions and optionally comprises from about 0.001% to about 4%, of zinc ions; at least about 100 ppm, by weight of the composition, of fluoride ions; at least about 0.03%, by weight of the composition, of a mineral surface active agent selected from homopolymers of itaconic acid, homopolymers of acrylic acid, copolymers of maleic acid and acrylic acid, copolymers of maleic anhydride or acid with methyl vinyl ether, and mixtures thereof; at least 5%, of water; less than 10%, by weight of the composition, of fused silica, calcium based abrasives, and mixtures thereof; less than 5%, of polyphosphates having n+3 or higher; wherein the weight ratio of total metal ion to the mineral surface active agent is equal to or less than 0.5.

The present invention relates to oral compositions comprising a stannous ion source, a fluoride ion source, and a polymeric mineral surface active agent that binds stannous, said compositions providing adequate therapeutic efficacy with minimal side effects of tooth staining and astringency. The composition simultaneously provides reduction and control of supragingival calculus. The present oral care compositions may be formulated as single phase or dual phase compositions. The present invention also provides a method for effective delivery of stannous-containing compositions with minimal side effects of tooth staining or astringency and with effective tartar control by administering to a subject a stable dentifrice composition comprising a clinically effective amount of stannous fluoride and / or other stannous salts in combination with a fluoride ion source and a polymeric mineral surface active agent, preferably a phosphate- or phosphonate-containing polymer.

An oral care composition having a first phase of clinically efficacious 2,4,4′-trichloro 2′-hydroxydiphenyl ether admixed in a first orally acceptable aqueous vehicle, and a second phase having a stannous salt (such as stannous fluoride) admixed in a second orally acceptable aqueous vehicle. The second phase has no less than 10 molar percent of soluble stannous ion respective to a mathematical sum of moles of the soluble stannous ion and moles of the stannous salt in the second phase. In one embodiment, the two phases are provided in a dual-tube toothpaste oral care kit.

Process for heat treating precipitated silica to improve stability. Oral care compositions comprising such heat treated precipitated silica abrasives and a stannous ion source.

An oral care composition containing a source of stannous ions, a source of fluoride ions and an insoluble source of zinc ions, such as zinc oxide. The composition contains an amount of citric acid sufficient to increase the level of soluble zinc ions.

Disclosed are methods for reducing the staining of dentifrice composition containing stannous comprising administering to a subject the dentifrice composition. The dentifrice composition is a dual phase dentifrice and is contained in physically separated compartments of a dentifrice dispenser. The first dentifrice composition comprises an effective amount of one or more linear polyphosphates having an average chain length of about 4 or more and has a total water content of up to about 20%. The second dentifrice composition comprises an effective amount of stannous ions. The molar ratio of polyphosphate anion to stannous ion is from about 0.2:1 to about 5:1 and the efficacy of the stannous ion in the dentifrice is not reduced by the polyphosphate. The dentifrice composition may alternatively be a single phase dentifrice. The single phase dentifrice will comprise an effective amount of one or more linear polyphosphates having an average chain length of about 4 or more and an effective amount of a stannous ion. The single phase dentifrice has a total water content of up to about 20%, the stannous ion is not delivered from stannous fluoride, a molar ratio of polyphosphate anion to stannous ion is from about 0.2:1 to about 5:1, and the efficacy of the stannous ion in the dentifrice is not reduced by the polyphosphate.

Processes for creating versatile and selective metal patterns (such as copper and nickel) combine the use of PEM coatings, microcontact printing (MCP), and electroless deposition. MCP is used to pattern a charged catalyst (such as palladium and stannous ions) onto oppositely charged PEM coated substrates. The substrate is then placed into an electroless deposition bath where a metal selectively plates at the catalyzed regions.

The present invention relates to flavor oils including mint-, fruit- and spice-type flavors that are specially processed to substantially eliminate low-molecular weight sulfur compounds, in particular dimethyl sulfoxide (DMSO), which has been found to be the main precursor of malodorous species such as dimethyl sulfide and methyl mercaptan. These malodorous species are produced via oxidation-reduction reactions involving such sulfur-containing compounds present in flavor oils. A preferred processing method is an aqueous-washing process, which has advantages of being simple, inexpensive and easy to implement while importantly avoiding the problems of typical processes including non-selective removal of desirable components and subjecting the flavor oils to extreme conditions that may destroy other components and result in undesirable changes in flavor or odor character. Other processing methods to selectively remove non-desired components include (1) distillation to remove polar low boiling point components, (2) filtration through adsorbents selective for sulfur compounds, (3) countercurrent extraction and (4) column chromatography. The processing methods may optionally be followed by reengineering to add back desired components that may have been removed or altered during the processing. The specially processed flavor oils are particularly useful in oral care compositions comprising components with chemical reducing capability such as stannous ions, which react with the sulfur-containing compounds to produce malodorous products.

Oral care compositions comprising citrulline and stannous ion source with a specific pH range are provided for promoting Gum Health of a user.

Oral care compositions comprising an acidic amino acid and stannous ion source are provided for promoting Gum Health of a user.

Oral care compositions comprising an amino acid and stannous ion source, especially in the absence of zinc ion source, are provided for promoting Gum Health of a user.

The invention discloses electroplating solution and a process for electroplating white copper tin by alkaline solution. The electroplating solution is characterized by comprising pyrophosphate, soluble copper salt, soluble tin salt, phosphoric acid, a stannous ion stabilizer, conducting salt and a right amount of additive, wherein the pyrophosphate is used as a complexing agent; the soluble copper salt and the soluble tin salt are used as main salt; and the phosphoric acid is used as an electroplating solution pH regulator. The electroplating solution disclosed by the invention is simple in composition, is convenient to maintain and has a wide current density range; the alkaline condition of the electroplating solution can be used for electroplating active metals and base materials easy to corrode.

The present invention relates to a single phase oral care composition comprising:a. a stannous saltb. a potassium saltc. a chelantd. monofluorophosphate (MFP).The composition of the invention has been found to allow prolonged contact between stannous ion and nitrate ion in a single dentifrice without toxic effects or insoluble products. The invention further provides for the maintenance of an efficacious fluoride ion level.

Oral care composition comprises a stannous ion source and a thickener comprising at least 2 agents selected from the group consisting of: i) a linear sulfated polysaccharide; ii) a natural gum; iii) and a non-ionic cellulose derivative. A method for treating the oral cavity comprises administering to the oral cavity the oral care composition.

Disclosed are methods for reducing the staining of dentifrice composition containing stannous comprising administering to a subject the dentifrice composition. The dentifrice composition is a dual phase dentifrice and is contained in physically separated compartments of a dentifrice dispenser. The first dentifrice composition comprises an effective amount of one or more linear polyphosphates having an average chain length of about 4 or more and has a total water content of up to about 20%. The second dentifrice composition comprises an effective amount of stannous ions. The molar ratio of polyphosphate anion to stannous ion is from about 0.2:1 to about 5:1 and the efficacy of the stannous ion in the dentifrice is not reduced by the polyphosphate. The dentifrice composition may alternatively be a single phase dentifrice. The single phase dentifrice will comprise an effective amount of one or more linear polyphosphates having an average chain length of about 4 or more and an effective amount of a stannous anion. The single phase dentifrice has a total water content of up to about 20%, the stannous ion is not delivered from stannous fluoride, a molar ratio of polyphosphate anion to stannous ion is from about 0.2:1 to about 5:1, and the efficacy of the stannous ion in the dentifrice is not reduced by the polyphosphate.

The invention discloses a method for carrying out selective area deposition of silver nano particles on the surface of a PDMS (Polydimethylsiloxane) elastic body, which implements selective area deposition of the silver nano particles by using a PDMS wrinkle pattern as a template and combining an electroless deposition technology. After being processed in an oxygen plasma, pre-stretched PDMS retracts to obtain the wrinkle pattern; the pattern is used as the template for selectively transferring stannous ions on a PDMS substrate; and finally, electroless deposition of the silver nano particles is carried out to obtain a selective area pattern of the silver nano particles. The PDMS is low in price, has excellent elasticity and light transmission, has no toxicity, is easy to process and is one of micro-fluidic chip materials which are the most widely applied currently. The electroless deposition technology is one of main methods of constructing a submicron-class metal thin film on the surface of the substrate, is simple to operate and lower in cost, and has no limitation to both the shape and the size of a sample due to the liquid phase reaction. The method disclosed by the invention has the characteristics of rapidness and simplicity and application of expensive materials and complex instruments and harsh process conditions are avoided.

Oral care compositions comprising a neutral amino acid and stannous ion source are provided for promoting Gum Health of a user.

This invention relates to oral care compositions comprising a first source of zinc which is zinc citrate, a second source of zinc which is zinc oxide or zinc lactate, a stannous ion source, and a polyphosphate, as well as to methods of using and of making these compositions.

An oral care composition comprising a fused silica abrasive and a stannous ion source.

The invention relates to the field of oral nursing, in particular to an oral nursing composition containing polyphenol compounds, a stannous ion source and a soluble non-antioxidant alkaline earth metal ion source and a method for reducing oxidation of the polyphenol compounds in the oral nursing composition containing the stannous ion source and the polyphenol compounds.

An oral care composition containing a stannous ion source, a zinc ion source, a polyphosphate, and a thickening agent. The thickening agent contains polyvinylpyrrolidone, a polysaccharide gum and carboxymethyl cellulose. The compositions have excellent rheology properties.

The present invention relates to a single phase oral care composition comprising:a. a stannous salt delivering a stannous ion;b. a potassium salt delivering a potassium ion wherein the potassium salt is selected from potassium nitrate, potassium gluconate, potassium citrate, potassium chloride, potassium tartrate, potassium bicarbonate, and mixtures thereof;c. a chelant;d. a fluoride ion source; ande. less than 0.01% of an alkyl sulphate or an alkyl ethoxylate sulphate;wherein the oral care composition provides a soluble fluoride ion level of greater than 50% of the total fluoride ion.The composition of the invention has been found to allow prolonged contact between stannous ion and nitrate ion in a single dentifrice without toxic effects or insoluble products. The invention further provides for the maintenance of an efficacious fluoride ion level.

The present disclosure provides low water dentifrice compositions comprising an effective amount of a zinc ion source, a stannous ion source, a polyphosphate and an acid in a calcium pyrophosphate base. The acid lowers the pH of the composition to enable stabilization of the metal ions and extend shelf-life of the composition.