The invention belongs to the field of nano materials, and discloses a preparation method of a carbon material loaded tubular
carbon nitride photocatalyst. The photocatalyst with large specific surface area, multiple active sites, high
photon-generated carrier separation and migration rate, low
photon-generated carrier
coincidence rate, visible light absorption
red shift, high photocatalytic activity and high stability is obtained by adjusting the
mass fraction of the carbon material. The preparation method comprises the following steps: S1, uniformly mixing the carbon material with
sodium chloride,
potassium chloride,
lithium chloride and
melamine, and calcining in a
corundum crucible; in the step S1, the preparation method of the carbon material comprises the following steps: (1)
cutting the white part of the shaddock peel into blocks,
drying, soaking in a KOH solution, and freeze-
drying; (2) calcining a sample in a tubular furnace, and washing the sample with HNO3 and
ultrapure water until the sample is neutral to obtain a carbon material; and S2, washing the product with
ultrapure water and
ethanol,
drying and collecting. The photocatalyst obtained by the invention promotes the improvement of the
hydrogen production performance by photolysis of water, and provides a new thought for further development of efficient photocatalysts.