The present invention discloses a preparation apparatus and an oxidative
combustion method of an organic
tritium carbon sample. The preparation apparatus comprises a reaction working
pipe, an oxidative
combustion furnace and an absorption device, wherein the reaction working
pipe comprises a
pipe body, a first gas inlet hole, a second gas inlet hole and a gas outlet hole, a heating zone is arranged in the oxidative
combustion furnace and is sequentially divided into a catalytic
reaction zone, a sample stacking zone and a sample
recovery zone, the lower portions are respectively provided with a temperature controller, the reaction working pipe is horizontally arranged in the oxidative combustion furnace, the pipe body penetrates through the heating zone, the gas outlet hole is connected to the absorption device, the absorption device comprises a collection
bottle and a low temperature
cold trap, the collection
bottle is arranged in the low temperature
cold trap, and the gas outlet hole is connected to the collection
bottle. According to the present invention, the structure is simple, the problems of
open fire production caused by combustion,
quartz pipe bursting, incomplete sample combustion and the like during the sample treatment process are effectively prevented, the generated water has the clear color, the sample treatment capacity is high, the sample
absorption rate of the combustible materials such as
tritium and carbon-14 is substantially improved, and the sample measurement requirements in the modern industry are met.