The invention relates to a method for separating and purifying waste
boric acid liquid in formed foil waste liquid and concentrating
boric acid, which comprises the following steps: adding
ammonia water into the
boric acid waste liquid to promote the waste liquid to separate out aluminum
hydroxide precipitate, and separating the aluminum
hydroxide precipitate from the waste liquid to obtain primary separated liquid; carrying out
ultrafiltration on the primary separated liquid, adding boric acid or
citric acid, and promoting
ammonium pentaborate in the primary separated liquid to be hydrolyzed into boric acid, so as to obtain acidizing fluid; freezing and crystallizing the acidizing fluid until
solid boric acid is separated out; and carrying out
solid-liquid separation on the precipitated boric acid
solid mixed solution, and carrying out
vacuum drying or normal-pressure
drying on the boric acid solid for recycling. According to the treatment method and
system, aluminum and
ammonium radicals can be efficiently separated from the aging waste liquid,
ammonium pentaborate is converted into boric acid to be efficiently recycled, the environment can be better protected, the purity of the recycled boric acid product and recycling of the recycled boric acid product in the formed foil industry are guaranteed, and the operation cost of an enterprise is reduced.