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Method for simultaneous and in-situ capture of phenolic compounds and ammonia in cigarette mainstream smoke by using liquid adding filtration discs

The invention discloses a method for simultaneous and in-situ capture of phenolic compounds and ammonia in cigarette mainstream smoke by using liquid adding filtration discs. The method comprises: A)mainstream smoke capture, wherein qualified cigarettes are selected according to weight and smoking resistance, a pre-treated filtration disc and a standard filtration disc are placed into a cigaretteclamper, the pre-treatment filtration disc is used at 1-3 h after a pre-treatment liquid is added, the cigarette is smoked by a linear smoking machine under a standard condition, each pore channel smokes four cigarettes, and the mainstream smoke of the cigarette is captured by a Cambridge filtration disc; B) filtration disc extraction, wherein the two filtration discs are placed into a hydrochloric acid solution with a concentration of 0.01 mol / L after the smoking is completed, oscillation is performed for 40 min at a room temperature at a rotation speed of 150 r / min, filtering is performed with a 0.45 [mu]m aqueous phase filtration membrane, and the sample is taken and is respectively analyzed through liquid chromatography and ion chromatography; and C) instrument analysis condition setting, wherein the liquid chromatography instrument conditions for determining the phenol-based compounds use the YC / T255-2008 cigarettes-determination of major phenolic compounds in mainstream cigarette smoke-high-performance liquid chromatography method, and the ion chromatography instrument conditions for determining the ammonia use YC / T 377-2010 cigarettes-determination of ammonia in mainstreamcigarette smoke-ion chromatography method.
Owner:中国烟草总公司贵州省公司
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