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38 results about "Dichlorophenylphosphine" patented technology

Dichlorophenylphosphine is an organophosphorus compound with the formula C₆H₅PCl₂. This colourless viscous liquid is commonly used in the synthesis of phosphine ligands. Dichlorophenylphosphine is commercially available. It may be prepared by an electrophilic substitution of benzene by phosphorus trichloride, catalyzed by aluminium chloride.

Preparation method of integrated phosphine light emission carbazolyl organic photoelectric material

The invention discloses a preparation method of 3, 7-dicarbazolyl-5-phenyl benzoxphosphine heteroindole, and belongs to the technical field of organic synthesis. The method comprises the following steps: carrying out a coupling reaction on 1, 4-difluoro-2-nitrobenzene under the catalysis of copper to obtain 4, 4 '-difluoro-2, 2'-dinitro-biphenyl, carrying out stannous chloride reduction and amido diazonium salt process conversion to obtain 4, 4 '-difluoro-2, 2'-diiodo-biphenyl, and carrying out 4, 4 '-difluoro-2, 2'-diiodo-biphenyl. The preparation method comprises the following steps: carrying out lithium-iodine exchange on 2, 2 '-diiodo-biphenyl, carrying out nucleophilic substitution reaction on the 2, 2'-diiodo-biphenyl and dichlorophenylphosphine to generate phenylphosphine heterobenzoindole, oxidizing the phenylphosphine heterobenzoindole to form phenylphosphine oxide heterobenzoindole, and carrying out substitution reaction on carbazole and aryl fluoride to synthesize the phosphine oxide type organic small molecular luminescent material with fluorescence activity. The 3, 7-dicarbazolyl-5-phenyl benzoxphosphine heteroindole synthesized by the method not only can be used as a photocatalyst in the field of organic synthesis, but also can be used as an organic photoelectric material.
Owner:ANYANG INST OF TECH

Preparation method of phosphine oxide type TADF organic photoelectric material

The invention discloses a preparation method of a symmetric phosphine oxide type TADF organic photoelectric material, and belongs to the field of organic functional materials. 2, 2 '-dinitro-biphenyl is subjected to stannous chloride reduction, amido acylation, electricity-rich aromatic ring bromination reaction and acid deacylation of a protecting group to form free amido, the amido is converted into 5, 5'-dibromo-2, 2 '-diiodo-biphenyl through a diazonium salt process, then the 5, 5'-dibromo-2, 2 '-diiodo-biphenyl is converted into 5, 5'-dibromo-2, 2 '-diiodo-biphenyl, and the 5, 5'-dibromo-2, 2 '-diiodo-biphenyl is converted into 5, 5 The preparation method comprises the following steps: carrying out lithium-iodine exchange on 2, 2 '-diiodo-biphenyl, carrying out nucleophilic substitution reaction on the 2, 2'-diiodo-biphenyl and dichlorophenylphosphine to generate phenylphosphine heterobenzoindole, oxidizing the phenylphosphine heterobenzoindole to form phenylphosphine oxide heterobenzoindole, and carrying out coupling reaction on brominated aromatic hydrocarbon and heteroaromatic hydrocarbon under the catalysis of copper to synthesize the small organic molecule luminescent material with fluorescent reactive oxygen species. The 2, 8-diphenothiazinyl-5-phenyl benzoxphosphine heteroindole synthesized by the method has the potential of becoming an organic micromolecule electroluminescent material and being used as a photosensitizer for organic photoreaction, and fits the development trend of multifunctional application of organic micromolecule materials.
Owner:ANYANG INST OF TECH
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