The invention discloses an environment-friendly green
ferrocene purification method, and belongs to the technical field of environment-friendly green
ferrocene purification methods. According to the method, a
steam distillation sublimation and
plasma stirring synergistic method is adopted, a
steam distillation technology is adopted, the characteristic that
ferrocene sublimates at the temperature of 100 DEG C is utilized, an
inert environment is provided through steam, the
system partial pressure is reduced, high-temperature
decomposition is avoided,
water diffusion steam distillation is adopted, the condensation blocking risk is reduced, the
mass transfer efficiency is improved, and non-thermal
plasma is introduced; and uniform stirring is realized through
active particles such as high-energy electrons and free radicals, so that the
retention time of ferrocene is shortened, and the generation of
caking is reduced. Light component impurities in ferrocene are reduced through
desolvation treatment, high-purity ferrocene is obtained, the
caking problem is solved,
solid waste
discharge is reduced, the
solvent can be recycled, the method has the advantages of being simple in process,
environmentally friendly and high in product purity, operation convenience and efficiency are effectively improved, and the method is suitable for industrial production. The industrial continuous automatic production of the ferrocene is favorably realized.