The application belongs to the technical field of electro-catalytic material and functional film preparation, and particularly relates to a method for in-situ construction of Ni-LDH film
electrode by
oxygen non-thermal
plasma induction and application of the method in alkaline
oxygen evolution reaction. The method comprises the following steps: adding
ethanolamine into propionic acid, adding a
nickel source, and preparing a
nickel-containing precursor solution under the condition of heating and stirring; aging and centrifuging the precursor solution, and taking supernatant as a film-forming
sol; spin-
coating the film-forming
sol on a
substrate surface and
drying to obtain a precursor film; and placing the precursor film in a
microwave non-thermal
plasma under an
oxygen atmosphere, and in-situ converting the precursor film into a Ni-LDH film
electrode containing interlayer anions. The method does not need high-temperature annealing and subsequent hydrothermal activation, and can directly obtain a Ni-LDH film with characteristics of layered double
hydroxide. The obtained film shows good
oxygen evolution catalytic activity and stability in an alkaline
electrolyte, and has an
overpotential less than 350 mV and a Tafel slope less than 80 mV / dec under a
current density of 10 mA / cm2.