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33results about How to "Control slump loss" patented technology

Early-strength polycarboxylate water reducing agent for component and preparation method for early-strength polycarboxylate water reducing agent

The invention discloses an early-strength polycarboxylate water reducing agent for a component and a preparation method for the early-strength polycarboxylate water reducing agent, and belongs to the field of water reducing agent preparation. The water reducing agent is formed by polymerization of the following ingredients in percentage by weight: 80-85% of methyl alkene butyl polyoxyethylene polypropylene oxide monomer with the molecular weight more than 2400, 10-15% of unsaturated monocarboxylic acid and derivative monomer thereof and 0.5-5% of unsaturated alkenyl sulfoacid and sodium salt thereof; the preparation method comprises the following steps: under the temperature condition of 20-40 DEG C, all ingredients are enabled to be subjected to polymerization reaction in an aqueous solution by adopting a redox initiation system, after polymerization reaction is performed, neutralization is performed through a neutralizing agent, so that the polymer with low air entraining amount and good dispersibility is obtained; the early-strength performance of the polycarboxylate water reducing agent is reinforced with the increasing of the macromonomer molecular weight; the using requirements of early strength or super early strength of the component are met.
Owner:广西宝添环保材料有限公司

Polycarboxylic acid high-performance pumping agent as well as production process and preparation device thereof

The invention relates to the technical field of concrete admixtures, in particular to a polycarboxylic acid high-performance pumping agent as well as a production process and a preparation device thereof. The polycarboxylic acid high-performance pumping agent comprises the following raw materials in parts by mass: 30-35 parts of polycarboxylic acid mother liquor, 3-5 parts of a slow release agent, 0.6-0.8 part of a high-performance viscosity modifier, 0.6-0.8 part of an anti-mud agent, 0.1-0.3 part of an air entraining agent, 0.1-0.3 part of an anti-freezing agent, 0.3-0.5 part of a water-retaining agent, 0.1-0.3 part of a defoaming agent and 20-40 parts of water. According to the polycarboxylic acid high-performance pumping agent provided by the invention, all the components have a synergistic effect, so that the prepared polycarboxylic acid high-performance pumping agent is good in flowing property, good in pumping effect and good in water reducing and retarding performance, and the slump loss of concrete can be effectively controlled; and the production process of the polycarboxylic acid high-performance pumping agent provided by the invention has the advantages of simple production process, convenience in construction, no need of special equipment, low preparation cost, high production efficiency and higher popularization and application values.
Owner:南京福盛新材料有限公司

Environment-friendly non-autoclaved tubular pile water reducing agent and preparation method thereof

The invention discloses an environment-friendly non-autoclaved tubular pile water reducing agent characterized by comprising the following components in parts by weight: 10 to 20 parts of 1,3-bis(oxiranylmethyl)-5-(2-propenyl)-1,3,5-triazine-2,4,6(1H,3H,5H)-trione / 4,6-diamino-1,3,5-triazine-2-acetic acid polycondensate, 5 to 10 parts of 7-amino-3-vinyl-3-cephem-4-carboxylic acid / 4,4'-diaminostilbene-2,2'-disulfonic acid / polyethylene glycol monoallyl ether / 4-vinylphenylboronic acid copolymer, 1 to 3 parts of 9-fluorenecarboxylic acid, 0.3 to 0.6 part of an initiator, 2 to 5 parts of plant polysaccharide and 35 to 45 parts of water. The invention further discloses a preparation method of the environment-friendly non-autoclaved tubular pile water reducing agent. The environment-friendly non-autoclaved tubular pile water reducing agent disclosed by the invention is remarkable in water reducing effect, has the advantages of low dosage, excellent plasticizing performance, no obvious negative influence on the comprehensive performance of concrete, good energy-saving and environment-friendly performance in the preparation and use processes, high reaction activity, low reaction temperatureand capabilities of effectively enhancing the compressive strength, remarkable reduction of the hardening and viscosity of the concrete and improvement of the construction performance of the concrete.
Owner:赵良文

Method for preparing polycarboxylic concrete water reducer with high slump retention capacity, and construction method of polycarboxylic concrete water reducer

The invention provides a method for preparing a polycarboxylic concrete water reducer with high slump retention capacity. The method comprises the following steps: heating and melting a first monomer, adding a catalyst in the molten first monomer for stirring, then adding a polymerization inhibitor for continuous stirring, and then adding a second monomer; after performing thermostatic reaction on the mixture for a certain period of time, adding the second monomer, and then adding a chain transfer agent in the mixture to be evenly stirred to obtain a component 1; diluting an initiator with water to obtain a component 2; and simultaneously dripping the component 1 and the component 2 in a reaction vessel for reaction, and then adjusting the pH value of a reaction solution to be 6-8, so as to prepare the polycarboxylic concrete water reducer with high slump retention capacity. The prepared polycarboxylic concrete water reducer with high slump retention capacity has low dosage, can obviously control the slump loss, and enhance the adaptability to the cement variety, gypsum form, mixing proportion, water consumption and concrete mixing process; and the prepared polycarboxylic concrete water reducer with high slump retention capacity has good adaptability to the ambient temperature, and particularly has good slump retention capacity in high temperature.
Owner:江西迪特科技有限公司

Method for synthesizing slump-resistant naphthalene-based efficient water reducing agent

ActiveCN103387349BRestoring water-reducing plasticizing functionControl slump lossLiquid productSuperplasticizer
The invention belongs to the technical field of building materials and particularly discloses a method for synthesizing a slump-resistant naphthalene-based efficient water reducing agent. The method comprises the steps of adding industrial naphthalene or refined naphthalene into a glass-lined reactor, heating to melt, adding 98% industrial concentrated sulfuric acid, carrying out sulfonation reaction for 2-3 hours at the temperature of 135-175 DEG C, cooling to the temperature of 116-138 DEG C, adding water, carrying out hydrolysis reaction for 0.5-2.5 hours, cooling to the temperature of 90-110 DEG C, adding an industrial formaldehyde solution, carrying out condensation reaction for 3-8 hours, cooling to the temperature of 68-95 DEG C, adding alkylamine or alkyloamide, reacting with a naphthalene sulfonic formaldehyde condensate for 0.5-2.5 hours at the reaction temperature of 55-90 DEG C, adding sodium hydroxide, neutralizing until the pH value is 6-7, filtering a liquid product so as to remove impurities, concentrating the liquid product and carrying out spray drying, thereby obtaining a powdered product. The product prepared by the method disclosed by the invention is applicable to the preparation of concrete admixtures and is also applicable to the preparation of dispersants and oilfield chemicals.
Owner:WUHAN DONGPENG SCI & TECH DEV CO LTD

Slump-retaining concrete water reducing agent and preparation method thereof

ActiveCN114873947AInhibition of early calcium hydroxide formationImprove mechanical strengthSolid waste managementChemistryCalcium hydroxide
The invention relates to a slump-retaining concrete water reducing agent and a preparation method thereof. The water reducing agent comprises the following raw materials in parts by weight: 80-90 parts of a branched modified water reducing agent, 2-3 parts of a small molecular polymer, 8-9 parts of a slump-retaining auxiliary agent and 60-80 parts of water, in the preparation process of the water reducer, a branched monomer is introduced for branched modification, so that the generation of early calcium hydroxide can be inhibited, gaps are filled, and the mechanical strength is enhanced. Meanwhile, the strong adsorption capacity of phosphonic acid groups is utilized, the plastic viscosity of a system is effectively reduced, adsorption to a water reducing agent and mixing water is reduced, the dispersing performance is improved, the viscosity of concrete is reduced, the cement hydration process is delayed through the retarding effect of the phosphonic acid groups, and the long-time flow retention capacity is shown. According to the invention, a plurality of branched chains are grafted on cement, and the branched chains not only can provide a steric hindrance effect, but also can release polycarboxylic acid with a dispersion effect in a high-alkalinity environment of cement hydration to control slump loss.
Owner:四川金江建材科技有限公司

Early-strength polycarboxylate water-reducing agent with slump-preserving function and preparation method thereof

The invention discloses an early-strength polycarboxylate superplasticizer having a slump-loss prevention function and a preparation method of the polycarboxylate superplasticizer. The polycarboxylate superplasticizer is prepared through the following steps: (I) copolymerizing 5-12% of a monomer a, 73-89% of a modified low-foam early-strength polyether monomer b with the molecular weight (M) in a range of 2000-5000, and 6-15% of a monomer c in an aqueous solution at 50-70 DEG C to obtain a copolymerization reactant, wherein the total amount of the monomer a, the monomer b, and the monomer c is 100% by weight; and (II) adding a pH value conditioning agent into the copolymer for a neutralization reaction, wherein the pH value of the copolymer is adjusted to 6.8-7.2. According to the invention, the early-strength polycarboxylate superplasticizer having a slump-loss prevention function enables the fluidity of cement paste of concrete to be well kept. The concrete is low in air content and short in setting time, and the early-strength of the concrete is significantly enhanced. The polycarboxylate superplasticizer enables the concrete to have certain slump maintenance, and is particularly suitable for production of a prefabricated component of a pile tube or duct piece.
Owner:SHENZHEN MAIDI CONCRETE ADDITIVES
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