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31results about How to "Raise the initial melting temperature" patented technology

Nickel-base high-temperature alloy with low density and high melting point and preparation process thereof

The invention relates to high-temperature alloy technology, and in particular provides an isometrical cast nickel-base high-temperature alloy with low density, high incipient melting temperature and good casting property and a preparation process thereof, which can be used for floating tile materials of a combustion chamber. The alloy comprises the following compositions by mass percentage: 0.03 to 0.06 percent of C, 5 to 12 percent of Cr, 5.5 to 6.5 percent of Al, 3 to 8 percent of Co, 3 to 7 percent of W, 2 to 4 percent of Mo, 1.6 to 3.2 percent of Nb, 0.01 to 0.03 percent of B, 0.008 to 0.025 percent of Y and the balance of Ni. A vacuum induction furnace is adopted to smelt a master alloy, and a smelting crucible is a CaO crucible or a MgO crucible; and the operation process comprises the following steps: putting alloying elements such as carbon, chromium, cobalt, tungsten, molybdenum and niobium in proportion and a nickel plate into the crucible; melting the alloy when the vacuum degree reaches between 50 and 0.1 Pa; and after completion of the melting, refining for 30 to 300 seconds at a temperature of between 1,550 and 1,600 DEG C, cutting off electricity, forming a film, breaking the film to add Al and Al-Y and Ni-B interalloy for uniform stirring, and casting a master alloy pig at a temperature of between 1,450 and 1,500 DEG C. The invention solves the problems of low incipient melting temperature, poor plasticity and inoxidability and the like of the nickel-base high-temperature alloy.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Method for melting nickel-base high-temperature return material K441alloy

The invention relates to a method for melting nickel-base high-temperature return material K441 alloy, comprising the following steps: refining the return material and/or waste cast pieces in a vacuum induction furnace, decreasing the temperature of molten alloy and casting the molten alloy into a primary material ingot, analyzing the chemical components of the primary material ingot and adjusting the components of the molten alloy by adopting the nickel, aluminum, tungsten, chromium, molybdenum, zirconium, chromium boron master alloy and/or the carbon as the adjusting element component material; refining the primary material ingot and the nickel, the tungsten, the chromium and/or the molybdenum in the adjusting element component material for the second time and heating to cast the molten alloy after a film forming on the molten alloy or adding the carbon, aluminum, chromium boron master alloy and/or the zirconium to the molten alloy to alloy and heating to cast the molten alloy into an alloy ingot after a film forming on the molten alloy. The qualification rate of the return material K441 alloy produced with the method is equal to the qualification rate of the cast piece produced from the new material, and the initial melting temperature of the return material K441 alloy is higher than the initial melting temperature of the alloy produced from the new material with the original production technology.
Owner:SHENYANG LIMING AERO-ENGINE GROUP CORPORATION

High-temperature oxidation resistant wearproof Co-based alloy wire and preparation method thereof

ActiveCN106756257AGood high temperature and wear resistanceHigh temperature and wear resistanceWire rodOxidation resistant
The invention discloses a high-temperature oxidation resistant wearproof Co-based alloy wire and a preparation method thereof. The high-temperature oxidation resistant wearproof Co-based alloy wire comprises the following ingredients: 13-17% of Cr, 11-15% of Ni, 10-14% of W, 2.4-4.3% of Mo, 1.2-1.6% of Al, 2.8-3.6% of Ti, 0.1-0.5% of Nb, 1.2-1.8% of Ta, 0.03-0.06% of Re, 0.01-0.05% of Ce, 0.02-0.1% of C, 0.005-0.015% of B, 0.02-0.07% of Zr and the balance of Co. The alloy preparation process route is vacuum melting-remelting-forging-hot rolling-drawing-solid solution treatment-aging treatment. Raw materials are compounded according to percentage by mass and then melted and re-melted; after that, forging and rolling are performed to obtain an alloy wire rod; multi-drawing is conducted to prepare an alloy wire of phi 0.06-0.4 mm; and finally, solid solution treatment and aging treatment are performed. Through reasonable ingredient control and adding of alloy elements, the alloy wire has high yield and excellent high-temperature wear resistance, high-temperature corrosion resistance, oxidation resistance and high strength. As a sealing brush wire material, the high-temperature oxidation resistant wearproof Co-based alloy wire has the advantages that the sealing effect can be effectively improved, and the service life is prolonged.
Owner:SOUTHEAST UNIV

Solid solution heat treatment method for reducing solid solution hole content of high-rhenium nickel-based single crystal superalloy

The invention provides a solid solution heat treatment method for reducing the content of solid solution holes in a high-rhenium nickel-based single crystal superalloy, and belongs to the field of heat treatment technology.The method comprises the steps that alloy raw materials are subjected to vacuum melting, a master alloy ingot is obtained and put into a vacuum induction melting furnace to be remelted; casting by adopting a rapid cooling method and a spiral crystal selection method to prepare a single crystal alloy test bar; cutting the cast high-rhenium nickel-based single-crystal high-temperature alloy test bar casting to obtain a high-rhenium nickel-based single-crystal high-temperature alloy test bar; cutting a small test block from the middle section of the high-rhenium nickel-based single-crystal high-temperature alloy test bar, and carrying out a differential thermal analysis experiment; carrying out homogenization treatment on the high-rhenium nickel-based single-crystal high-temperature alloy test bar; and carrying out high-temperature solution treatment on the homogenized high-rhenium nickel-based single-crystal high-temperature alloy test bar. The heat treatment process is easy to operate and high in feasibility, the content of solid solution holes in the high-rhenium nickel-based single-crystal high-temperature alloy can be greatly reduced, and the structure compactness of the alloy is improved.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Directional solidification nickel-base high-temperature alloy and heat treatment process thereof

The invention relates to a directionally solidified Ni-based high temperature alloy and a heat treatment technology of the alloy, in particular to a guide wheel blade material with low density, low cost, high incipient melting temperature, oxidation and corrosion resistance and good heat fatigue performance, and a heat treatment technology of enhancing the tensile performance, duration, heat and cold fatigue of the alloy. The alloy components (in weight percent) are as follows: B 0.003 to 0.03, C 0.02 to 0.2. Cr8.0to 10.0, A 14.5 to 6.5, Co 4.0 to 12.0, Nb 1.8 to 2.5, W2.5 to 4.5, Mo 2.5 to 4.5, Y 0.005 to 0.05, and the rest is Ni. The heat treatment technology of the invention is as follows :(1) the temperature of the material is preserved for 3 to 5 hours at the temperature of 1210 to 1240DEG C, and the material is air cooled to room temperature; (2) the temperature of the material is preserved for 3 to 5 hours at the temperature of 1040 to 1080DEG C, and the material is air cooled to room temperature; and (3) the temperature of the material is preserved for 16 to 32 hours at the temperature of 850 to 900DEG C, and the material is air cooled to room temperature. The alloy of theinvention is characterized by low density, low cost, high incipient melting temperature, oxidation and corrosion resistance, good heat fatigue performance, etc., and is applicable to the directional nickel-based guide wheel blade material.
Owner:辽宁红银金属有限公司

A kind of rhenium-free nickel-based single crystal superalloy and preparation method thereof

The invention discloses a rhenium-free nickel-based single crystal superalloy and a preparation method thereof. The composition of the rhenium-free nickel-based single crystal superalloy of the present invention is represented by mass percentage as 7.25-7.75% of Cr, 4.8-5.2% of Co, 1.8-2.2% of Mo, 7.8-8.2% of W, and 6.3-6.7% of Ta , 6.0-6.2% Al, 0.12-0.18% Hf, 0.04-0.06% C, 0.003-0.005% B, 0.010-0.030% Y, and the rest is Ni. The preparation of the above-mentioned rhenium-free nickel-based single crystal superalloy comprises the following steps: using a vacuum induction furnace to melt the master alloy, and preparing a cast rod of the master alloy by gravity casting; using the seed crystal method to pass the Bridgeman directional solidification technology at a temperature gradient of 150-250K / cm , the single crystal test bar was prepared at a pulling rate of 5-100 μm / s; the single crystal superalloy was solid solution treated in the range of 1295-1305 °C for 2-4 hours, followed by air cooling, and then in the range of 1090-1310 °C 2-4 hours of high-temperature aging treatment within 2-4 hours, followed by air cooling; then 16-24 hours of low-temperature aging treatment in the range of 850-890 ° C, followed by air cooling.
Owner:NANJING UNIV OF SCI & TECH

Homogenizing heat treatment method for 7xxx series aluminum alloy with low Cu content

The invention relates to a homogenization heat treatment method for a low-Cu-content 7xxx series aluminum alloy, and belongs to the technical field of metal heat treatment. The method comprises the following steps: (1) a temperature rising stage: the alloy is subjected to a temperature rising process with a gradually reduced temperature rising rate, so that a dispersed phase is uniformly separated out, and the initial melting temperature of an AlZnMgCu phase is increased; and (2) a heat preservation stage: the alloy is subjected to a homogenization heat preservation process, so that the AlZnMgCu phase is redissolved. According to the homogenizing heat treatment method, the initial melting temperature of the quaternary phase can be effectively increased, rapid redissolution of the quaternary phase is achieved, the heat treatment time is saved, and meanwhile it can be ensured that the size and number density of the precipitated dispersed phase meet the requirements. More importantly, the method is simple in process control, strong in operability and high in heat treatment efficiency, can achieve the effect of conventional two-stage homogenization treatment, and is particularly suitable for homogenization treatment of industrial large-specification cast ingots.
Owner:GRIMAT ENG INST CO LTD

A kind of anti-high temperature oxidation and wear-resistant cobalt-based alloy wire and its preparation method

ActiveCN106756257BGood high temperature and wear resistanceHigh temperature and wear resistanceWire rodWear resistant
The invention discloses a high-temperature oxidation resistant wearproof Co-based alloy wire and a preparation method thereof. The high-temperature oxidation resistant wearproof Co-based alloy wire comprises the following ingredients: 13-17% of Cr, 11-15% of Ni, 10-14% of W, 2.4-4.3% of Mo, 1.2-1.6% of Al, 2.8-3.6% of Ti, 0.1-0.5% of Nb, 1.2-1.8% of Ta, 0.03-0.06% of Re, 0.01-0.05% of Ce, 0.02-0.1% of C, 0.005-0.015% of B, 0.02-0.07% of Zr and the balance of Co. The alloy preparation process route is vacuum melting-remelting-forging-hot rolling-drawing-solid solution treatment-aging treatment. Raw materials are compounded according to percentage by mass and then melted and re-melted; after that, forging and rolling are performed to obtain an alloy wire rod; multi-drawing is conducted to prepare an alloy wire of phi 0.06-0.4 mm; and finally, solid solution treatment and aging treatment are performed. Through reasonable ingredient control and adding of alloy elements, the alloy wire has high yield and excellent high-temperature wear resistance, high-temperature corrosion resistance, oxidation resistance and high strength. As a sealing brush wire material, the high-temperature oxidation resistant wearproof Co-based alloy wire has the advantages that the sealing effect can be effectively improved, and the service life is prolonged.
Owner:SOUTHEAST UNIV

A low-rhenium third-generation nickel-based single crystal alloy and its preparation method

The invention belongs to the field of nickel-based high-temperature alloy, and particularly relates to low-rhenium third-generation nickel-based single crystal alloy and a preparation method thereof. The alloy is composed of Cr, Co, W, Mo, Re, Ta, Al, Hf and Ni, wherein the content of Re is 3.0%-4.5%, and the alloy is characterized in that the value of Ta / (W+Mo) is controlled to be between 1 to (1-2). The main steps are that a vacuum self-consuming furnace is adopted, and raw materials are prepared into consumable electrodes which are prepared into mother alloy through multiple tests; and then a directional solidification furnace is adopted for preparing single crystal testing bars through a spiral crystal selection method, and finally the single crystal high-temperature alloy testing bars are subjected to heat treatment. The way of adjusting the value of Ta / (W+Mo) is mainly adopted for improving the persistent strength and hot corrosion resistance of the alloy, the alloy is made to meet the requirement for the third-generation nickel-based single crystal high-temperature alloy, the Re content is low, and no TCP phases are precipitated during long-term ageing at 900 DEG C, so that the stability is good.
Owner:JIANGSU UNIV

A service damage recovery method for precipitation-strengthened polycrystalline cast nickel-based alloys

The invention belongs to the technical field of metallurgy, and provides a service damage recovery method of a precipitation strengthening type polycrystal cast nickel-based alloy. The method mainly comprises the processes of hot isostatic pressing, solid solution and aging. Hot isostatic pressing is used for overcoming hole and loose defects in an alloy material, meanwhile dissolving part of coarsened or nodulized gamma' and ensuring that incipient melting does not happen to the alloy material. Solid solution testament is used for dissolving residual coarsened or nodulized gamma' phases formed in the service process of the alloy material. Aging treatment is used for adjusting the form and size of gamma' so as to obtain optimal matching of strength and plasticity, and finally the nickel-based alloy material without hole defects and with large-size square gamma' and small-size point-like gamma' coexisting is obtained. After recovery treatment, the high-temperature endurance performance of the alloy material can be close to the level before service. According to the service damage recovery method, operation is simple, the production efficiency is high, the economic benefits are high, and universality, generality and adaptability are high; and the requirements for repair and life prolonging of gas turbine high-temperature components can be met.
Owner:XIAN THERMAL POWER RES INST CO LTD
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