The invention provides a 1, 2-butadiene rectification preparation device and process, and relates to the field of
petrochemical industry. The device comprises a 1, 3-butadiene
concentration unit and a 1, 2-butadiene product unit, the 1, 3-butadiene
concentration unit comprises a 1, 3-butadiene concentration
tower, a first
tower kettle
reboiler, a first
tower top condenser and a first
reflux tank; and the 1, 2-butadiene product unit comprises a 1, 2-butadiene product tower, a second tower kettle
reboiler, a second tower top condenser and a second
reflux tank. The process comprises the steps of light component removal rectification and heavy component removal rectification. According to the method, heavy components of a butadiene extraction unit of an
ethylene device are used as raw materials, a continuous rectification mode of removing light components first and then removing heavy components is combined with a
pasteurization treatment technology, a 1, 2-butadiene product with the purity being larger than or equal to 97.5 wt% can be obtained, 1, 3-butadiene is recycled, the overall
utilization rate of resources is increased, and meanwhile
energy conservation and emission reduction of enterprises are facilitated.