The application discloses a method for preparing high-purity
vanadium pentoxide in a short process, and belongs to the technical field of non-
ferrous hydrometallurgy. The method comprises the following steps: firstly, after pretreatment of
vanadium-containing leaching solution,
sodium sulfide and na-
methylmercury sulfonate are added, aging is carried out, impurities are removed,
hydrogen peroxide is added and heated, pH is adjusted, attapulgite is added, aluminum
sulfate is added, aging and
impurity removal are carried out; secondly,
vanadium precipitation treatment is carried out,
ammonium polyvanadate is washed, dried and calcined, and high-purity vanadium
pentoxide with a grade of greater than or equal to 99.5% is obtained. In the application, the vanadium-containing leaching solution is used to produce high-purity vanadium
pentoxide, the
impurity removal process is advanced, high-purity vanadium pentoxide with a grade of greater than or equal to 99.5% can be prepared, and the vanadium
recovery rate can reach 98%. The preparation process is greatly simplified, the production efficiency is high, the cost is reduced, the
treatment time is short, energy saving and emission reduction and
green production are beneficial, the production cost is reduced by 3000-5000 yuan /
ton, the vanadium
recovery rate can be increased by about 3%, the process is more
environmentally friendly, the vanadium
recovery rate is higher, and the production efficiency is also higher. The application is suitable for preparing high-purity vanadium pentoxide in a short process.