The invention provides a steel and iron material scale EBSD
sample preparation method which comprises the following steps:
cutting out a piece of steel to be analyzed, and roughly
grinding an observation surface of the steel to be analyzed; after rough
grinding, sequentially carrying out inlaying, mechanical
grinding and
polishing,
oxide polishing, vibration
polishing and
cutting on the observation surface, wherein the mechanical grinding and polishing comprises mechanical grinding and mechanical polishing, during mechanical polishing, suspension liquid of 9 microns, suspension liquid of 3 microns and suspension liquid of 1 micron are used respectively, and the polishing time is 9 min, 7 min and 7 min respectively; a suspension liquid used for
oxide polishing is an aluminum
oxide suspension grinding polishing solution, and the polishing time is 45 min. According to the prepared oxide scale EBSD sample, an oxide layer on the surface of steel is completely preserved, the surface protection effect is good, meanwhile, a steel base body of the sample makes direct contact with an EBSD sample table, good
conductivity is guaranteed, and obvious image drifting in the detection process is avoided.