The invention belongs to an alkali treatment
surface modification MXene material preparation method and an
electrolyte, Ti3AlC2
powder is slowly added into
polytetrafluoroethylene containing concentrated HCl and LiF, aluminum layer
etching is carried out, and after
etching is completed, washing is carried out until the solution is neutral; dispersing the obtained product in water, continuously introducing
inert gas for degassing treatment, sealing at
room temperature for ultrasonic stripping, centrifuging the obtained dispersion liquid, and freeze-
drying the supernate to obtain the few-layer Ti3C2Tx
nanosheet; the method comprises the following steps: weighing a few
layers of Ti3C2Tx nanosheets, slowly adding an alkali solution under stirring, carrying out a stirring reaction under
inert gas, carrying out vacuum
filtration on a reacted sample, washing a
filter cake with water until a filtrate is neutral, and carrying out
freeze drying to obtain surface functionalization modified MXene. The electrochemical performance research of the material finds that the alkali intercalation modified MXene has excellent
ion capture performance and good stability on various ions (Na < + >, Pb < 2 + >, Al < 3 + > and the like).