A
system for ultra-high-pressure
spark plasma sintering, characterized in that it comprises a six-sided press body, a high-power DC
pulse power supply (1), and a high-pressure synthesis
assembly block; wherein the six-sided press body has a frame and a
hydraulic drive system for generating ultra-
high pressure, wherein six
carbide press hammers (6) collectively enclose a cubic space used to hold the high-pressure synthesis
assembly block in which a sample is enclosed; wherein two poles of the high-power DC
pulse power supply (1) are each connected via two conductive
copper strips (2) to an upper and a lower large support block (3), wherein a steel ring (4) is mounted on each end section of the two large support blocks (3), and wherein the
carbide press hammers (6) are embedded in the end sections of the steel rings (4).wherein small support blocks (5) are arranged between the
hard metal press hammers (6) and the large support blocks (3), the small support blocks (5) each being in contact with the large support blocks (3) and the
hard metal press hammers (6), wherein a high-frequency
pulse current from the high-power DC
pulse current supply (1) is transmitted to the
hard metal press hammers (6) via the conductive
copper strips (2), the large support blocks (3) and the small support blocks (5); wherein the high-pressure synthesis
assembly block comprises a
pressure transmission medium (13), wherein an insulating tube (14) is embedded in an inner wall of a cavity of the
pressure transmission medium (13), wherein a
graphite tube (11) is mounted on the insulating tube (14), the
graphite tube (11) being connected at a top and a bottom to a
hexagonal boron nitride tube (15),wherein an inner
diameter and an outer
diameter of the
hexagonal boron nitride tube (15) are equal to those of the
graphite tube (11), wherein a powdered sample (12) is arranged in the middle of the graphite tube (11), wherein the powdered sample (12) is in contact with an inner wall of the graphite tube (11), wherein conductive graphite plugs (10) are provided at both ends of the graphite tube (11), wherein a total length of the sample (12) and the conductive graphite plugs (10) is equal to the total length of the graphite tube (11) and the two upper and lower
hexagonal boron nitride tubes (15), wherein above the conductive graphite plugs (10) in a direction away from the sample (12) a conductive graphite plate (9), a conductive
molybdenum plate (8) and a conductive steel cap (7) are successively arranged, wherein the high-frequency pulsed
direct current is successively passed through the hard
metal press hammers (6), the conductive steel cap (7), the conductive
molybdenum plate (8),The conductive graphite plate (9) and the conductive graphite plugs (10) are transferred to the sample (12) to form a
closed circuit.