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33results about How to "Shorten saponification time" patented technology

Collecting agent for sorting monazite and ilmenite and using method of collecting agent

The invention provides a collecting agent for sorting monazite and ilmenite and a using method of the collecting agent. The collecting agent comprises 10-15 parts of tall oil, 25-35 parts of oxidizedparaffin soap, 40-50 parts of palm oil, 10-15 parts of fatty acid methyl ester sodium sulfonate and 10-15 parts of sodium hydroxide. The preparation method comprises the following steps: carrying outmicrowave pretreatment on tall oil, oxidized paraffin soap, palm oil and sodium fatty acid methyl ester sulfonate, and then mixing and stirring at 70-85 DEG C; and adding sodium hydroxide, and mixingunder the condition of 85-100 DEG C to obtain the collecting agent. A novel microwave pre-activation pretreatment mode is adopted on equipment, a direct reaction kettle reaction is replaced, the saponification time is shortened, the production cost is reduced, and the collecting effect is better. The collecting agent is used; the comprehensive grade P of monazite concentrate can be increased to 10.29% or above, the operation recovery rate P is increased to 88.03% or above, the comprehensive grade TiO2 of ilmenite is increased to 50.00% or above, the operation recovery rate TiO2 is increased to96.22% or above, and good economic benefits are achieved.
Owner:盛和资源(连云港)新材料科技有限公司 +3

Method for preparing grafted modified starch

The invention relates to a method for preparing grafted modified starch. The method comprises the following steps of: (1) preparing starch milk from the common starch and then performing acidification for 1.5 to 2.5 hours; (2) introducing nitrogen into the acidified starch milk to remove oxygen from a system and then adding dihydrogen manganese pyrophosphate and grafted monomers of acrylic acid, methyl acrylate, ethyl acrylate and vinyl acetate sequentially to perform a graft copolymerization reaction; (3) adding sodium hydroxide and sodium hypochlorite into the starch copolymer to perform saponification aftertreatment; and (4) neutralizing by adding sulfuric acid until the pH value is 6 and 8, and then performing dehydration, drying, pulverization, sieving, packaging and metering to obtain the grafted modified starch finished product. The method has the advantages that: the properties of the grafted modified starch are stable; the process operation is simple; and chemicals used in the modifying process have low price and convenient and readily available source. The grafted modified starch product has the advantages of meeting a starching requirement, effectively reducing the costof sizing agents and reducing pollution of PVA to ecological environment, along with excellent properties, stable quality and lower price.
Owner:TIANJIN TIANFUTONG BIOTECH DEV
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