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276 results about "Nano sized particle" patented technology

Method for preparing natural material inorganic nanoparticle composite nano-fiber through electrostatic spinning

The invention relates to a method for preparing natural material inorganic nanoparticle composite nano-fiber through electrostatic spinning, which comprises steps that a template is added into diluted aqueous alkali, the mixture is heated to 80-90 DEG C through an oil bath, mixed for 1-10 hours, gradually added with tetraethyl orthosilicate, centrifugally washed by deionized water and absolute ethyl alcohol sequentially, and dried and reflowed in HCL-ethanol mixed liquor to remove the template, so freeze dried mesoporous silicon is obtained; and natural materials are dissolved in the solvent to prepare the natural material solution, the mesoporous silicon is added into the natural material solution for electrostatic spinning, fumigating and crosslinking are carried out for 0-48 hours, so the natural material mesoporous silicon composite nano-fiber is obtained. The natural material inorganic nanoparticle composite nano-fiber which is prepared by the method has good biocompatibility, a simple preparation method and moderate reaction conditions, is low in experimental raw material price, has high drug-loading rate, can be controlled to be released for a long term, and can be applied in the biomedicine and tissue regeneration fields of growth factor and gene release of tissue engineering, cancer treatment and the like.
Owner:DONGHUA UNIV

Method for preparing gold nano particle and graphene composite material through fast reduction

The invention discloses a method for preparing a gold nano particle and grapheme composite material through fast reduction. The method specifically comprises the steps of 1, preparing reduced grapheme oxide water solution by taking sodium borohydride as a reducer; 2, adding gold chloride acid in the reduced grapheme oxide water solution, and obtaining the gold nano particle and grapheme composite material in an in-situ reduction way by utilizing the reducibility of the grapheme through ultrasonic action under normal temperature; 3, centrifugally washing the obtained solution by using de-ionized water for multiple times so as to obtain the gold nano particle and grapheme composite material of which the dimension is uniform and the distribution is uniform. The method disclosed by the invention has the advantages that the technology is simple, the preparation period is short, the repeatability is strong, environment protection is realized, and a composite product is uniform and stable; the prepared gold nano particle and grapheme composite material has good stability in water solution and is not easy to reunite, and meanwhile, the method has the characteristics of multiple reaction active sites, large specific surface area, good biocompatibility, electric conduction and the like; the method has a wide application prospect in aspects of catalyzing, sensing, environment protection, SERS (Surface Enhanced Raman Scattering) and the like.
Owner:SOUTHEAST UNIV

Cu2O ultra-fine nano-particles and self-assembly nanospheres as well as preparation method thereof

InactiveCN101805011AGood sustained releaseSlow release method, convenient to control the whole reaction processNanostructure manufactureCopper oxides/halidesMicrosphereUltra fine
The invention discloses Cu2O ultra-fine nano-particles and self-assembly nanospheres as well as a preparation method thereof, relating to the preparation method of the nano-particles. A whole reaction mixed liquid is divided into two phases through regulating the proportion of each substance in a reaction system, wherein one phase contains metal salt while the other phase contains a reducing agent. The metal salt is released to the phase containing the reducing agent, and contacted with the reducing agent at a part close to the interface of two phases to carry out reduction reaction, and the release action and a protecting agent in the reaction system commonly act in the whole reaction system so as to achieve the aim of controlling the appearances and the sizes of the product Cu2O ultra-fine nano-particles. The Cu2O ultra-fine nano-particles can be prepared by using the release method; if the reaction mixed liquid containing the Cu2O ultra-fine nano-particles continuously keeps the temperature for certain time at certain temperature, Cu2O self-assembly nanospheres with larger particle sizes formed by self-assembling the Cu2O ultra-fine nano-particles are prepared due to the Ostwald maturating action.
Owner:XIAMEN UNIV
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