The invention discloses an electrochemical high-flux testing method based on a photolithographic
mask and a micro
liquid tank and a device and relates to the technical field of
metal corrosion,
microcell electrochemistry and systematic data accumulation application. The device comprises a micro
liquid tank testing
system, a testing liquid updating
system, a high-precision XYZ three-dimensional moving platform, a microscopic
monitoring system, an electrochemical testing
system, a storage and
control system and a connection system, wherein the connection system is used for controlling instructions and testing data to be effectively transmitted among the systems. Due to
modular design, the device is high in expandability; with the combination of a photolithographic
mask technique and the micro
liquid tank testing system, and a high-flux idea, the reaction area of a
working electrode is precisely controlled, a high solution amount /
working electrode reaction
area ratio is achieved, influence of reaction products is reduced, seam
corrosion is eliminated, risks of liquid leakage, blocking and
oxygen diffusion are reduced, relatively low solution resistance is achieved,
mask graphs and micro-tube sizes can be selected according to demands, high-flux and automatic measurement on
microcell electrochemistry are achieved, and the measurement and analysis efficiency are improved.