The invention discloses a method of preparing transparent
pigment yellow 180. The method comprises the following steps: preparing a diazotization solution, preparing a
coupling solution, preparing a
buffer solution through
ammonium chloride and
ammonia water, controlling the pH to 7-7.5, adding bi-octadecyl-dimethyl
ammonium chloride, firstly, dripping 1 / 20-1 / 8 of the
coupling solution, simultaneously dripping the diazotization solution and the
coupling solution, controlling the dripping reaction time to 15 minutes to 8 hours, and controlling the
reaction temperature to 10-50 DEG C; continuing to stir after dripping the solutions to ensure a complete
coupling reaction, filtering and washing to remove the inorganic salt and a part of water-soluble impurities to obtain a crude product, adding an assistant and water, heating, and finally, filtering,
drying and crushing to obtain a finished product. The method generates little production in the production process, the cost is low, the produced
pigment is uniform in particle
diameter distribution, the particles are soft, the
crystal structure and
crystal size are uniform with the product treated by an
organic solvent, and the product is high in
color strength, bright in color and excellent in light resistance and
solvent resistance. The acylamino in the groups of the
pigment yellow 180 greatly improves the combination firmness of the molecules, thereby improving such properties as
solvent resistance,
heat resistance, and the like.