The invention relates to a super-hard wear-resistant transparent film layer material which is compounded on a nano scale and takes the
silicon-doped carbonized
polymer point as a construction element and a preparation method of the super-hard wear-resistant transparent film layer material, and belongs to the technical field of preparation of super-hard wear-resistant scratch-resistant transparent film materials. The preparation method comprises the following steps: weighing propylamino
silsesquioxane and
citric acid in a
molar ratio of 1: (0.1-4), dissolving the propylamino
silsesquioxane and the
citric acid in deionized water, and then carrying out
hydrothermal reaction at 160-200 DEG C for 3-8 hours; then naturally cooling to
room temperature to obtain a faint yellow transparent Si-CPDs
aqueous solution, and filtering by using a 0.22 mu m polyether
sulfone filter membrane to obtain Si-CPDs curing liquid with
silicon hydroxyl on the surface; and
spin coating,
dip coating or
spray coating the curing liquid onto the surface of a
glass slide subjected to
Plasma treatment for 3-5 minutes, and curing for 0.5-3 hours at the temperature of 60-200 DEG C to obtain the super-hard wear-resistant transparent film layer. The
film material can be used for preparing surface hard wear-resistant protective
layers of displays, transparent optical devices and solar cells.