The invention discloses a method for preparing
gadolinium oxysulfide
ceramic hollow microspheres, which comprises the following steps: adding additives into a water
solvent, uniformly mixing to prepare a premixed solution, and the additives comprise a dispersing agent, a
monomer, a cross-linking agent, a
green body reinforcing agent, a closed pore forming agent and a
sintering aid; carrying out ball milling on Gd2O2S
ceramic powder and the premixed liquid to prepare Gd2O2S
slurry with the
solid content of 75-85%, adding an initiator and a catalyst, and uniformly mixing for later use; a semi-arc-shaped super-hydrophobic track coated with a super-hydrophobic film is manufactured, the track is arranged on an inclined rack, and a heating belt is attached to the lower portion of the inclined plane of the track; a dispensing
machine needle head is selected to enable a
titration needle cylinder to be located at the position 18-15 cm above the track, Gd2O2S
ceramic slurry is injected into the
titration needle cylinder, the inclined plane is controlled to be heated to 150-210 DEG C, the size of liquid drops is controlled to be 0.18-1 mm through the air
inlet pressure of
compressed air and the size of a needle hole, the liquid drops drop on the
metal track coated with the super-hydrophobic film from the top end of the inclined plane, and the Gd2O2S ceramic
slurry is obtained. The Gd2O2S microspheres roll downwards and are heated and cured into Gd2O2S
microsphere blanks; and
drying and
degreasing the formed Gd2O2S ball blank, and
sintering to obtain the Gd2O2S ceramic hollow
microsphere.