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175results about How to "Realize green manufacturing" patented technology

Liquid die forging and rolling compound formation method for GH4033 high-temperature alloy irregular-section large ring piece

The invention relates to a liquid die forging and rolling compound formation method for a GH4033 high-temperature alloy irregular-section large ring piece. The method comprises the following steps of: 1) smelting; 2) performing liquid die forging, namely fixing a liquid die forging mold on an indirect extrusion casting machine, pouring a quantitative amount of alloy solution into the liquid die forging mold at the pouring temperature of between 1350 and 1450 DEG C, pressurizing at the speed of 40 to 50 mm/s, filling for 1 to 6 seconds at the specific pressure of 300 to 400 MPa, keeping the pressure for 50 to 90 seconds, and thus obtaining a similarly final section ring blank; 3) homogenizing; 4) performing afterheat isothermal rolling, namely cooling the homogenized similarly final section ring blank to the temperature of between 1100 and 1140 DEG C, and performing afterheat isothermal rolling on a radial shaft compound ring rolling machine; 5) performing thermal treatment, namely performing solid solution instant thermal treatment, keeping the ring blank at the temperature of between 900 and 1000 DEG C for 1 to 2 hours, performing air cooling, then heating to the temperature of 1080 DEG C, keeping the temperature for 8 hours, performing air cooling to the temperature of 750 DEG C, keeping the temperature for 16 hours, and performing air cooling; and 6) finishing.
Owner:SOUTHWEST UNIVERSITY

Method for preparing carbon microspheres through hydrothermal carbonization of biomass

The invention discloses a method for preparing carbon microspheres through hydrothermal carbonization of a biomass. The method comprises the following steps: stirring and mixing camellia seed husk powder which serves as a raw material and deionized water, treating the mixture ultrasonically, transferring the treated mixture into a stainless steel reactor, introducing an inert gas into the stainless steel reactor to remove oxygen, putting the stainless steel reactor into an air blowing drying box, carrying out reaction at a constant temperature, cooling the product of reaction to room temperature, pouring out the upper-layer liquid, tanking out the solid, clearing the solid ultrasonically with deionized water and ethanol in sequence until the washing liquid is colorless, extracting with ultrasonic waves and microwaves in the solution of ethanol in water, filtering the mixture in vacuum, and drying in a vacuum drying box to obtain the carbon microspheres. The method disclosed by the invention has the advantages that the raw material for preparing the carbon microspheres is a biomass waste which is wide in source and low in cost, the process of preparing the carbon microspheres is simple and is friendly to environment, no poisonous and harmful reagents are adopted in the whole preparation process, and the prepared poisonous carbon microspheres are uniform in size and can be used conveniently. In addition, the method is low in production cost and can realize large-scale production.
Owner:NANCHANG HANGKONG UNIVERSITY

Multi-pass metal drawing device based on water lubrication drawing

The invention discloses a multi-pass metal drawing device based on water lubrication drawing. The multi-pass metal drawing device comprises a support, a drawing cavity which is fixed in the support, a sealing ring, a mold group and a lubrication chamber group which are arranged in the drawing cavity, and a cover plate which is fixed on the support, wherein the mold group is an ultra-smooth nano diamond composite coating mold; a drawing cavity lubricant inlet is aligned with the center line of a support lubricant inlet; the sealing ring, the lubrication chamber group and the mold group are sequentially placed in the drawing cavity along the drawing direction of a pipeline material; and the opening direction of a lubrication chamber is aligned with the drawing cavity lubricant inlet and outlet. The multi-pass metal drawing device can ensure that the contact area between the pipeline material and the mold group is completely immersed in a lubricant during drawing, then the excellent water lubrication property of a diamond film is brought into play, and a drawing area is effectively lubricated and cooled, so that the service life of the mold is prolonged, and the processing surface quality and the surface smooth finish and cleanliness are improved; and meanwhile, the characteristics of safety and non-pollution of a water base lubricant also ensure that a processing environment is greatly improved.
Owner:SHANGHAI JIAO TONG UNIV +2

Low-conductivity super-long-acting organic base type anti-freezing cooling liquid

InactiveCN102174313APrevent corrosion of metal partsStorage stableHeat-exchange elementsCycloalkaneChemistry
The invention provides low-conductivity super-long-acting organic base type anti-freezing cooling liquid, which comprises the following components in percentage by weight: 15 to 96 percent of anti-freezing agent, 0.05 to 1.5 percent of natural alkaloid, 0.5 to 2.5 percent of hetero-cycloalkane, 0.01 to 0.3 percent of azole component, and the balance of deionized water. In invention, since the natural alkaloid is matched with nonionic organic compounds, the prepared anti-freezing cooling liquid has the characteristics of low freezing point, high boiling point, no scale formation, corrosion protection, high heat efficiency and the like; in addition, the prepared anti-freezing cooling liquid also has ultra-low conductivity which can reach 5 mus/cm and is a few hundredths of the conductivity of a common water cooling medium because the anti-freezing cooling liquid does not contain the components of inorganic salts, organic carboxylic acid and the like. The anti-freezing cooling liquid with ultra-low conductivity can effectively slow up the corrosion on metal parts of a cooling system, and meet the requirement of special conditions such as the cooling of a wind generator set and the like on the insulation safety of the anti-freezing cooling liquid. The anti-freezing cooling liquid realizes environmental protection and ultra-long-acting service, and is particularly suitable for special equipment such as a wind generator set, an imperial sedan engine and the like.
Owner:ADVANCED MFG TECH CENT CHINA ACAD OF MASCH SCI & TECH

Methods for preparing and using pre-reduced fluxed pellets by taking steel slag as part of raw materials

The invention relates to a method for preparing pre-reduced fluxed pellets by taking steel slag as part of raw materials. The method comprises the following steps of (1) screening the steel slag, screening out steel slag particles with the particle size of 2-4 mm, and grinding the rest steel slag into steel slag powder; (2) drying fly ash, and grinding the fly ash into fly ash powder; (3) mixing the steel slag powder, the fly ash powder, iron oxide red, iron ore concentrate powder and a composite binder in a mixer; (4) taking the steel slag particles with the particle size of 2-4mm as a pelletizing core, and continuously putting the steel slag particles into a pelletizer for pelletizing to obtain green pellets; and (5) carrying out drying, preheating and roasting to obtain finished pelletsof the pre-reduced fluxed pellets. After the technical scheme is adopted in blast furnace production, the cost of blast furnace production is reduced, so that the market competitiveness of an iron-making process is enhanced, meanwhile, cyclic utilization of secondary resources of an iron and steel plant can be realized, then application of high-added-value products is realized, and further, greenmanufacturing of blast furnace smelting is realized.
Owner:ANGANG STEEL CO LTD

GH4169 high-temperature alloy special-cross-section large annular piece liquid forging and rolling composite forming method

The invention discloses a GH4169 high-temperature alloy special-cross-section large annular piece liquid forging and rolling composite forming method which comprises the following steps: 1) smelting; 2) liquid forging: fixing a liquid forging mold on an indirect squeezing casting machine, pouring an alloy solution in constant volume into the liquid forging mold, wherein the pouring temperature is 1350-1400 DEG C, the pressurization speed is 35-40mm/s, the type filling time is 1-6 seconds, and the specific pressure is 350-400MPa; and keeping the pressure under the pressure for 35-90 seconds, thereby obtaining a near terminal cross section annular blank; 3) homogenizing: cooling the near terminal cross section annular blank to 1150-1160 DEG C, performing heat preservation for 20-30 hours, then rising the temperature to 1180-1190 DEG C, and performing heat preservation for 110-130 hours; 4) residue heat isothermal rolling: reducing the temperature of the near terminal cross section annular blank after homogenization to 1010-1120 DEG C, and carrying out residue heat constant temperature rolling on a radial and axial composite rolling annular machine; 5) heat treatment: performing heat preservation on the annular blank at a temperature of 715-725 DEG C for 8 hours, and then cooling to 615-625 DEG C in a furnace at a speed of 50 DEG C/h, performing heat preservation for 8 hours, and carrying out air cooling; and 6) finishing.
Owner:SOUTHWEST UNIVERSITY

Green preparation method for hydroxyl oxime acid rare-earth flotation agents

The invention provides a green preparation method for hydroxyl oxime acid rare-earth flotation agents. The green preparation method comprises the steps of fatty acid esterification, fatty acid ester oximation and acidification. After the fatty acid esterification and before the fatty acid ester oximation, waste liquid is not treated, and a fatty acid esterification mixed product is totally added into a reaction kettle for performing oximation directly. The invention also provides another green preparation method for the hydroxyl oxime acid rare-earth flotation agents. The green preparation method comprises the steps of fatty acid esterification, fatty acid ester separation and purification, fatty acid ester oximation and acidification; when the step of fatty acid ester acidification is performed, the waste liquid obtained by separating and purifying the fatty acid ester is added. A hydroxyl oxime acid rare-earth collecting agent is synthesized by adopting the process provided by the invention, the waste water discharge during a synthesizing process can be reduced; the green preparation of the hydroxyl oxime acid rare-earth flotation agents can be realized; the economic benefit of an enterprise can be greatly improved; meanwhile, the flotation agents obtained by the method provided by the invention have excellent flotation performance.
Owner:INST OF MULTIPURPOSE UTILIZATION OF MINERAL RESOURCES CHINESE ACAD OF GEOLOGICAL SCI

Preparation method of rare earth-doped gadolinium oxysulfide and oxygen-containing gadolinium sulphate up-conversion phosphor

The invention provides a preparation method of rare earth-doped gadolinium oxysulfide and oxygen-containing gadolinium sulphate up-conversion phosphor, and belongs to the field of material science. The method comprises the following steps that 1, Gd(NO3)3.6H2O, Yb(NO3)3.6H2O and Ln(NO3)3.6H2O are mixed, deionized water is added, and a RE(NO3)3 solution is obtained; 2, ammonium sulfate is dissolved into the RE(NO3)3 solution, stirring is conducted, stirring continues, ammonia water is added, the pH value is regulated, and suspension is obtained; 3, the suspension is subjected to a hydrothermal reaction for 1-72 h at the temperature of 100 DEG C to 150 DEG C and then naturally cooled to room temperature, and a reaction product is obtained; 4, the reaction product is centrifugally separated, washed and dried, and a white powder precursor is obtained; 5, the white powder precursor is calcined, and the rare earth ion-doped Gd2O2S or Gd2O2SO4 up-conversion phosphor is obtained. According to the method, the problems of usage of sulfur-containing raw materials and discharge of harmful by-products in a conventional method are effectively solved, and the method is a green and environment-friendly preparation technique.
Owner:NORTHEASTERN UNIV

Machining center lubricity test system and optimization method

The invention relates to a machining center lubricity test system and an optimization method and belongs to the field of testing of machining center lubrication systems. Thermosensitive parts of a spindle system and a feed system are identified by thermal imaging testing of the spindle system and the feed system, and temperature sensors are mounted at the thermosensitive parts. A test system of a machining center lubrication system is set up; the lubrication amount is adjusted by adjusting a lubrication time interval of a machining center; the spindle system and the feed system of the machining center move continuously in different lubrication amount states; and simultaneously, temperature data at the thermosensitive parts is acquired. The lubrication amount of the spindle system and the feed system of the machining center is optimized based on temperature rises of the thermosensitive parts. The invention provides the test system and the optimization method for optimizing the lubrication amount of the machining center lubrication system; the problem of unreasonable lubrication amount setting of the machining center lubrication system at present is solved; the movement performance of a machine tool can be improved; the use cost of the machine tool is lowered; and the pollution of lubricating oil is reduced.
Owner:通用技术集团沈阳机床有限责任公司

Liquid die forging/rolling composite forming method for magnesium alloy irregular-section large-size ring piece

The invention relates to a liquid die forging/rolling composite forming method for a magnesium alloy irregular-section large-size ring piece, which comprises the following steps: smelting, liquid die forging, homogenizing, excess heat isothermal rolling, heat treatment and finishing, wherein in the liquid die forging process, after a liquid die forging die is fixed onto an indirect extrusion casting machine, the smelted magnesium alloy solution is quantitatively cast into the liquid die forging die, and kept under the specific pressure of 140-200 MPa for 35-150 seconds to obtain the similar end-section ring blank, wherein the casting temperature is 680-740 DEG C, the pressurization speed is 50-100 mm/s, and the cavity filling time is 1-6 seconds; and in the excess heat isothermal rolling process, when the homogenized similar end-section ring blank is cooled to 300-400 DEG C, isothermal rolling is carried out on a radial/axial composite ring rolling machine. The method provided by the invention can simplify the blank making process of the alloy ring piece, lower the cost, enhance the production efficiency, effectively improve the microstructure state of the liquid die forging die magnesium alloy ring piece, and enhance the comprehensive mechanical properties.
Owner:SOUTHWEST UNIVERSITY

Injection molded steel-tube sea sand recycled concrete column with built-in stiffening member

The invention relates to an injection molded steel-tube sea sand recycled concrete column with a built-in stiffening member. The injection molded steel-tube sea sand recycled concrete column comprises an injection molded steel tube which is filled with sea sand recycled concrete. Two ends of the injection molded steel tube are respectively provided with an end cover. A FRP section steel stiffening member is also arranged inside the sea sand recycled concrete. The internal surface of the injection molded steel tube has good elastoplasticity and strength as well as corrosion resistance. According to the invention, sea sand is directly applied in the recycled concrete of the injection molded steel tube, and it is unnecessary to process sea sand. The sea sand recycled concrete is poured into the injection molded steel tube to form the injection molded steel-tube recycled concrete column, and then two ends of the injection molded steel tube are sealed by the use of seal covers with plastic washers. The injection molded steel tube provides tightening force for the recycled concrete such that sea sand and the recycled concrete are tightly combined. In addition, as a corrosion resistant layer inside the injection molded steel tube has good elastoplasticity and strength and has fracture resistance and compressive strength 3.5 times higher than a common steel tube, the corrosion resistant layer can play a role in corrosion prevention and isolation and can be used to make the injection molded steel tube and the recycled concrete to be more tightly combined. Thus, the injection molded steel-tube sea sand recycled concrete column has better functional effects.
Owner:GUANGDONG UNIV OF TECH

Knife handle suitable for low-temperature minimal quantity lubrication

ActiveCN110883591ASolve problems not suitable for low temperature MQL cuttingOvercome tightnessMilling cuttersAdverse effect compensationNumerical controlCooling effect
The invention provides a knife handle suitable for low-temperature minimal quantity lubrication, and belongs to the technical field of cooling and lubrication of numerical control machine tools. The knife handle comprises a knife handle body, a peripheral static structure, a multi-layer sealing structure, a heat insulation structure and a bearing supporting structure. The problems that in the minimal quantity lubrication technology, the cooling performance is insufficient, and lubrication is insufficient in the low-temperature cooling machining technology are solved, the oxygen isolation protection effect of an ultralow-temperature medium, the cooling effect of the ultralow-temperature medium and the anti-attrition lubrication effect of minimal quantity lubrication are integrated, and therefore a good machining effect is achieved on the aspect of materials difficult to machine. The knife handle can be used for machining the materials difficult to machine through a traditional numericalcontrol machine tool, the application range of an outer rotating inner knife handle is widened, the cutting heat of the materials difficult to machine in the cutting machining process is effectivelyreduced, the service life of a knife is prolonged, traditional cutting fluid is replaced, and green manufacturing is achieved.
Owner:DALIAN UNIV OF TECH

Green preparation method of polyimide gas separation membrane

The invention belongs to the technical field of membrane separation and in particular relates to a green preparation method of a polyimide gas separation membrane. The membrane preparation process comprises the following process steps: (1) synthesis of water-soluble polyimide: dissolving the prepared hydroxypolyimide in N,N-dimethylformamide, adding a sulfonation or carboxylation reagent and K2CO3, reacting at the temperature of 56 DEG C for 20 hours, and dissolving a product in a mixed solution of methanol and dichloromethane for recrystallization, so as to obtain water-soluble polyimide; (2) preparation of a polyimide gas separation membrane: taking water as a solvent, dissolving the water-soluble polyimide in water to prepare a casting solution, uniformly performing knife coating on a tetrafluoroethylene plate, standing at a room temperature for 12 hours, and drying in a drying oven at the temperature of 50 DEG C for 6 hours, thereby obtaining the product polyimide gas separation membrane. According to the method disclosed by the invention, the organic solvent is replaced with water for film mulching in the film preparation process based on a green film preparation technology, so that no volatile organic vapor is produced. The prepared polyimide gas separation membrane is excellent in permeability of CO2 gas and high in separation factor of CO2/N2.
Owner:JIANGNAN UNIV

Carboxylic ester structure containing diene monomer and polyester thereof, and sulfur-containing polyester

The invention discloses a carboxylic ester structure containing diene monomer and polyester thereof, and sulfur-containing polyester. The monomer is prepared through the following steps: 1) with one selected from the group consisting of vanillin, syringaldehyde, p-hydroxybenzaldehyde, 3-fluoro-4-hydroxybenzaldehyde, 3-bromo-4-hydroxybenzaldehyde and 3-methyl-4-hydroxybenzaldehyde as a raw material, dissolving the raw material into an organic solvent, then allowing an obtained solution to react with alkenyl halide under the action of a catalyst, and allowing a reaction product to be recrystallized or separated through a chromatography column so as to obtain an olefine aldehyde monomer; and 2) with the olefine aldehyde monomer as a raw material, allowing the olefine aldehyde monomer to reactunder the action of a catalyst and a promoter without a solvent or after the olefine aldehyde monomer is dissolved in an organic solvent, and allowing a reaction product to be recrystallized or separated through a chromatography column so as to obtain the carboxylic ester structure containing diene monomer. The polyester provided by the invention is prepared under the action of a Hoveyda-Grubbs catalyst and p-benzoquinone. The sulfur-containing polyester provided by the invention is prepared by a reaction of the polyester and a dimercaptan compound. The invention relates to a novel monomer and a polymer. The preparation processes for the monomer and the polymer provided by the invention have the characteristics of rich raw material sources, simple preparation process, no generation of flammable and explosive low-boiling-point volatile matters, greenness, environmental friendliness and universality.
Owner:GUIZHOU UNIV

Low-conductivity super-long-acting organic base type anti-freezing cooling liquid

InactiveCN102174313BMeet insulation safety requirementsReduce corrosionHeat-exchange elementsOrganic baseCarboxylic acid
The invention provides low-conductivity super-long-acting organic base type anti-freezing cooling liquid, which comprises the following components in percentage by weight: 15 to 96 percent of anti-freezing agent, 0.05 to 1.5 percent of natural alkaloid, 0.5 to 2.5 percent of hetero-cycloalkane, 0.01 to 0.3 percent of azole component, and the balance of deionized water. In invention, since the natural alkaloid is matched with nonionic organic compounds, the prepared anti-freezing cooling liquid has the characteristics of low freezing point, high boiling point, no scale formation, corrosion protection, high heat efficiency and the like; in addition, the prepared anti-freezing cooling liquid also has ultra-low conductivity which can reach 5 mus / cm and is a few hundredths of the conductivity of a common water cooling medium because the anti-freezing cooling liquid does not contain the components of inorganic salts, organic carboxylic acid and the like. The anti-freezing cooling liquid with ultra-low conductivity can effectively slow up the corrosion on metal parts of a cooling system, and meet the requirement of special conditions such as the cooling of a wind generator set and the like on the insulation safety of the anti-freezing cooling liquid. The anti-freezing cooling liquid realizes environmental protection and ultra-long-acting service, and is particularly suitable for special equipment such as a wind generator set, an imperial sedan engine and the like.
Owner:ADVANCED MFG TECH CENT CHINA ACAD OF MASCH SCI & TECH
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