30results about How to "Achieve practical purposes" patented technology

The invention relates to a method for preparing indium niobium co-doped titanium dioxide powder through a co-precipitation method. The method comprises the following steps: (1) preparing a solution, weighting InCl3.4H2O and NbCl and respectively dissolving in absolute ethyl alcohol, thereby obtaining an InCl3 solution and a NbCl5 solution; (2) weighting TiCl4 and dissolving in absolute ethyl alcohol, thereby obtaining a TiCl4 absolute ethyl alcohol solution; (3) dropwise adding the InCl3 solution into the NbCl5 solution, thereby obtaining a mixed solution A; (4) dropwise adding the TiCl4 absolute ethyl alcohol solution into the mixed solution A, thereby obtaining a mixed solution B; (5) using ammonium hydroxide for adjusting pH of the mixed solution B till pH is more than or equal to 11, thereby forming a suspension; (6) performing suction filtration on the suspension, drying the obtained precipitate, grinding and sieving, thereby obtaining precursor powder; (7) roasting the precursor powder prepared in the step (6) at 1100-1200 DEG C, thereby obtaining the indium niobium co-doped titanium dioxide powder.

An in-situ EXAFS characterization method for the crystallization kinetics of amorphous alloys belongs to the field of nanocrystalline material preparation technology. It uses Fourier transform and structural function derivation, and uses a specific JMA equation for segmental fitting to analyze crystals. Kinetics, making the analysis more accurate and reliable.

The invention discloses a method for synthesizing copper-rare earth nanometer petal-shaped metal oxides, which comprises: weighing copper and rare earth soluble salt compounds in deionized water according to a molar ratio of 0.3 to 2:1, and dissolving them in deionized water at 0 to 90 Stir at ℃ for 10-90 minutes; add coordination solvent, continue to stir, and let the solution stand for 30-120 minutes to obtain an acidic precursor; add a neutralizing precipitant to the acidic precursor solution to make the solution If stratification occurs, add the coordination solvent again, and repeat the operation from the beginning of stirring to the end of standing until the solution appears stratified; After 3-5 hours, a metal oxide material with a petal-like lamellar structure is obtained. The invention realizes the mixing of materials at the atomic size, and can accurately control the atomic ratio; after low-temperature sintering, a copper-rare earth nano-petal-like sheet structure with high purity and uniform sheets composed of nanoparticles is prepared.

The invention discloses a method for preparing nano-powder with a core-shell structure assisted by in-situ co-precipitation with surfactants. The preparation process is as follows: Weigh the nitrates of barium, strontium and magnesium according to the precise stoichiometric ratio and dissolve them in water to prepare A solution, and press Accurate stoichiometric ratio Weigh butyl titanate and dissolve in ethanol-oxalic acid solution to prepare B solution, weigh a certain amount of surfactant and dissolve in hot water-alcohol to prepare C solution, slowly drop ammonia into A, B and The co-precipitation reaction was carried out in the mixed solution of C, and the pH of the reaction system was controlled to be 2. After the precipitate was filtered, washed, heat-treated and ground, Ba1-nSrnTiO3@MgO core-shell nanopowder with high crystallinity was obtained. The preparation process of the invention is simple, the cycle is short, and the cost is low, and the obtained nano-composite powder has good dispersibility, uniform particle size, high crystallinity and coating structure, which can achieve the purpose of practical application.

The invention relates to a preparation technique for jacket-type glass piston. Wherein, using the blown piston-core shell as the jacket inner layer, fused sealing the broken small end with a glass tube; connecting a glass tube on the shell opening as a inner branch tube, blasting one end of glass tube and the large end into a glass ball; cutting part of the ball on blaze to cover a glass tube as the jacket outer layer; connecting and fused sealing two ends and the necked glass balls on ends of inner layer; connecting a out branch tube on outer glass tube; lengthening the inner branch tube; annealing and grinding the piston inner core and shell. This invention improves precision and reduces cost.

The method for measuring the kinetic curve of the ordering process of metallic glass in situ by synchrotron radiation belongs to the field of nanocrystal preparation technology, and mainly solves the problem of dynamic characteristics of the ordering process of metallic glass, including: in-situ synchrotron radiation of ordering metallic glass Determination; atomic structure distribution calculation; data dynamics fitting; ordered dynamics feature analysis. This method can accurately and reliably measure and analyze the kinetic characteristics of the ordering process, so as to guide the production and preparation process of nanocrystalline materials and achieve the purpose of practical industrialization.

The invention discloses a solid section temperature variation determination method, which is characterized by comprising the following steps: 1, measuring a change curve of surface temperatures of a solid along with time in a known environment by a determinator, and fitting the measuring curve to a continuous curve to avoid breakpoints during measuring; 2, carrying out differentiation on the fitted measuring curve to obtain a cooling velocity curve; 3, calculating a temperature-time curve of a random location of the measured section of the solid; 4, calculating the start point of a cooling curve of the random location on the measured section; 5, calculating all points at the temperature interval delta ti; 6, superposing overcooling austenite continuous isothermal cooling transition curves of steel and iron materials; and 7, calculating the depth of a through hardening layer. The solid section temperature variation determination method simplifies a complex calculation process without reducing the calculation accuracy, and achieves the purpose of practicability.

The neutron diffraction characterization method for the crystallization kinetics of bulk amorphous alloys, through Fourier transform and structure function derivation of the diffraction data, obtains the distribution data of atoms in nanocrystals under different time conditions, and uses specific JMA equations Segmented fitting, based on which the crystallization kinetics analysis was carried out. The present invention starts from the most fundamental atomic structure, accurately and reliably measures and analyzes the kinetic characteristics of nanocrystal formation, and achieves the purpose of practical application.

A method for characterizing the kinetic properties of amorphous-crystal transitions with high-energy X-rays, belonging to the technical field of nanocrystalline alloy preparation, by performing Fourier transform and structure function derivation on diffraction data to obtain the distribution of atoms in the matrix under different time conditions Data, and use a specific JMA equation for segmental fitting to obtain the Avrami index, based on which the amorphous-to-crystal transition kinetics analysis is performed, making the analysis method more convenient and accurate.

A method for characterizing the ordering process of metallic glasses by using EXAFS, comprising: measurement of EXAFS absorption spectrum of ordered metallic glasses; calculation of atomic structure distribution; data dynamic fitting; analysis of ordering dynamics characteristics. This method can accurately and reliably measure and analyze the kinetic characteristics of the ordering process, so as to guide the production and preparation process of nanocrystalline materials and achieve the purpose of practical industrialization.

The invention relates to a composite preparation method for a fine crystal titanium alloy, which comprises the following steps of: performing cold isostatic pressing and vacuum sintering on hydrogenated dehydrogenation titanium alloy powder, then performing first heating high-temperature isothermal forging by adopting medium strain rate over a transformation point to close internal holes of the powdery alloy, improve the compactness of the alloy and improve the plasticity of the alloy, performing second heating low-temperature isothermal forging by adopting medium strain rate below the transformation point to further compact and thin the powdery titanium alloy, and finally performing thermal treatment to obtain the high-compactness fine crystal powdery titanium alloy. According to the preparation method, the preparation period of common forged titanium alloy is effectively shortened, the loss of raw materials is reduced, near net shape precision forgings can be simultaneously formed, the prepared powdery titanium alloy has no component segregation, the compactness is more than 99 percent, the equiaxial tissues are uniform and fine, the size of alpha phase is less than 2 microns, and the mechanical property is excellent.

A high-energy X-ray characterization method for the kinetic process of nanocrystallization. Through Fourier transform and structure function derivation of radiation data, the distribution density data of atoms in nanocrystals at different time conditions are obtained, and the specific JMA equation is used for analysis. The Avrami index is obtained by segment fitting, and the crystallization kinetics analysis is performed based on this, which makes the analysis more accurate and reliable.

A method for characterizing the ordering process of bulk metallic glasses using in-situ neutron diffraction, including: in-situ neutron diffraction measurement of ordering of metallic glasses; calculation of atomic structure distribution; data dynamic fitting; ordering kinetic characteristics analyze. The present invention starts from the disorder-to-order transition of atomic stacking, combines the ordering process with macroscopic production and preparation conditions, accurately and reliably measures and analyzes the kinetic characteristics of the ordering process, and guides nanocrystalline The production and preparation process of materials achieves the purpose of practical industrialization.

The invention discloses a solid section temperature change measurement system. The solid section temperature change measurement system is characterized by comprising a module for intercepting solid surface temperature and time relations, a data fitting module, a fitting data differential module, a parameter input and calculation module and a CCT (continuous cooling transformation) and TTT (time temperature transformation) curve superposition module. Influences of internal heat sources, quality, physical properties and ingredients of solids on heat transfer are embodied on temperature time curves of the solid surfaces classified according to shape, and different temperature moments form a cooling curve from the measured section center parts of the solids to the random surface positions by measuring surface temperature time curves of to-be-measured objects, obtaining temperature change speeds of the object surfaces and calculating moments with the same temperature as the surfaces from the center parts of the measured solids to the random surface positions. The complex calculation process is simplified while calculation accuracy is not reduced, and the goal of practicality is achieved simultaneously.

The invention relates to a method for preparing nano (1-x)Ba1-nSrnTiO3-xMgO complex-phase powder in situ by coprecipitation. A preparation flow comprises the following steps: weighing nitrates of barium, strontium and magnesium into water according to an accurate stoichiometric ratio to prepare a solution A; weighing butyl titanate according toan accurate stoichiometric ratio and dissolving into an ethanol-oxalic acid solution to prepare a solution B; slowly dropwise adding ammonia water into a mixed solution of the solution A and the solution B and carrying out a coprecipitation reaction; controlling the pH value of the reaction system to be 2-10; and carrying out filtering, washing, heat treatment and grinding on precipitate to obtain the nano (1-x)Ba1-nSrnTiO3-xMgO complex-phase powder. The preparation process is simple, short in period and low in cost; and the obtained nano complex-phase powder has good dispersity, uniform grain diameter and high degree of crystallization and can be put into practice.