11 results about "Amorphism" patented technology

This invention discloses a method for preparing amorphous Cu-MOFs and their applications, relating to the field of metal-organic framework materials technology. The key technical points are: CuCl2 is used as the copper source and 4,4′-bipyridine as the ligand, and Cu-MOFs are synthesized via a solvothermal method. Transmission electron microscopy shows that the obtained material exhibits a typical micron-scale sheet-like morphology. After etching with ammonia, the sample morphology transforms into rough-surfaced nanospheres with a significantly increased pore size, indicating a local rearrangement of its framework structure. X-ray diffraction analysis shows that the original Cu-MOF has high crystallinity, while the diffraction peaks of the etched aCu-MOF essentially disappear, exhibiting amorphous characteristics. As a signal conversion element in a colorimetric sensor, aCu-MOF can achieve reliable detection of ampicillin under neutral conditions. Using thiram as a cofactor, a highly selective thiram colorimetric sensing system can be constructed.

The present invention discloses a method for screening doping elements for Te-containing phase change materials based on first principles, belonging to the field of phase change storage technology. The present invention uses first principles calculations to analyze the local structure and bonding properties of amorphous models based on element-doped Te-containing phase change materials from different angles at the atomic scale, thereby screening and optimizing different doping elements and doping components. The physical mechanism by which element doping comprehensively improves the crystallization rate, amorphous thermal stability, and reliability of Te-containing phase change materials is obtained at a microscopic level. By optimizing the three goals of improving amorphization stability, crystallization rate, and cycle characteristics, and comparing and analyzing multiple indicators for each optimization goal, the present invention achieves screening and optimization of different doping elements and doping concentrations, providing guidance for the research of element-doped Te-containing phase change materials and devices, thereby greatly reducing experimental costs, shortening the development cycle of materials and devices, and improving R&D efficiency.

The present application relates to amorphous PbO / Ga2O3 composite material and its preparation method and X-ray detector, belong to metal oxide photoelectric function block material field. Amorphous PbO / Ga2O3 composite material, its molecular formula is (PbO) x (Ga2O3) 1‑x , 0.6≤x<0.8. The PbO / Ga2O3 composite material prepared by the present application is amorphous, stable in nature, has strong X-ray absorption capacity, low dark current density and high photoelectric response.

The purpose of the present invention is to provide a method for regenerating a crystalline fluororesin.　The problem can be solved by a method for amorphizing a crystalline component of a crystalline fluororesin according to the present invention, which is characterized by comprising bringing an ionic crystal represented by general formula: MaXb (wherein M is an alkali metal, an alkaline earth metal, NH4 or aluminum; X is a halogen element, NO3, CO3, SO4 or PO4; and a and b each are an integer) into contact with the crystalline fluororesin.

The present application relates to oil and gas exploration technology field, particularly to a kind of amorphous material genesis determination method in rock, on the basis of existing thin section identification analysis method and scanning electron microscopy analysis method, introduce element test and element three end element analysis method, using statistical and element geochemistry View, realize the quantitative analysis of amorphous material genesis in rock, and then analyze rock diagenesis main control factor.Through the determination method, the influence degree of sedimentation and volcanic action can be determined by analyzing the genesis type of amorphous material in rock, and then the main control factor of diagenesis is determined, which can effectively solve the problem of amorphous material genesis identification in rock.

This invention provides a method for quickly identifying the cause of abnormalities that occur during the spray application of amorphous refractory materials. [Solution] Multiple state quantities related to the spraying of amorphous refractory materials are detected from multiple sensors, and when an abnormal value is detected among the values ​​obtained from the multiple sensors, the cause of the abnormal value is identified. To this end, a correspondence relationship is created in advance between the cause of the abnormal value and the detected values ​​of other state quantities excluding the state quantity detected as the abnormal value, and when an abnormal value is detected among the values ​​obtained from the multiple sensors, the cause of the abnormal value is identified based on the correspondence relationship.

The present disclosure is directed to a method to co-synthesize amorphous and crystalline porous materials, including a phase of crystalline solids possessing well-defined structures and uniform pore sizes, and an amorphous phase. A sol-gel formulation which includes a water-soluble fraction of ODSO as an additional component is provided that precipitates multiple solid phases.

Provided herein are methods and apparatus for growing molybdenum (Mo) in features. The methods may be used to grow single-grain Mo in features with super-conformal, conformal, and / or top-heavy growth profiles. In some embodiments, methods involve inducing a local crystallization in an amorphous molybdenum-containing material, etching at least a portion of the amorphous molybdenum containing material, and growing the molybdenum crystallites. The methods may be used for bottom-up deposition of Mo in a feature. In some embodiments, then methods may produce molybdenum gap-fill with a reduced number of crystallite grains inside a feature, nearly a single crystalline domain, or a single crystal inside a feature. The methods may be used for logic and memory applications.

The invention relates to the technical field of material science and solid mechanics, and discloses a method and system for representing densification of an amorphous material under mechanical deformation, and the method comprises the following steps: applying a mechanical load to the amorphous material to initiate local plastic deformation of the amorphous material; milling the deformed region of the amorphous material by adopting a focused ion beam technology to prepare a cross-section sample, and then obtaining the microstructure change of the cross-section sample through a transmission electron microscope to confirm the densified region of the cross-section sample; the degree of densification of the cross-sectional sample is detected and quantified by analyzing an electron diffraction pattern. According to the embodiment of the invention, the key challenge of accurately quantifying the local structure change (the most significant is permanent volume compression (densification)) in the amorphous material under the action of various contact-induced mechanical loads is solved.

The present disclosure relates to a difficultly compatible heterogeneous material component and its sequential additive manufacturing method and system. A second material (10b) is deposited on the surface of a first base layer (11) formed by a first material (10a) to form a second base layer (12) by using a solid phase additive manufacturing process, an amorphous transition layer (13) is formed at the interface region of the first base layer (11) and the second base layer (12), and the first material (10a) and the second material (10b) constitute a difficultly compatible material system; after the amorphous transition layer (13) is formed, a material same as or compatible with the material of the corresponding deposited side base layer is used to form a target component (10) by layer-by-layer deposition on the first base layer (11) and / or the second base layer (12) by using a melting additive manufacturing process; in the melting additive manufacturing process, the amorphous transition layer (13) is actively cooled by using a cooling device, so that the temperature of the amorphous transition layer (13) is maintained below its crystallization temperature, thereby inhibiting the formation of brittle intermetallic compounds.

To provide a novel soft magnetic material that is lower in density and has superior shapeability compared to existing soft magnetic materials. [Solution] Using hematite as the essential raw material and silica, alumina, and calcium oxide as secondary raw materials, the raw material mixture is adjusted in atomic fraction (%) to be i) 15% to 40%, ii) 0.1% to 21% aluminum, iii) 0.1% to 15% calcium, iv) the total of iron, silicon, aluminum, and calcium is 90% or more, and v) the difference between the total content of aluminum and calcium and the iron content is minus 6% or more. This raw material mixture is heated to approximately 1500°C to melt, held for approximately 1 hour, and then rapidly cooled to obtain a material with a density of 3.0 g / cm³. 3 The following, and with a mass magnetic susceptibility of 1.9 cm², 3 We were able to obtain a novel amorphous magnetic inorganic composition with a value of 1 / g or higher.