The invention discloses a central control method for production of tetrakis (dimethylamino)
tin. The production method of the tetrakis (dimethylamino)
tin comprises the following steps: S1, reacting n-
butyllithium and
dimethylamine in a
solvent to generate
lithium dimethylamino; s2, adding
tin tetrachloride to react to generate
tetra (dimethylamino) tin; a central control detection method in the S1 comprises the following steps: taking a reaction solution, adding water for
quenching, adding a
phenolphthalein indicator, titrating with
hydrochloric acid, and calculating a reaction process; the central control detection method in the step S2 comprises the following steps: taking reaction liquid for nuclear
magnetic testing, and judging the reaction process according to characteristic peak information in a nuclear magnetic spectrum. The two reaction steps in the production process of
tetra (dimethylamino) tin are subjected to central control detection, so that the content of active substances can be effectively monitored, the reaction progress can be effectively judged, the complete reaction of each step is ensured, the safety of the production process is improved, the
utilization rate of raw materials is increased, and the yield of products is increased; the
operability, the stability and the
repeatability of production are realized, and the experiment process is more intuitively known and controlled.