The invention relates to a preparation method of a high-temperature structure-function combining B4C / Al
neutron absorbing material. The preparation method comprises the concrete steps of (1) adopting a
high energy ball milling method for ball-milling aluminum
powder into flake aluminum
powder; (2) placing the flake aluminum
powder into an air furnace for pre-oxidizing, and forming a layer of nanometer aluminum
oxide film on the surface of the aluminum powder; (3) uniformly mixing the pre-oxidized flake aluminum powder and micron-sized B4C particles; (4) pressing molding the uniformly mixed powder; (5) conducting
pressureless sintering or hot pressed
sintering on a pressing-molded pressing blank; and (6)
forging, extruding or rolling a sintered billet so as to obtain the high-temperature structure-function combining B4C / Al
neutron absorbing sectional material or
sheet material. By adopting the method, a certain amount of nanometer aluminum
oxide can be introduced into a pure aluminum matrix, and the micron-sized B4C particles are added, so that the aluminum-based
neutron absorbing material with two-phase reinforcement of micron B4C and nano Al2O3 can be prepared, has both a neutron absorbing performance and an excellent high-temperature
mechanical property, and can be applied in the fields of spent fuel
dry storage, transportation and the like.