The invention discloses a method for preparing a
powder sample of an X-
ray photoelectron
spectrometer, and relates to the technical field of X-
ray photoelectron spectrometers, which comprises the following steps of: weighing a
powder sample to be detected, putting the
powder sample into a
crucible, and then putting the
crucible filled with the powder sample into a
drying box for
drying treatment; the method comprises the following steps: putting a sample and spectroscopically pure into an agate
grinding body, fully
grinding and uniformly mixing, sieving for later use after
grinding, weighing the sieved powder, and dividing into a plurality of equal parts; preparing a tabletting mold, placing a powder sample in the tabletting mold, and grinding and uniformly mixing the sample again through an upper mold; according to the method disclosed by the invention, the
spectral purity is proportionally added into the powder sample, so that the number display intensity of the powder sample during detection can be improved, and the final detection effect is further improved; according to the invention, the sample is sheeted by using the pressing
machine, so that the stability of the formed sample can be improved, the loosening phenomenon in the transfer and detection process can be avoided, and meanwhile, the flatness of the surface of the sample can be ensured, so that the accuracy of detection data can be ensured.