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30results about How to "Good superconducting properties" patented technology

Low-fluorine solution deposition and heat treatment process of YBCO (Yttrium Barium Copper Oxide) superconducting thin film

The invention provides a low-fluorine solution deposition and heat treatment process of a YBCO (Yttrium Barium Copper Oxide) superconducting thin film. The low-fluorine solution deposition and heat treatment process comprises the following steps of: firstly, preparing a low-fluorine YBCO solution; secondly, preparing and drying a gel thin film and pre-treating the dried film; and finally, carrying out final treatment on the dry film: using mixed gas of moisture oxygen gas and inert gas and keeping the mixed gas at the furnace temperature of 790-810DEG C for 1-2 hours; switching the atmosphereinto the mixed gas of dry oxygen gas and inert gas with the same oxygen partial pressure; continuously keeping the mixed gas at the furnace temperature of 790-810DEG C for 10-30 minutes; and finally,naturally cooling the mixed gas along with the furnace, switching the atmosphere into dry O2 after the temperature is reduced to 400-500 DEG C, preserving the heat for 2-4 hours, finally naturally cooling to room temperature along with the furnace and taking out a sample. The YBCO superconducting thin film which is finally obtained in the invention has a high c-axle texture and critical current density Jc as high as (1-5)*106A / cm<2> at the liquid nitrogen temperature.
Owner:XIAN UNIV OF TECH

Method for preparing high-temperature superconducting gadolinium-barium-copper-oxygen thin film by utilizing chemical solution method

The invention discloses a method for preparing a high-temperature superconducting gadolinium-barium-copper-oxygen thin film by utilizing a chemical solution method. The method comprises the steps of firstly preparing low-fluorine-gadolinium-barium-copper-oxygen solution which adopts gadolinium oxide or gadolinium acetate tetrahydrate, barium acetate and copper acetate as initial raw materials and adopts a complexing agent, dissolving the initial raw materials in a solvent to form fluorine-contained gadolinium-barium-copper-oxygen solution, then preparing and drying a gel thin film, and finally conducting preprocessing and final processing on the thin film to obtain the high-temperature superconducting GBCO (gadolinium-barium-copper-oxygen) thin film. According to the thin film prepared by the method provided by the invention, the surface of the thin film is smooth, and the thin film has good superconductivity, and is low in preparation cost, simple in process and easy to control; the heat treatment cycle is shortened greatly, and compared with the low-fluorine-gadolinium-barium-copper-oxygen solution prepared by other methods, the method has the advantages that the fluorine content in the low--fluorine-gadolinium-barium-copper-oxygen solution is lower, the preprocessing of the thin film can be completed by the rapid heat processing within the time not more than 2h, and the performances of the obtained thin film can realize the characteristics of high-clinical conversion temperature Tc and high-clinical current density Jc.
Owner:江苏天诚智能集团有限公司 +1

A kind of method for preparing magnesium boride superconducting film

The invention discloses a device and a preparation method for preparing a magnesium borate super-conducting film. The device comprises a deposition chamber, wherein a bubble meter is communicated with the deposition chamber through a pipeline; a gas mixing device is communicated with the deposition chamber through a pipeline; the deposition chamber is communicated with a waste gas treatment device. The preparation method comprises the following steps: preparing a substrate; placing the substrate in a substrate container of a substrate heating device; closing the deposition chamber; vacuumizing; introducing 2 to 10 sccm of (Cp)2Mg and introducing Ar-diluted B2H6 gas to generate an MgB2 film; after a first layer of MgB2 film is generated, cutting off the (Cp)2Mg of the bubble meter and the Ar-diluted B2H6 gas supplied by the gas mixing device; vacuumizing the deposition chamber until the vacuum degree reaches 10 <-4> Pa, introducing 5 to 10 sccm of B2H6 gas; depositing an amorphous elemental boron layer at 450 DEG C to 600 DEG C; repeating the steps 3 to 5 to prepare a plurality of layers of MgB2 films. According to the device and the preparation method, the problems that the process is complicated, the preparation cost is high, the superconducting character of a finished product is degenerated because a sample is easily subjected to external pollution during a transferring process and the like in the prior art for preparing a multi-layer MgB2 superconducting film are solved.
Owner:GUIZHOU UNIV

Rapid sintering preparation method of tl-2212 superconducting thin film

The invention discloses a rapid sintering preparation method of Tl-2212 superconducting thin film. Silver foil or gold foil is used to seal and wrap the amorphous precursor film containing thallium and the burning target containing thallium, and the Sintering in the environment. The invention includes four processes including the preparation of a precursor film, the preparation of a thallium source accompanying firing target, the rapid temperature-raising sintering of the precursor film in an argon / oxygen environment, and the oxygen-supplementing heat treatment of a primary sample. Compared with the traditional sintering method, the sintering conditions for growing Tl‑2212 thin films using this technology are not affected by the deposition method of the precursor film, the powder particle size of the starting material of the thallium source accompanying firing target and its preparation method, avoiding the Due to the replacement of the manufacturer's raw materials and the pioneering film deposition method, it is necessary to re-explore the sintering process for a long time. At the same time, the method also greatly reduces the amount of the thallium source accompanying the burning target, shortens the heating and cooling time and constant temperature time, reduces the production cost, and improves the repeatability of the experiment.
Owner:GUANGXI TEACHERS EDUCATION UNIV

Method for preparing nanostructure using photo-activation nano active water

The invention discloses a method for producing nanometer structure with nano-photocatalytic active water. Templates and nanometer materials to be processed are immerged in the nano-photocatalytic active water; under irradiation of ultraviolet, the nanometer materials are deposited on the templates to generate the nanometer structure. Nanometer atom in the active water can be deposited on the templates or a work piece to crank out a nanometer product, thus replacing methods of high temperature, microvacuum, electron beam, laser, and vapor phase, and the like, for producing the nanometer structure. The nanometer structure prepared by the method is compact, well distributed, and is provided with strong bonding force, and is characterized by distinct properties of mechanics, optics, heat exchange, electromagnetic, superconduct, electricity, physics, and chemistry, and the like, particularly, the nanometer structure can be applied to important fields of national defense, military affairs, medical treatment, epidemic situation, industry and agriculture, and has important significance, can be capable of being applied to key technology which can not be solved by current technology. The technical craft is simple and is suitable for industrialized production; the cost is low; the technique can become a technical revolution.
Owner:张金龙

Method for preparing gadolinium-barium-copper-oxygen (GdBCO) high-temperature superconducting thin film by using chemical solution method

The invention discloses a method for preparing a gadolinium-barium-copper-oxygen (GdBCO) high-temperature superconducting thin film by using a chemical solution method. The method comprises the steps of: firstly, preparing a low-fluorine GdBCO solution, wherein the low-fluorine GdBCO solution is prepared by adopting gadolinium oxide or gadolinium acetate, barium acetate and copper acetate as initial raw materials, adopting a complexing agent and dissolving the initial raw materials in a solvent; then, preparing and drying a gel thin film; and finally carrying out preprocessing and final processing on the thin film to obtain the GdBCO high-temperature superconducting thin film. The thin film prepared by using the method provided by the invention is smooth in surface, favorable in supoerconducting property, low in preparation cost and simple in a process which is easy to control; and the period of a thermal treatment process is greatly shortened, compared with low-fluorine GdBCO solutions prepared with other methods, the GdBCO high-temperature superconducting thin film is lower in fluorine content and can be preprocessed through rapid thermal treatment being less than 2 hours, and the obtained thin film also has the characteristics of high critical transformation temperature Tc and high critical current density Jc.
Owner:XIAN UNIV OF TECH
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