The invention provides a combined type multifunctional experiment tower and an experiment device thereof. The experiment tower is assembled by a tower kettle segment, a plate type tower segment, a filler tower segment, a condensing tower segment, an entrainment test tower segment and a plurality of closing plates. The experiment device is formed by the connection of the experiment tower, a gas bomb, a fan, a recirculation tank and a flowmeter by a conduit, a valve, and the like. The experiment device can realize the cold-hot die rectification experiment technological process by switching the valve, and the experiment technological process is very convenient to convert. The absorption and desorption experiment technological processes further can be realized by the reassembly of the tower segments and the connection between the tower device and the external equipment, so that the research field of the absorbent is widened. The experiment device is modularized in structure, convenient toinstall, and strong in experiment function, can run under the condition of the water and the electricity, can be used for performing the on-line research of the tail gas recovery in chemical factories such as the oil refinery, the coal chemical factory and the like, and can be used for treating the wastewater which is more dispersed and is small in quantity in the oil extraction factory and the like.