Relating to the technical field of large-scale
high concentration hydrogen peroxide production technologies, particularly to
hydrogen peroxide production technologies by an
anthraquinone process, the invention provides a production method of
hydrogen peroxide. The method includes: taking heavy aromatics, tetrabutylurea and trioctyl
phosphate as solvents, adopting 2-ethylanthraquinone as a reaction material, adding a well prepared working solution into a circulating working solution
storage tank, making use of a circulating working solution pump to send the working solution into a working solution thermoregulator, using circulating cooling water to lower the temperature of the working solution to about 35DEG C, then bringing the working solution to the bottom of a
fluidization hydrogenation reactor, adding a hydrogenation catalyst into the
fluidization hydrogenation reactor in advance through a catalyst adding groove, at the same time, passing
compressed hydrogen through a hydrogen buffer filter to filter out impurities, then letting the
compressed hydrogen enter the bottom of the
fluidization hydrogenation reactor, using the
compressed hydrogen to blow and stir the catalyst and the working solution so as to undergo
hydrogenation reaction at a temperature of about 50DEG C, under a pressure of about 0.26mPa, and at hydrogenation efficiency of about 13g / L.