The invention discloses a shut-down method of a diesel oil
liquid phase hydrogenation device, which comprises the following steps: (1) firstly reducing the feeding temperature of a diesel oil
raw material, introducing supplementary
hydrogen into the diesel oil
liquid phase hydrogenation device by a new
hydrogen compressor at the same time, stopping feeding the diesel oil
raw material after the
reaction temperature is reduced, introducing light distillate oil to wash each catalyst
bed layer in a reactor, and stopping feeding the light distillate oil after the
reaction temperature is reduced; after the washing is finished, stopping injecting the light distillate oil; (2) closing a supplemental
hydrogen valve, enabling supplemental hydrogen to pass through the
heating furnace and the gas-liquid mixer, enabling the heated supplemental hydrogen to enter from the top of the reactor to perform first purging, then introducing part of
fuel gas of the
heating furnace into a catalyst
bed layer at the lower part of the reactor to perform second purging, stored oil of the lower
bed flows out from the bottom of the reactor under the combined action of supplementary hydrogen and
fuel gas. According to the method, the oil carrying effect of the catalyst during shutdown is effectively improved, the purging time is shortened, and the shutdown process of the liquid-phase hydrogenation device can be rapidly completed.