The invention relates to a method and a device for determining material
solid / liquid interfacial energy by experiment, and belongs to the field of solidification technology in material preparation. The invention is characterized by comprising the following steps that: A, a
metal ingot is
cut into a cylindrical bar with a proper size through a
wire cutting machine; the cylindrical bar is cleaned up and dried by a blow drier; the dried cylindrical bar is placed into a suited alundum tube and is fixed on a draw bar; the draw bar with the dried cylindrical bar as a sample, a cooling tank and a
servo motor are assembled well; and a position of the sample in a
heating system is adjusted by the draw bar and it is ensured that a part of the sample bar is melted well; B,
argon as protective gas isfed into the
heating system; after 20 minutes, the
heating system is started, when a temperature in a furnace of the heating
system rises to an objective temperature, the temperature in the furnace is kept for a period of time to ensure the stabilization of
heat flow in the furnace; C, a
metal globular
solid which is congener with the sample is placed on the surface of the molten sample from the upper portion of the device; when the surface of the
metal globular
solid is infiltrated with the molten sample, a
servo drawing
system is started; the sample is pulled down fast and enters into the cooling tank to be quenched and thus a feature of a solid /
liquid interface is maintained; and a
contact angle value is obtained by a
direct measure and is substituted into an interfacial tension balance formula and interfacial energy is calculated out by the formula. The present device realizes a core idea that a feature of a solid /
liquid interface of a sample at a high temperature is maintained byfast
quenching.