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104results about How to "Rapid quenching" patented technology

Method and device for determining material solid/liquid interfacial energy by experiment

The invention relates to a method and a device for determining material solid / liquid interfacial energy by experiment, and belongs to the field of solidification technology in material preparation. The invention is characterized by comprising the following steps that: A, a metal ingot is cut into a cylindrical bar with a proper size through a wire cutting machine; the cylindrical bar is cleaned up and dried by a blow drier; the dried cylindrical bar is placed into a suited alundum tube and is fixed on a draw bar; the draw bar with the dried cylindrical bar as a sample, a cooling tank and a servo motor are assembled well; and a position of the sample in a heating system is adjusted by the draw bar and it is ensured that a part of the sample bar is melted well; B, argon as protective gas isfed into the heating system; after 20 minutes, the heating system is started, when a temperature in a furnace of the heating system rises to an objective temperature, the temperature in the furnace is kept for a period of time to ensure the stabilization of heat flow in the furnace; C, a metal globular solid which is congener with the sample is placed on the surface of the molten sample from the upper portion of the device; when the surface of the metal globular solid is infiltrated with the molten sample, a servo drawing system is started; the sample is pulled down fast and enters into the cooling tank to be quenched and thus a feature of a solid / liquid interface is maintained; and a contact angle value is obtained by a direct measure and is substituted into an interfacial tension balance formula and interfacial energy is calculated out by the formula. The present device realizes a core idea that a feature of a solid / liquid interface of a sample at a high temperature is maintained byfast quenching.
Owner:SHANGHAI UNIV

Multifunctional one-furnace multi-strip quick high-efficiency heat treatment production line and process for bimetal strip saw blades

The invention discloses a multifunctional one-furnace multi-strip quick high-efficiency heat treatment production line and a process for bimetal strip saw blades, and relates to a heat treatment production line and a quenching process for bimetal strip saw blades. By the production line and the process, a technology for heating and cooling the saw blades quickly is implemented, the saw blades have high quality, and high efficiency, high capacity, low input, low cost and low energy consumption are achieved. Quick step quenching is performed by a deep cooling, water cooling, air cooling and nitrogen composite cooling process, so that the high efficiency and high capacity of production and the high quality of the saw blades can be ensured; and all process equipment is integrated into one production line, all processes such as quenching, tempering, sand blasting, cleaning, drying, marking, oiling, straightening and the like are finished on one production line, and a plurality of band saw blades of various specifications can be produced on one production line simultaneously. After the production line is implemented, the capacity of the saw blades is improved by about 3 times, the quality of products is improved by about 30 percent, energy such as electricity, water, oil, gas and the like is saved by over 200 percent, project investment is saved by over 200 percent, plant and land are saved by over 150 percent, production cost is reduced by over 50 percent, and the contradiction and technical bottleneck problem of conventionally exchanging quality for yield and exchanging high input for high capacity for years are radically solved.
Owner:曹玉贵

Quick quenching device and method for shaft parts

The invention discloses a quick quenching device and method for shaft parts. The quick quenching device for shaft parts is provided with a temperature monitoring device, a laser device, a liquid nitrogen cooling system, a workpiece clamp and a connecting plate assembly, wherein the connecting plate assembly is provided with a manipulator connecting plate, a connecting component and a spray nozzle connecting plate, a laser head is installed on the manipulator connecting plate, and a liquid nitrogen spray nozzle is installed on the spray nozzle connecting plate and is connected with a liquid nitrogen cooling system control valve through an air delivery pipe. The workpiece clamp is arranged under the connecting plate assembly and is provided with a chuck, a tip and a control system for controlling rotation of the chuck, and a workpiece is arranged between the chuck and the tip. The temperature monitoring device is arranged on one side of the connecting plate assembly and is used for monitoring the temperature of a laser quenching zone on the workpiece. By the adoption of the quick quenching device and method for shaft parts, the automation degree of surface laser strengthening of large shafts can be improved, working efficiency can be improved, shaft surface strengthening and near-net shaping can be also achieved, additional machining is not needed basically, and working procedures and cost are saved.
Owner:LIAONING UNIVERSITY OF TECHNOLOGY

New method for performing data correction by using cell metabolite relative content as cell number index

The invention discloses a new method for performing data correction by using cell metabolite relative content as cell number index. The new method is characterized by comprising the steps of: realizing the fast quenching of biochemical metabolism in cells by using a simple sample pre-processing method; efficiently extracting small molecule metabolites by an optimized extraction solvent; and roundly and half quantitatively measuring the small molecule compounds in a biological sample by a metabonomics method based on measuring technology like mass spectrum, nuclear magnetic resonance and the like so as to identify a quantitative index of symbolic metabolites in cells to be as the cell number, and regarding the quantitative index as a weight factor to perform data correction. Compared with the quantitative index of the prior cell number, the method is simple, fast and with good repeatability; additional experimental working and the error caused by the additional working are reduced; the accuracy and reliability of experiment result are improved; the difficulty for relatively quantifying the number of in vitro cultured cells is solved; a new displacing method is supplied for cell metabonomics and relevant researches; and the method can be widely used in the relevant researches in the field of cell molecular biology.
Owner:CHINA PHARM UNIV

Method for extracting scopoletin compounds from tobacco

The invention discloses a method for extracting scopoletin compounds from tobacco. The method is characterized by comprising the following steps of preparing tobacco extracts; performing water dissolution on the tobacco extracts; then, performing extraction; eluting the extraction liquid in a macroporous resin chromatographic column by ethyl alcohol; after eluant is collected, performing reduced pressure concentration; then, performing capillary tube sampling thin-layer chromatography; merging the eluant with the similar ingredients; performing reduced pressure concentration until the materials are dry so that a tobacco polar extract is obtained; merging samples showing brownish black spots by a thin-layer chromatography method; performing reduced pressure concentration; obtaining coarse extracts; uniformly stirring the coarse extracts and silica gel; using a positive phase silica gel column for separation and elution; by using the thin-layer chromatography method, merging flavor matters according to different Rf values in accordance with different polarities to obtain fine extracts; performing positive phase column chromatography on the fine extracts; performing elution; segmenting TLC detection into five parts from A to E; performing reverse phase silica gel column chromatography on the section B; then, feeding the sample to a half preparation chromatography system for separation; under each chromatography condition, maintaining the time for 7.23 minutes; and performing separation to obtain the monomeric compound.
Owner:GUIZHOU TOBACCO SCI RES INST
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