The invention provides a scandate active material with high Sc2O3 content and application thereof in an impregnated
diffusion cathode, and belongs to the technical field of manufacturing of thermal
diffusion cathodes for vacuum electronic devices, and the scandate active material is obtained by mixing BaCO3, CaCO3, Al2O3 and Sc2O3 according to a
molar ratio of 12: 2: 3: 1,
grinding, pressing into a sheet, heating to 1100-1150 DEG C in air,
sintering for 24-48 hours, cooling and
grinding. By optimizing the proportion of the components, the scandate active substance with the Sc2O3 mole percentage exceeding 5.5% is obtained, and the scandate active substance does not contain an ineffective active substance BaAl2O4, so that the emission performance of the impregnated
diffusion cathode is improved; the
composite material is applied to an impregnated diffusion
cathode, and cathode
surface modification treatment is carried out in combination with a
surface etching technology, so that pore blockage caused by mechanical
polishing or
processing is effectively eliminated, and synchronous improvement of cathode emission
current density and working stability is realized.