The invention discloses a chemical
analysis method for
copper phase in
copper concentrate, which belongs to the field of chemical analysis. The method comprises the following steps: S1 separating the water-soluble
copper in the copper concentrate to be tested, and determining the content of the water-soluble copper by atomic absorption method; S2 separating the
copper oxide in the filter residue A obtained in step S1, and measuring the content of
copper oxide by atomic absorption method; S3 separates the natural copper in the filter residue B obtained in the step S2, and adopts atomic absorption method to measure the content of natural copper; S4 separates the
copper sulfide in the filter residue C obtained in the step S3, adopts a
titration method to measure the content of
copper sulfide; wherein, the The step of separating
copper sulfide in the step S4 includes: first heating and dissolving filter residue C with dilute
nitric acid, then adding dilute
sulfuric acid to continue heating and decomposing, then evaporating the solution to
dryness, adding dilute
sulfuric acid to heat and dissolve to obtain a mixture of copper and iron, and then masking Iron and the
titration method was used to determine the content of copper
sulfide. Adopting the method of the invention avoids the use of highly toxic liquid
bromine, and the determination process is
safer.