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40results about How to "Realize full component utilization" patented technology

Resourceful treatment method for soot from copper melting furnace

The invention discloses a resourceful treatment method for soot from a copper melting furnace. The method comprises the following steps: separating lead-copper and tin-arsenic-zinc-antimony in soot byhigh-temperature alkaline cooking; introducing hydrogen sulfide into the obtained filtrate to precipitate tin-arsenic-antimony, then continuously introducing hydrogen sulfide to participate zinc, dissolving zinc participates by adding sulfuric acid, and performing concentration and crystallization to obtain industrial pure zinc sulfate; adding lead-copper to a hydrochloric acid solution, then adding sodium chlorate, and cooling the obtained solution to obtain lead chloride filtering residues and copper chloride filtrate; adding tin-arsenic-antimony filtering residues to hydrochloric acid fordissolution so as to obtain an antimony-containing solution, extracting the antimony-containing solution by adding an extraction agent, then performing reverse extraction with p ammonia water, performing concentration and crystallization on the obtained stripping solution to obtain antimony chloride, adding the obtained fifth filtering residues to a sodium sulfide solution for reaction, and then performing filtering so as to obtain tin-containing filtrate arsenic sulfide residues. By adopting the method provided by the invention, the separation and recovery of valuable metals in the soot are achieved, the recovery rate is high and the product finally obtained has high purity; and meanwhile, most of by-products thereof are recovered, the cost is low and the process is short.
Owner:王柯娜

Slag modification reducer and preparation method thereof, and method for Fe recovery with slag waste heat

The invention discloses a slag modification reducer. The slag modification reducer is shaped like spherical particles with a particle diameter of 10-30 mm and comprises 100 parts by weight of a fusionagent, 5-24 parts by weight of a reduction agent, 8-18 parts by weight of a binder and 0-10 parts by weight of a fluxing agent. The invention also discloses a method for Fe recovery with slag waste heat. The method comprises the following steps: (a) during a course when slag is discharged from a smelting furnace and poured into a heat-preservation container, the slag modification reducer is addedinto a slag flow, and a modified reduction reaction takes place; and (b) after the slag completes the reaction with the modification reducer, solid slag in the heat-preservation container is crushed,and metal Fe particles and/or Fe ore concentrate powder are obtained through magnetic separation. The method aims at the fact that the slag contains a lot of waste heat and residual Fe resources, directly conducts high-temperature waste heat modification of the slag, adjusts chemical components and a smelting temperature of the slag, reduces reduction potential energy of Fe oxides and then uses amiddle-low temperature roasting temperature and a grinding-separation technology to realize efficiency recovery of Fe in the slag.
Owner:CHINA ENFI ENGINEERING CORPORATION

Method for recovering metal lead from waste lead-containing glass and producing water glass

The invention relates to a method for recovering metal lead from waste lead-containing glass and producing water glass. The method comprises: placing waste lead-containing glass, a flux, a reducing agent and a catalyst into a high-temperature reaction furnace according to a certain ratio, and carrying out a reaction to reduce out lead while produce molten residue; hydrolyzing the molten residue, and separating to obtain a hydrolyzing liquid and dissolving residue; adding a precipitant to the hydrolyzing liquid to precipitate out lead sulfide and obtain crude water glass; adding an acid solvent to the dissolving residue to neutralize; carrying out dissolving washing on the obtained acid dissolving residue by using the crude water glass again, and separating and recovering the final crude water glass and generating the tailing residue; adding a precipitant and a desulfurizing agent to the final crude water glass to prepare the refined water glass, and recovering the precipitated lead sulfide; and washing the tailing residue, and carrying out acid dissolving treatment again. According to the present invention, with the method, the metal lead can be recovered from the waste lead glass and the water glass can be produced; and the process is simple and is easy to performed, the solid waste emission does not exist, the utilization of the whole components of the lead-containing glass waste is achieved, and the economic benefits are significant.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY +3

Method for preparing functional grape seed nanosphere particles by using grape seeds and product thereof

The invention discloses a method for preparing functional grape seed nanosphere particles by using grape seeds, the method comprises the following steps: crushing grape seeds in residues after wine brewing, firstly extracting grape seed oil by petroleum ether-ultrasonic assistance through process optimization, then extracting procyanidine in the grape seeds by using ethanol, dissolving the grape seed lignin in a tetrahydrofuran aqueous solution (the normal temperature is about 25 DEG C, and heating is not needed), performing rotary evaporation precipitation and washing, and then preparing grape seed nanosphere particles with excellent morphology and high added value. The method is easy to operate and low in cost, the application value of the grape seed residues is effectively improved, all-component utilization of the grape seed residues is achieved, and the prepared nanosphere particles have high ultraviolet absorption capacity and certain oxidation-reduction capacity and are suitable for large-scale production. The nanosphere particles can be used as an efficient and natural raw material and have a huge application prospect in preparation of anti-ultraviolet coatings or protective articles and preparation of cosmetics and drug carriers.
Owner:QILU UNIV OF TECH +1

A kind of resource treatment method of copper smelting furnace soot

The invention discloses a resourceful treatment method for soot from a copper melting furnace. The method comprises the following steps: separating lead-copper and tin-arsenic-zinc-antimony in soot byhigh-temperature alkaline cooking; introducing hydrogen sulfide into the obtained filtrate to precipitate tin-arsenic-antimony, then continuously introducing hydrogen sulfide to participate zinc, dissolving zinc participates by adding sulfuric acid, and performing concentration and crystallization to obtain industrial pure zinc sulfate; adding lead-copper to a hydrochloric acid solution, then adding sodium chlorate, and cooling the obtained solution to obtain lead chloride filtering residues and copper chloride filtrate; adding tin-arsenic-antimony filtering residues to hydrochloric acid fordissolution so as to obtain an antimony-containing solution, extracting the antimony-containing solution by adding an extraction agent, then performing reverse extraction with p ammonia water, performing concentration and crystallization on the obtained stripping solution to obtain antimony chloride, adding the obtained fifth filtering residues to a sodium sulfide solution for reaction, and then performing filtering so as to obtain tin-containing filtrate arsenic sulfide residues. By adopting the method provided by the invention, the separation and recovery of valuable metals in the soot are achieved, the recovery rate is high and the product finally obtained has high purity; and meanwhile, most of by-products thereof are recovered, the cost is low and the process is short.
Owner:王柯娜

Biomass-based papermaking reinforcing agent prepared by taking agricultural residues as raw materials, and preparation method and application thereof

ActiveCN113832769ASolve the problem of conversion and utilization of high added valueRealize cleaner productionReinforcing agents additionPaper/cardboardAgricultural scienceAgricultural engineering
The invention discloses a biomass-based papermaking reinforcing agent prepared by taking agricultural residues as raw materials. A preparation method comprises the following steps: removing non-plant impurities in the agricultural residue raw materials, and treating the raw materials; carrying out autocatalytic hydrolysis treatment on agricultural residues obtained after material preparation to loosen the tissue structure of the raw materials; grinding a material obtained after autocatalysis treatment to enable the size of the material to reach a cellular level; carrying out biological enzyme treatment on the roughly ground material to further destroy the cell wall structure of the raw material; and carrying out micronization treatment on the material subjected to enzyme treatment to make cell walls microfibrillated so as to obtain a product that is the biomass-based reinforcing agent. In agricultural residues such as corncobs, rice husks, bagasse pith, sweet sorghum residue pith and corn straw pith, large-scale high-added-value utilization is not performed on most of the agricultural residues due to low fiber cell content, so that the problem of high-added-value conversion and utilization of the raw materials is solved, and a new way is provided for full utilization of the agricultural residues.
Owner:TIANJIN UNIV OF SCI & TECH

A method for producing butyric acid from corn cob full components

The invention discloses a method for producing butyric acid by utilizing the whole components of corn cobs. Using γ-valerolactone and 1,3-dimethylimidazole dimethyl phosphate ([Mmim]DMP) as solvents, corn cobs were pretreated, and water was used as anti-solvent to precipitate corn cobs, and the residue was obtained by suction filtration , using dried corn cob residue as substrate, cellulase for enzymatic hydrolysis to obtain fermentable sugar; lignin extracted from the pretreatment solvent was precipitated with acid and used to prepare macropores for clostridium tyrobutyricum Calcium alginate-lignin microspheres, so that it can use fermentable sugar to ferment to produce butyric acid, and realize the comprehensive utilization of all components of corn cob. The present invention effectively utilizes the full-component fermentation of corncobs to produce butyric acid, and the combined use of [Mmim]DMP and γ-valerolactone greatly improves the pretreatment effect, enhances the enzymatic hydrolysis efficiency of corncobs, and obtains high yield The fermentable sugar of Clostridium tyrobutyricum was embedded in macroporous calcium alginate-lignin microspheres, and the production of butyric acid was also improved compared with free cells.
Owner:NANJING TECH UNIV

Method for preparing xylooligosaccharide from biomass raw material and application of xylooligosaccharide in preparation of feed additive

The invention discloses a method for preparing xylooligosaccharide from a biomass raw material and application of the xylooligosaccharide to preparation of a feed additive, and the preparation method comprises the following steps: removing impurities from the biomass raw material containing lignocellulose, crushing, adding water, uniformly mixing, adding into a high-pressure reaction kettle, carrying out subcritical hydrothermal hydrolysis reaction at 170-220 DEG C under the condition of homogeneous stirring, filtering, washing, and drying to obtain the xylooligosaccharide. And after the reaction is finished, rapidly cooling to normal temperature, carrying out solid-liquid separation, collecting a hydrolysis mixed solution, and finally, carrying out post-treatment. The preparation of the xylooligosaccharide can be completed through a one-step subcritical hydrothermal hydrolysis reaction, and the particle size of the crushed biomass raw material and the subcritical hydrothermal hydrolysis reaction conditions are synergistically optimized, so that the yield of the xylooligosaccharide can be remarkably improved, and the generation of byproducts can be effectively reduced; the prepared xylooligosaccharide is rich in polysaccharide active ingredients, so that the utilization of the feed by animals can be effectively promoted; in the preparation process, the use of auxiliary materials such as maltodextrin, corn starch and beta-cyclodextrin is avoided, and the production cost can be remarkably reduced.
Owner:CHANGSHA LVYE BIOTECHNOLOGY CO LTD

A device and method for preparing bio-aviation fuel based on ketone platform compounds

The invention provides a device and a method for preparing bioaviation fuel. The device comprises a biomass ketonization reaction system, a carbon chain elongation reaction system, a zeolite catalytic reaction system and an alkane and arene mixing system, wherein the biomass ketonization reaction system is used for catalytically converting biomass into ketones and other monofunctional compounds in an orientated manner, and separating the ketones from the other monofunctional compounds; the carbon chain elongation reaction system is used for converting the ketone platform compounds produced by the biomass ketonization reaction system into alkanes and cycloalkanes through aldol condensation, hydrogenation isomerism and other reactions; the zeolite catalytic reaction system is used for converting the other monofunctional compounds produced by the biomass ketonization reaction system into arenes through zeolite catalytic conversion; the alkane and arene mixing system is used for mixing the alkanes, the cycloalkanes and the arenes according to a certain ratio to obtain the final aviation fuel. With the method, full-component utilization of the biomass can be achieved, the aviation fuel containing the straight-chain alkanes, the cycloalkanes, the arenes and many other components can be prepared, and the ratio of the components is controllable; a novel way of converting the biomass into the aviation fuel is provided.
Owner:JIANGSU UNIV

A rail car type anaerobic-aerobic combined fermentation composting device

The invention relates to a rail car type anaerobic-aerobic combined fermentation and composting device, comprising a liquid storage tank, a sealed box-type casing, and an anaerobic fermentation device and an aerobic fermentation device located in the box-type casing; The box-type housing is provided with a mobile fermentation tank, and the mobile fermentation tank has the first and second working states located in the anaerobic fermentation device and the aerobic fermentation device; the anaerobic fermentation device is sealed, and the bottom is provided with a second A liquid storage tank with a spray head on the inner top; the aerobic fermentation device is provided with an odor outlet pipe and an air intake pipe extending from the outside of the box-type casing to the aerobic fermentation device; the bottom is provided with a second storage tank Liquid tank; the liquid outlets of the first and second liquid storage tanks are connected to the liquid inlet of the liquid storage tank, and the liquid outlet of the liquid storage tank is connected to the spray head. The invention is suitable for high-efficiency clean composting treatment and high-efficiency utilization of all components of multiple wastes, and is especially suitable for comprehensive utilization of multiple wastes mainly in counties or villages.
Owner:NANJING AGRI MECHANIZATION INST MIN OF AGRI
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