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31results about How to "Special affinity" patented technology

Chitosan/ionic liquid cross-linked gel film with sandwich structure and preparation method thereof

The invention belongs to the technical field of film separation and relates to a chitosan/ionic liquid cross-linked gel film with a sandwich structure and a preparation method thereof. The film is characterized in that the film has the sandwich structure, the upper and lower surface layers are arranged as cross-linked surfaces and a gel layer is arranged in the middle. The preparation method comprises the following steps: (1) uniformly mixing chitosan, ionic liquid and solvent under a certain temperature, paving on a polytetrafluoroethylene plate, and drying to remove the solvent to obtain a gel film; (2) soaking the gel film in the solution containing the cross-linking agent and catalyst for 0.2-12 hours and performing the surface cross-linking reaction on the gel film; (3) drying the cross-linked gel film in air for 24 hours, and then transferring into a vacuum drying oven, and processing for 24 hours at 30 DEG C, thereby acquiring the chitosan/ionic liquid cross-linked gel film with the sandwich structure. According to the preparation method provided by the invention, the upper and lower surfaces of the film are cross-linked, so that the chitosan/ionic liquid cross-linked gel film with the sandwich structure is formed, the ionic liquid is difficult to run off, the lasting stability of the physical structure and property of the film is ensured and the preparation method is fit for the separating of the carbon dioxide in the mixed gas and the recycling of the organic steam.
Owner:JIANGNAN UNIV

Preparation method of organic phosphorus pesticide residue detection sensor based on copper/copper oxide nano-wires

The present invention discloses a preparation method of an organic phosphorus pesticide residue detection sensor based on copper / copper oxide nano-wires. The preparation method comprises: (1) synthesizing copper nano-wires; (2) carrying out high temperature calcining to prepare copper oxide nano-wires; 3) preparing a copper nano-wire / graphene / chitosan complex; (4) preparing a copper oxide nano-wire / single-walled carbon nano-tube complex; (5) preparing a modified electrode; and (6) electrochemically detecting the organic phosphorus pesticide residue content. According to the present invention, the Cu / CuO nanometer material has good catalytic performance and excellent sensing performance, has special affinity for thiol-based compounds, can specifically test organic phosphorus pesticides, and further has advantages of low raw material cost and simple and easily-available raw materials, and the detection method is rapid, sensitive and convenient; with the good film forming property of the chitosan, the step for modifying the composite material onto the electrode surface is simplified so as to substantially reduce the electrode preparation cost; and the organic phosphorus pesticide residue is effectively adsorbed onto the electrode material surface by the single-walled carbon nano-tube to form a layer of the barrier for hindering the electron transfer so as to achieve the pesticide detection.
Owner:莆田方家铺子食品营养研究中心

Comprehensive method for removing non-condensable gas dissolved in refrigerant

The invention discloses a comprehensive method for removing non-condensable gas dissolved in a refrigerant, and relates to the technical field of refrigerant production and processing methods, in particular to the comprehensive method for removing the non-condensable gas dissolved in the refrigerant, and the method for removing the non-condensable gas in the refrigerant is divided into four independent methods and two combined methods. The method I specifically comprises the following steps: heating at constant pressure; the second method comprises the steps of degassing and membrane filtration; the third method comprises the following steps: ultrasonic degassing; a fourth method: molecular sieve adsorption; wherein the combination of the first method and the second method and the combination of the first method, the second method and the third method can also be used for removing the non-condensable gas. According to the comprehensive method, in the transferring and sub-packaging process of transferring and sub-packaging the refrigerant into another container, constant-pressure heating, degassing membrane filtration, ultrasonic degassing and molecular sieve adsorption methods are combined to remove non-condensable gas dissolved in the refrigerant.
Owner:HONGMENG TECH ZHEJIANG CO LTD

Intestinal dialysis composition for pet dogs and cats and preparation method of intestinal dialysis composition

The invention discloses an intestinal dialysis composition for pet dogs and cats and a preparation method of the intestinal dialysis composition and belongs to the field of veterinary care. The dialysis composition comprises the following components: 10-20g of unprocessed rehmannia roots, 10-20g of chitosan, 10-20g of calcium butyrate, 50-100g of modified zeolite and 200-300ml of acetic acid witha volume percentage of 4%. The preparation method comprises the following steps: sufficiently dissolving the unprocessed rehmannia roots, the chitosan and the calcium butyrate into the acetic acid, adding the modified zeolite, blending the components into a paste, performing sufficient infiltration, performing pelletizing by using a pelletizer, and performing drying at 60 DEG C for 4 hours, so asto obtain a finished product of which the particle size is 0.8-1.2mm. Components of the intestinal dialysis composition for pet dogs and cats take synergetic effects into play, uremia toxins such as urea and decomposition products, namely substances such as ammonia, phosphate and creatinine, of the uremia toxins, in intestines, can be adsorbed, small molecule substances such as the uremia toxins such as urea in blood can be promoted to be discharged to enterocoels, then the concentration of the small molecule substances in blood can be reduced, hyperazotemic and hyperphosphatemia caused by kidney failure can be relieved, and recovery of kidney failure can be facilitated. The composition is economic and practical and convenient to operate.
Owner:JIANGSU AGRI ANIMAL HUSBANDRY VOCATIONAL COLLEGE

Intestinal dialysis composition for pet dogs and cats and preparation method thereof

The invention discloses a composition for intestinal dialysis of pet dogs and cats and a preparation method thereof, belonging to the pet medical field. The dialysis composition comprises the following components: 10-20g of raw rhubarb, 10-20g of chitosan, 10-20g of calcium butyrate, 50-100g of modified zeolite, and 200-300ml of acetic acid with a volume fraction of 4%. During preparation, fully dissolve raw rhubarb, chitosan and calcium butyrate in acetic acid, then add modified zeolite to make a paste, make it fully infiltrated, granulate with a granulator, and dry at 60°C for 4 hours. Finished products with a particle size of 0.8‑1.2mm. The components of the intestinal dialysis composition for pet dogs and cats provided by the present invention cooperate with each other, and can absorb uremic toxins such as urea in the intestinal tract and their decomposition products such as ammonia, phosphate, creatinine, etc., and promote blood circulation. Small molecular substances such as uremic toxins such as urea are excreted into the intestinal cavity, thereby reducing the concentration in the blood, relieving hypernitremia and hyperphosphatemia caused by renal failure, and benefiting the recovery of renal failure. Economical and easy to operate.
Owner:陕西琢真小动物健康产业研发中心有限公司

A kind of sandwich structure polyether block amide gel membrane and its thermal crosslinking preparation method

The invention belongs to the technical field of gas-membrane separation and relates to a polyether-block-amide gel membrane with a sandwich structure and a thermal-cross-linking preparation method thereof. The polyether-block-amide gel membrane is characterized by being provided with the sandwich structure, wherein the upper surface layer and the lower surface are cross-linked layers, and a gel layer is arranged in the middle. The preparation method comprises the following process steps: (1) mixing polyether block amide, ionic liquid and a solvent uniformly at certain temperature, flatly laying the mixture on a polytetrafluoroethylene plate, and drying the solvent to prepare the gel membrane; (2) respectively coating a layer of solution containing a thermal initiator and a cross-linking agent on the upper surface layer and the lower surface layer of the gel membrane, transferring into a baking oven, controlling certain temperature and time, and carrying out surface thermal cross-linking reaction of the gel membrane; and (3) drying the cross-linked gel membrane for 24 hours in the air, then transferring into a vacuum drying box, and treating for 24 hours at the temperature of 30 DEG C to obtain the polyether-block-amide gel membrane with the sandwich structure. The polyether-block-amide gel membrane and the preparation method have the advantages that by cross linking of the upper surface layer and the lower surface layer of the membrane, the polyether-block-amide gel membrane with the sandwich structure is formed, and the loss of polyethylene glycol is not easy, so that the durability and the stability of the physical structure and the properties of the membrane are guaranteed. The polyether-block-amide gel membrane and the preparation method are applicable to separating carbon dioxide in mixed gas and recovering organic vapor.
Owner:JIANGNAN UNIV

Nickel base filter material-based gas phase magnesium purification method and device

ActiveCN110835695ATake advantage of high temperature resistanceExtended service lifePhysical chemistryMetal impurities
The invention provides a nickel base filter material-based gas phase magnesium purification method. The method is characterized in that a nickel base filter material is adopted to filter magnesium vapor, under a certain temperature and vacuum degree, on one hand, the nickel material does not react with the magnesium vapor, so that new impurities cannot be brought to a system; on the other hand, the nickel material and impurities Al and Mn in the magnesium vapor have special affinity, so that a stable solid solution can be formed; and meanwhile, the nickel material can be used as a site for nucleation of a certain of impurities in the magnesium vapor, so that the energy barrier of nucleation is reduced, the certain impurities are deposited in advance, and removal is achieved. According to the method, the method can be applied to industrial large-batch gas phase magnesium purification; the production efficiency is improved by an order of magnitude, and meanwhile, the Mn content in magnesium is reduced to 10 ppm or less, the Al content is reduced to 10 ppm or less, and the Si content is reduced to 20 ppm or less; and non-metal impurity elements such as F, Cl and S can be removed, so that the purity of a product is improved, and the purity of the obtained magnesium is 99.99% or above.
Owner:国科镁业科技(河南)有限公司

Application of Elemental Silicon Filter Material in Gas Phase Magnesium Purification and Production System Containing It

The invention provides the application of elemental silicon filter material in gas-phase magnesium purification. In the gas-phase magnesium purification process, magnesium vapor passes through the elemental silicon filter material. In a certain range of temperature and vacuum degree, elemental silicon will not interact with magnesium vapor on the one hand. The reaction will not form a more stable substance with magnesium in thermodynamics, and will not bring new impurities to the system; on the other hand, the impurities Mn, Al, and Ca in silicon and magnesium vapor have special affinity and can form more Stable solid solution, so as to achieve removal; at the same time, elemental silicon can be used as the nucleation site of certain impurities in magnesium vapor, lowering the nucleation energy barrier, allowing certain impurities to deposit in advance, thereby achieving removal. The invention can effectively remove impurities in the magnesium vapor through the function of the elemental silicon filter material, greatly improve the purity of the magnesium, and the purity of the obtained magnesium is above 99.99%. The production system provided by the invention is suitable for large-scale industrial production, can effectively improve the efficiency of magnesium purification, and reduce the cost of magnesium purification.
Owner:国科镁业科技(河南)有限公司

A kind of sandwich structure polyether block amide gel film and its photocrosslinking preparation method

The invention belongs to the technical field of gas film separation and relates to a polyether block amide gel film with a sandwich structure and a photo-crosslinking preparation method thereof. The film is characterized in that the film has the sandwich structure, the upper and lower surfaces are arranged as crosslinking layers and the middle layer is arranged as a gel layer. The preparation method comprises the following steps: (1) uniformly mixing polyether block amide, ionic liquid and solvent at a certain temperature, paving on a polyfluortetraethylene plate, and drying to remove the solvent so as to obtain the gel film; (2) coating upper and lower surfaces of the gel film with a layer of solution containing photoinitiator and cross-linking agent, transferring into an ultraviolet light curing machine for curing for 20 minutes and carrying out the surface photo-crosslinking reaction of the gel film; (3) drying the gel film after photo-crosslinking in air for 24 hours, and then transferring into a vacuum drying oven and treating for 24 hours at 30 DEG C, thereby acquiring the polyether block amide gel film with the sandwich structure. According to the preparation method provided by the invention, the upper and lower surfaces of the film are subjected to photo-crosslinking so as to form the polyether block amide gel film with the sandwich structure, so that the ionic liquid is difficult to run off, the lasting stability of the physical structure and property of the film is ensured and the film is fit for the separation of carbon dioxide in the mixed gas and the recycling of the organic steam.
Owner:JIANGNAN UNIV

Traditional Chinese medicine compound gel suppository for contraception and preparation method thereof

The invention belongs to the field of research of natural medicines and particularly relates to a traditional Chinese medicine compound gel suppository for contraception and a preparation method thereof. The effective components of the suppository provided by the invention are lightyellow sophora roots and Chinese pulsatilla roots, and the mass ratio of the lightyellow sophora roots to the Chinesepulsatilla roots is 3:1; and the suppository also comprises Carbomer, beta-cyclodextrin, glycerol, sodium hydroxide, ethanol and distilled water. The preparation method comprises the following steps:drying the lightyellow sophora roots and the Chinese pulsatilla roots according to the ratio, then performing reflux extraction, performing rotary evaporateion and concentration on the extracting solution, and metering the volume of the distilled water to obtain a mother solution for later use, wherein each 100ml of the mother solution contains 2g of crude medicines; and mixing the mother solution with ethanol and glycerol to obtain a mixture, then mixing the mixture with a carbomer solution in which beta-cyclodextrin is added, performing uniform mixing, then performing injection molding andcooling, eliminating the overflowing part, and performing mold release to obtain the suppository. The suppository provided by the invention has a good contraception effect, also has a lubrication function, and is safe and effective.
Owner:DALIAN UNIV

A kind of sandwich structure chitosan/ionic liquid cross-linked gel film and preparation method thereof

The invention belongs to the technical field of film separation and relates to a chitosan / ionic liquid cross-linked gel film with a sandwich structure and a preparation method thereof. The film is characterized in that the film has the sandwich structure, the upper and lower surface layers are arranged as cross-linked surfaces and a gel layer is arranged in the middle. The preparation method comprises the following steps: (1) uniformly mixing chitosan, ionic liquid and solvent under a certain temperature, paving on a polytetrafluoroethylene plate, and drying to remove the solvent to obtain a gel film; (2) soaking the gel film in the solution containing the cross-linking agent and catalyst for 0.2-12 hours and performing the surface cross-linking reaction on the gel film; (3) drying the cross-linked gel film in air for 24 hours, and then transferring into a vacuum drying oven, and processing for 24 hours at 30 DEG C, thereby acquiring the chitosan / ionic liquid cross-linked gel film with the sandwich structure. According to the preparation method provided by the invention, the upper and lower surfaces of the film are cross-linked, so that the chitosan / ionic liquid cross-linked gel film with the sandwich structure is formed, the ionic liquid is difficult to run off, the lasting stability of the physical structure and property of the film is ensured and the preparation method is fit for the separating of the carbon dioxide in the mixed gas and the recycling of the organic steam.
Owner:JIANGNAN UNIV
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