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112results about How to "Small fiber diameter" patented technology

Preparation method of silicon-carbide-fibrofelt-enhanced silica aerogel composite material

The invention relates to a preparation method of a silicon-carbide-fibrofelt-enhanced silica aerogel composite material, and relates to an aerogel composite material. According to the invention, a carbon-rich silicon carbide micro-nano ceramic fibrofelt with small fiber diameter, high porosity, communicating pores, fast impregnation speed, and good compatibility with a substrate is prepared with a static electro-spinning technology combined with a precursor conversion method; a silica sol is prepared with an acid-alkali two-step method; with an infiltration technology, the electro-spun silicon carbide ceramic fibrofelt or precast is soaked into the sol; and through processes such as gel process, aging, curing, solvent exchange, supercritical drying, and the like, the silicon-carbide-fibrofelt-enhanced silica aerogel composite material is obtained. The prepared composite material has the characteristics of low density, large specific surface area, super-hydrophobicity, low thermal conductivity, and the like. The strength and toughness of the material are also greatly improved. The carbon-rich silicon carbide fiber has an infrared shielding effect, such that composite material thermal insulation effect and ultra-high-temperature stability can be improved.
Owner:ZHONGKE RUNZI (CHONGQING) ENERGY SAVING TECH CO LTD

Preparation method for multi-component net-shaped nanofiber membrane

The invention relates to a preparation method for a multi-component net-shaped nanofiber membrane. The preparation method includes the detailed steps that step1, mixing and beating are performed on meta-position aramid fibers, halogen salt and organic solvent by the mass ratio of 1:0.004-0.4:2.996-18.6, and a meta-position aramid fiber solution is prepared through mixing; step2, functionality high-molecular polymers and the solvent are mixed by the mass ratio of 1:5.4-98.99, then nano-particles are added, and heating and mixing are performed to prepare a functionality high-molecular solution, wherein the mass fraction of the nano-particles in the solution is 0.01-5%; step3, the meta-position aramid fiber solution obtained in the step1 and the functionality high-molecular solution obtained in the step2 are mixed by the mass ratio of 1:0.05-0.5 in a dripping mode, and then ultrasonic treatment is performed to obtain a spinning solution; step4, under the conditions of 20 DEG C-30 DEG C indoor temperature and 20-70% relative humidity, the spinning solution is used for electrostatic spinning, and finally the multi-component net-shaped nanofiber membrane with a 5nm-20nm net-shaped nanofiber diameter and reaches over 95% in net-shaped structure coverage rate is obtained. The preparation technology is simple and low in cost, tensile strength of material reaches 100MPa-2000MPa, and the functionality advantage is remarkable.
Owner:DONGHUA UNIV

Method for preparing nano-silver-containing composite fibrous membrane capable of being used for medical dressings

The invention relates to a method for preparing a nano-silver-containing composite fibrous membrane capable of being used for medical dressings. The composite fibrous membrane comprises nano-silver-containing polycaprolactone (PCL) / polyvinylpyrrolidone (PVP), and is prepared on the basis of an electrostatic spinning method. The method includes: (1) using N,N-dimethylformamide (DMF) as a reducing agent, reducing silver nitrate in water bath at the temperature of 80-95 DEG C, and stirring continuously for 4-7 hours to obtain a nano-silver colloid solution; (2), mixing the PCL and the PVP according to a certain proportion, dissolving the mixture in cosolvent dichloromethane, and stirring uniformly to obtain a mixed solution; (3) diluting the nano-silver colloid solution by certain times, adding the diluent into the mixed solution, and stirring uniformly to obtain electrostatic spinning liquid; (4) performing electrostatic spinning on the electrostatic spinning liquid to obtain the nano-silver-containing PCL / PVP composite fibrous membrane. The fibrous membrane has the advantages of good biocompatibility, hydrophilia and hydrophobicity controllability, high water absorption and the like; the surface of the fibrous membrane contains nano-silver, so that the fibrous membrane has strong antibacterial action and is suitable for preparing the medical dressings.
Owner:WUYI UNIV

Preparation method of waterproof moisture-permeable nanofiber composite membrane

The invention relates to a preparation method of a waterproof moisture-permeable nanofiber composite membrane, and belongs to the technical field of textile materials. According to the preparation method, polyacrylonitrile is taken as a main raw material, polyvinylidene fluoride and polyurethane are added, the waterproof and moisture-permeable nanofiber composite membrane is prepared, and the waterproof and moisture-permeable membrane prepared from polyacrylonitrile nanofibers has the characteristics of high porosity, fine fiber diameter and small pore diameter. The waterproof and moisture-permeable effect of the fiber membrane is effectively improved, the hydrophobic microporous membrane is preliminarily obtained by blending polyacrylonitrile, polyvinylidene fluoride and polyurethane through a solution, the waterproof moisture-permeable membrane with a certain welding structure is obtained in combination with heat treatment, penetration of liquid water is effectively prevented, polyurethane is a block polymer, polar groups such as hydrophilic groups which exist on a macromolecular chain segment provide a carrier for water vapor transfer, meanwhile, the polyurethane has a certain hydrophobic property by the hydrophobic group on the chain segment, and by addition of the polyurethane, the nanofiber composite membrane has excellent comprehensive performance.
Owner:欧名龙

Centrifugal gas-electric spinning device by utilizing negative-pressure array

The invention discloses a centrifugal gas-electric spinning device by utilizing a negative-pressure array. The centrifugal gas-electric spinning device comprises a high-voltage alternating-current generator, an air supply device, a box body, a centrifugal sprayer, a centrifugal driving mechanism and negative-pressure receiving devices. The interior of the centrifugal sprayer is provided with a liquid storage cavity. Filament outlet holes are arranged in the centrifugal sprayer. Each negative-pressure receiving device comprises a collector, a negative-pressure pipe and a negative air-pressure generator. Negative-pressure pipe openings are formed by negative-pressure pipes in the bottom of the box body. Collectors are nested into the negative-pressure pipe openings. The multiple negative-pressure receiving devices are arrayed in an annular array with the centrifugal sprayer as the center. The high-voltage alternating-current generator is formed for generating an electric field. Airflow spraying out of the filament outlet holes is formed by the air supply device. The centrifugal gas-electric spinning device by utilizing the negative-pressure array has following beneficial effects: nanofibers are formed by sprayed polymers under airflow, an electric field, negative pressure and centrifugal force such that a three-dimensional structure is formed by nanofibers on the negative-pressure receiving devices; thickness of fiber disposition is increased; biological materials are better compatible and the application scope of technology materials is broad; and a support structure obtained is beneficial for cell growth of tissue engineering.
Owner:GUANGDONG UNIV OF TECH

Preparation method and device for three-dimensional support for spinning by utilizing gas-electro spinning based on negative-pressure collection

The invention discloses a preparation method and device for a three-dimensional support for spinning by utilizing gas-electro spinning based on negative-pressure collection. A device comprises an alternating-current high-voltage generator, a liquid supply device, a gas liquid device, a coaxial sprayer and a negative-pressure collecting device. The coaxial sprayer is provided with a liquid outlet and a gas outlet. The gas supply device is used for conveying a spinning solution or melts to the coaxial sprayer and enabling melts to flow out of the liquid outlet. The gas liquid device can generate air flow blowing from the liquid outlet to the negative-pressure collecting device via the liquid outlet. The alternating-current high-voltage generator can form an alternating electric field between the coaxial sprayer and the negative-pressure collecting device. The negative-pressure collecting device comprises a collector, a negative-pressure pipe and a negative-pressure generator. The spinning solution or melts form solution jet flow or melt jet flow in the coaxial sprayer and the collector under effect of airflow and the alternating electric field.The preparation method and device for the three-dimensional support for spinning by utilizing gas-electro spinning based on negative-pressure collection have following beneficial effects: by adoption of spinning technology based on the negative-pressure collector, the nanofiber three-dimensional support featuring a broad range of preparation material, small fiber diameters, uniformly-distributed filament diameters, a loose structure, great thickness and superior mechanical properties is obtained and has great technological universality.
Owner:FOSHAN QINGZI PRECISION MEASUREMENT & CONTROL TECH

Glass cloth and printed wiring board

The present invention is(1) a glass cloth composed of a group of warp yarns and a group of weft yarns wherein one of the group of the warp and weft yarns are arranged with substantially no gap between the yarns, and, in that group, a width A (μm) of a cross-section of the yarn arranged with substantially no gap, a single-fiber diameter L (μm) of the yarn, the number N of single-fibers constituting the yarn and a weaving density C (ends / 25 mm) of the glass cloth composed of the yarns satisfy the following equation (1-a):C×A / (25×L×N)≧1.0, and   (1-a)(2) a glass cloth composed of a group of warp yarns and a group of weft yarns wherein both of the groups of the warp and weft yarns are arranged with substantially no gap between the yarns, and, in both the groups, a width A (μm) of a cross-section of the yarn, a single-fiber diameter L (μm) of the yarn, the number N of single-fibers constituting the yarn and a weaving density C (ends / 25 mm) of the glass cloth satisfy the following equation (1-b):C×A / (25×L×N)≧0.75.   (1-b)The glass cloth according to the present invention is useful as a substrate for a printed wiring board. The printed wiring board using the glass cloth of the present invention as a substrate is capable of being bored with a laser beam to produce micro-holes (the roughness of the inner wall, the reproducibility and the roundness of the micro-holes are improved) therein, especially, is able to prepare uniform and small via-holes which are recently required for high-density wiring.
Owner:ASAHI SCHWEBEL
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