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Method for enriching agaric polysaccharide in purified black agaric by using macroporous absorption resin
The invention belongs to the field of natural organic chemistry, and relates to a method for enriching agaric polysaccharide in purified black agaric by using macroporous absorption resin. The invention is characterized in that a macroporous absorption technology is applied to separate the purified black agaric polysaccharide, the absorption selectivity to the agaric polysaccharide is good, the absorption and analysis are both fast, and the absorption capacity is larger; and the extraction is convenient and fast, the raw material source is rich, the production is low, the separating effect is obvious, the extracting purity is high, semi-finished products of agaric polysaccharide with the content of more than 35 percent and final products of agaric polysaccharide with the content of more than 98 percent can be obtained, and the defects that the conventional method has lower extraction rate and low extraction purity are overcome. The method selects macroporous absorption resin with stable physical-chemical properties, larger surface area, faster exchange velocity, high mechanical strength, strong anti-pollution capability and good heat stability, can absorb the agaric polysaccharide selectively from solution by physical absorption, and has fast absorption and analysis and larger absorption capacity.
Owner:HEILONGJIANG DINGHENGSHENG PHARM CO LTD
Method for enriching and purifying procyanidin in pine bark
ActiveCN102093328AHigh adsorption selectivityParsing fastOrganic chemistryAbsorption capacityDistillation
The invention belongs to the field of natural organic chemistry, relating to a method for enriching and purifying procyanidin in pine bark. The method is characterized in that an intermittent distillation and macropore adsorbent resin coupling technology is used to separate and purify the procyanidin, and the technology is good for absorption selectivity of the procyanidin; and by using the intermittent distillation and macropore adsorbent resin coupling technology, absorption is quick and deabsorption is also quick, absorption capacity is large, extraction is convenient and quick, raw material source is rich, production cost is low, separation effect is obvious, extraction purity is high, above 50% of semi-finished product procyanidin and above 95% of final product procyanidin can be achieved, and the defects of low conventional extraction rate and low extraction purity are overcome. In the method, the macropore adsorbent resin which has the advantages of stable physicochemical property, large surface area, fast exchange speed, high mechanical strength, strong pollution resistance capability and good heat stability is selected, the procyanidin is selectively absorbed from solution through physical absorption, absorption is quick and deabsorption is also quick, and absorption capacity is large.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method for enriching and purifying schizandrol A in schisandra
ActiveCN101786945AHigh adsorption selectivityParsing fastIon-exchange process apparatusEther separation/purificationThermal stabilityAdsorption selectivity
The invention belongs to the field of natural organic chemistry, relating to a method for enriching and purifying schizandrol A in schisandra by utilizing macroporous adsorbent resin. The invention is characterized in that the macroporous adsorption technology, which is used for separating and purfying the schizandrol A, has good adsorption selectivity on the schizandrol A, rapid adsorption, rapid resolution and large adsorption capacity; and the extraction is convenient and fast, the source of raw materials is abundant, the production cost is low, the separating effect is obvious, the extraction purity is high, and the semi-finished product of the schizandrol A of which the content is more than 35% and the final product of the schizandrol A of which the content is more than 98% can be obtained, so that the defects that relatively low extraction rate and low extraction purity of routine extraction are overcomed. The macroporous absorbent resin selected by the invention has stable physicochemical property, larger surface area, fast exchange speed, high mechanical strength, strong anti-pollution ability and good thermostability, thereby being capable of selectively adsorbing the schizandrol A from solution by physical adsorption with the characteristics of fast adsorption, fast resolution and larger adsorption capacity.
Owner:HEILONGJIANG DINGHENGSHENG PHARM CO LTD
Improved composites and methods for conductive transparent substrates
ActiveCN101558456AFast resistivityAvoid high temperature firing stepsTransparent/reflecting heating arrangementsNon-conductive material with dispersed conductive materialConductive materialsOptoelectronics
The present invention is directed to a conductive article and method of making the same that includes a substrate (10); a conductive composite (14) including a conductive material in a matrix that includes one or more film forming resins having at least one functional group capable of polymerization; one or more adhesion promoters; and one or more compounds, which are reactive with the film forming resin and which also contain at least one acidic moiety.
Owner:DDP SPECIALTY ELECTRONICS MATERIALS US LLC
Airfield runway ice and snow melting device
The invention discloses an ice and snow melting device for an airport runway. It has an airport runway. The airport runway includes a runway base layer and a runway surface layer. A heat dissipation system is arranged between the runway base layer and the runway surface layer. The heat dissipation system and The heat source system is connected, and the heat source system includes a circulation pump and a heat source; the heat dissipation system is composed of a finned cooling pipe, an oil inlet main pipe, an oil return main pipe and a pipeline, and the outlet end of the oil return main pipe of the heat dissipation system is connected to the oil return port of the heat source. Connected, the pipe body of the oil return main pipe is respectively connected with the outlet ends of a plurality of fin heat dissipation pipes, the inlet end of the fin heat dissipation pipes is connected with the outlet end of the oil inlet main pipe, and the inlet end of the oil inlet main pipe is connected with the circulation The outlets of the pumps are connected, and the inlets of the circulating pumps are connected with the outlets of the heat source through pipes. The invention can overcome the problem that the normal flight of the aircraft is affected by ice and snow or freezing fog on the airport runway, saves energy, has the characteristics of simple equipment structure, fast ice and snow melting speed, long service life and the like.
Owner:高远新
Method for enriching and purifying common phellinus fungus general flavone in common phellinus fungus
ActiveCN102078339AHigh adsorption selectivityParsing fastFungi medical ingredientsImmunological disordersBiotechnologyCoupling
The invention belongs to the field of natural organic chemistry and relates to a method for enriching and purifying common phellinus fungus general flavone in common phellinus fungus by using a batch distillation-macroporous absorption resin coupling method. The method is characterized in that the common phellinus fungus general flavone is separated and purified by applying a macropore adsorption technology, the adsorption selectivity to the common phellinus fungus general flavone is better, the separation effect is remarkable, the extraction purity is high, the semi-finished product with more than 35 percent of the common phellinus fungus general flavone and the final product with above 90 percent of the common phellinus fungus general flavone can be obtained, and the defects of relatively lower conventional extraction rate and low extraction purity are overcome. Macroporous absorption resin with stable physicochemical property, large surface area, higher switching speed, high mechanical strength, strong contamination resistance and good thermal stability is selected, and the common phellinus fungus general flavone is selectively absorbed from a solution through physical adsorption, thus the method has the advantages of high adsorption, high deabsorption speed and larger adsorption capacity.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method for enriching and purifying betulin in birch barks
ActiveCN102093458AHigh adsorption selectivityParsing fastSteroidsHeat stabilityUltimate tensile strength
The invention belongs to the field of natural organic chemistry and relates to a method for enriching and purifying betulin in birch barks by utilizing a batch distillation-macroporous absorption resin method. The method has the advantages of good adsorption selectivity to betulin, quickness of adsorption and resolution, larger adsorption capacity, convenience and quickness of extraction, rich raw material source, low production cost, obvious separation effect and high extraction purity, can be used for obtaining a semi-finished betulin product with a content higher than 35 percent and a finished betulin product with a content higher than 98 percent and overcomes the defects of relatively lower conventional extraction ratio and low extraction purity. In the invention, macroporous absorption resin having stable physical and chemical properties, larger surface area, higher exchange speed, higher mechanical strength, strong antipollution capacity and good heat stability is used, which can selectively adsorb the betulin from the solution through physical adsorption, thus the invention has the advantages of quickness of adsorption and resolution and larger adsorption capacity.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method for enriching and purifying folic acid in houseleek by macroporous absorbent resin
ActiveCN101775016AHigh adsorption selectivityParsing fastOrganic chemistryAbsorption capacityDesorption
The invention relates to a method for enriching and purifying folic acid in houseleek by macroporous absorbent resin, which belongs to the field of natural organic chemistry. The invention is characterized in that the macroporous absorbent technology is used for separating and purifying the folic acid, the adsorption selectivity on the folic acid is good, both the adsorption and the desorption are fast, the adsorption capacity is large, the extraction is convenient and fast, the raw material sources are rich, the production cost is low, the separation effect is obvious, the extraction purity is high, the folic acid semi-finished products with the content higher than 35 percent and the folic acid finished products with the content higher than 98 percent can be obtained, and the defects of relatively low extraction rate and low extraction purity of the conventional method are overcome. The invention adopts the macroporous absorbent resin with the advantages of stable physicochemical property, large superficial area, high exchange speed, high mechanical strength, strong pollution resistance capability and good thermal stability, the folic acid can be selectively absorbed in the solution through physical absorption, and the invention has the advantages of fast absorption, fast desorption and large absorption capacity.
Owner:HEILONGJIANG DINGHENGSHENG PHARM CO LTD
Novel method for extracting gentiopicrin from wild gentian
InactiveCN103709216AReduce extraction timeActive ingredients are highly activeSugar derivativesSugar derivatives preparationWild GentianUltrafiltration
The invention belongs to the field of natural organic chemistry, relates to a method for extracting gentiopicrin from wild gentian in the Great Khingan Mountains, and in particular relates to a novel method for purifying the gentiopicrin by utilizing supercritical CO2 fluid extraction, ultrafiltration separation, macroporous resin adsorption and column chromatography. The method has the advantages that 1, due to the application of supercritical CO2 fluid extraction, original taste and color can be prevented from being damaged by heat, heat sensitivity can be ensured, easy-to-oxidize substances can be prevented from being damaged, and extract can be separated and purified in an extraction process; 2, due to the adoption of a macroporous resin purification technology, good purification effects on active ingredients are achieved, and industrial production is facilitated; 3, ultrafiltration is finished at normal temperature, so that the structural changes, loss and biological activity of the active ingredients can be prevented from being reduced by heat effects, and the yield of the active ingredients is improved.
Owner:DAXINGANLING GADOL SPORTS INGREDIENT
Self-propagating preparation method for Gd<2>Ti<2-x>Zr<x>O<7> pyrochlore
InactiveCN106986377ARaise the reaction temperatureHigh purityTitanatesSelf-propagating high-temperature synthesisReaction temperature
The invention discloses a self-propagating preparation method for Gd<2>Ti<2-x>Zr<x>O<7> pyrochlore. The self-propagating preparation method is characterized by including acquiring Ti, TiO<2>, ZrO<2>, Gd<2>O<3> and CuO powder to be used as raw materials according to certain proportions; carrying out dry ball milling, uniform mixing and drying on the raw materials and compressing the raw materials to obtain blanks; placing the blanks in self-propagating quasi-isostatic pressure devices, igniting the blanks by the aid of ignition devices to carry out reaction and applying pressures after combustion is completed to obtain the Gd<2>Ti<2-x>Zr<x>O<7> pyrochlore. The self-propagating preparation method has the advantages that self-propagating high-temperature synthesis is combined with fast densification processes, and accordingly pyrochlore-type man-made rock densification solidified bodies which are high in thermal stability and chemical stability and excellent in anti-irradiation property can be synthesized in a few minutes; the self-propagating preparation method is high in synthesis speed, production efficiency, reaction temperature and product purity, low in energy consumption and applicable to long-term safety solidification treatment and disposal on nuclide of actinium series in high-level radioactive waste, processes are simple, and the like.
Owner:SOUTHWEAT UNIV OF SCI & TECH
Method for enriching and purifying cardiac glycoside of wormseed mustard herb
InactiveCN101732391AHigh adsorption selectivityParsing fastDigestive systemBlood disorderDesorptionThermal stability
The invention belongs to the field of natural organic chemistry and relates to a method for enriching and purifying cardiac glycoside of wormseed mustard herb by macroporous absorption resin. The method is characterized in that: the method adopts macroporous absorption technology to separate and purify the cardiac glycoside, has good adsorptive selectivity on the cardiac glycoside, rapid adsorption and desorption, high adsorption capacity, convenient and rapid extraction, rich source of raw materials, low production cost, obvious separation effect and high extraction purity, can obtain a cardiac glycoside semifinished product with content of over 35 percent and a cardiac glycoside final product with content of over 98 percent, and overcomes the disadvantages of low extraction rate and extraction purity in the prior art. The macroporous absorption resin with stable physicochemical property, large surface area, high exchange speed, high mechanical strength, strong antipollution capacityand good thermal stability is selected, can selectively adsorb the cardiac glycoside from solution through physical adsorption, and has rapid adsorption and desorption and large adsorption capacity.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method with ultra-high pressure for extracting ganoderma lucidum polysaccharide in glossy ganoderma
InactiveCN107857828AHigh adsorption selectivityLarge adsorption capacityUltra high pressurePlant cell
The purpose of the present invention is to overcome the disadvantages of relatively low extraction rate and low extraction purity of conventional techniques, and provide a method for extracting polysaccharides from Ganoderma lucidum by using ultra-high pressure technology. The application of ultra-high pressure technology in the present invention is a treatment method that applies a pressure greater than 100 hydrostatic pressure to the raw material under normal temperature and near normal temperature conditions. The ultra-high pressure can make the solvent enter the interior of the plant cells, and the solvent can carry the active ingredient after the pressure is released. And overflow, to achieve high extraction efficiency of plant active ingredients, use macroporous resin to adsorb and purify Ganoderma lucidum polysaccharides, good adsorption selectivity to Ganoderma lucidum polysaccharides, fast adsorption and resolution, and large adsorption capacity.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method for preparing aureusidin in liverwort by superhigh pressure technique
The invention belongs to the field of natural organic chemistry, and relates to a method for purifying aureusidin in liverwort by a superhigh pressure technique and macroporous resin enrichment. The method has characteristics that the extraction speed of aureusidin by the superhigh pressure technique is high; the time is saved; the extraction rate is high; aureusidin is separated and purified by a macroporous adsorption technique; the adsorptive selectivity to aureusidin is good; the adsorption is rapid; the resolution is rapid; the adsorption capacity is larger; the separation effect is obvious; the extraction purity is high; semifinished aureusidin with the content above 30% and finished aureusidin with the content above 90% can be obtained; and the defects that the conventional extraction rate is lower and the extraction purity is low are overcome.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method for simultaneously extracting icariin and baohuoside I and II from herba epimedii
InactiveCN103910772AStable physical and chemical propertiesIncrease surface areaSugar derivativesSugar derivatives preparationHydrolysateSimulated moving bed
The invention discloses a method for simultaneously extracting icariin and baohuoside I and II from herba epimedii. The method comprises the following steps of: crushing herba epimedii plant and then passing the crushed herba epimedii plant through a screen mesh, adding alcohol liquor, heating for reflux extraction, and filtering to obtain filtrate B, concentrating under reduced pressure to recycle alcohol to obtain initial extract; extracting the initial extract by pure water, regulating PH, stewing and carrying out suction filtration to obtain icariin extract; carrying out elution on the icariin extract by adopting macroporous adsorption resin, carrying out elution by using alcohol and collecting eluant; adding medical active carbon into the eluant, heating and refluxing, cooling, and filtering to obtain filtrate C; separating, purifying and crystallizing the filtrate C by simulated moving bed chromatography to obtain herba epimedii crystal, and collecting filtrate D; drying the herba epimedii crystal to obtain a pure icariin finished product; adding tween into the filtrate D, carrying out enzymolysis by glucosaccharase or cellulose, and separating and purifying the enzymatic hydrolysate by a chromatographic column mixed and filled by the macroporous resin to obtain products baohuoside I and II.
Owner:成都合盛生物技术有限公司
Epoxy modified nitrocellulose enamel and preparation method thereof
ActiveCN103409050AGood color retentionImprove thermal stabilityAnti-corrosive paintsEpoxy resin coatingsEpoxyNitrocellulose
The invention provides an epoxy modified nitrocellulose enamel and a preparation method thereof. The epoxy modified nitrocellulose enamel is prepared by stirring and mixing the following components in parts by weight: 30-45 parts of epoxy nitrocellulose enamel, 5-20 parts of pigment, 5-10 parts of talcum powder, 5-20 parts of precipitated barium sulphate, 2-6 parts of 10% bentonite pregel, 0.5-1.5 parts of dibutyl phthalate, 0.1-0.3 part of anti-settling agent CP-88, 25-40 parts of 1 / 2 second nitrocotton solution, 1.0-2.5 parts of dry mixed material, 0.1-0.3 part of 10% silicone oil and butyl ester solution and 1-5 parts of mixed solvent. The epoxy modified nitrocellulose enamel has favorable adhesive force, flexibility, glossiness and fullness.
Owner:天津灯塔涂料工业发展有限公司
Method for enriching and purifying forskolin in Rosa davurica flower
The invention belongs to the oranic chemistry field of natural products and relates to a method for enriching and purifying forskolin in Rosa davurica flower by utilizing macroporous adsorption resin. The method is characterized in that the macroporous adsorption technology is used to separate and purify forskolin, thus the adsorption selectivity on forskolin is good; adsorption and desorption are performed fast and the adsorption capacity is larger; and forskolin is convenient and fast to be extract, the raw material sources are rich, the production cost is low, the separation effect is obvious, the extraction purity is high, and the content of a forskolin is more than 35% in forskolin semi-finished product and a forskolin of which content is more than 90% in forskolin finished product can be obtained, and the defects of the conventional extraction method, namely lower extraction efficiency and low extraction purity can be overcome. The method selects the macroporous adsorption resinwith stable physical and chemical properties, larger surface area, higher exchange speed, high mechanical strength, high contamination resistance and good thermal stability to selectively adsorb forskolin from solution through physical absorption, thus absorption and desorption can be performed fast and the adsorption capacity is larger.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
A method for simultaneously extracting icariin and baohuoside I and II from epimedium
InactiveCN103910772BStable physical and chemical propertiesIncrease surface areaSugar derivativesSugar derivatives preparationHydrolysateSimulated moving bed
The invention discloses a method for simultaneously extracting icariin and baohuoside I and II from herba epimedii. The method comprises the following steps of: crushing herba epimedii plant and then passing the crushed herba epimedii plant through a screen mesh, adding alcohol liquor, heating for reflux extraction, and filtering to obtain filtrate B, concentrating under reduced pressure to recycle alcohol to obtain initial extract; extracting the initial extract by pure water, regulating PH, stewing and carrying out suction filtration to obtain icariin extract; carrying out elution on the icariin extract by adopting macroporous adsorption resin, carrying out elution by using alcohol and collecting eluant; adding medical active carbon into the eluant, heating and refluxing, cooling, and filtering to obtain filtrate C; separating, purifying and crystallizing the filtrate C by simulated moving bed chromatography to obtain herba epimedii crystal, and collecting filtrate D; drying the herba epimedii crystal to obtain a pure icariin finished product; adding tween into the filtrate D, carrying out enzymolysis by glucosaccharase or cellulose, and separating and purifying the enzymatic hydrolysate by a chromatographic column mixed and filled by the macroporous resin to obtain products baohuoside I and II.
Owner:成都合盛生物技术有限公司
Preparation process for extracting scopolamine from belladonna
InactiveCN108164523AHigh adsorption selectivityParsing fastOrganic chemistryInorganic saltsDesorption
The invention adopts the macroporous adsorption technology to separate and purify scopolamine, has the advantages of good adsorption selectivity to the scopolamine, fast adsorption and desorption, large adsorption capacity, convenient and rapid extraction, abundant raw material sources, low production cost, obvious separation effect, and high extraction purity, and overcomes the shortcomings of relatively low conventional extraction rate and low extraction purity. Macroporous adsorptive resin with stable physical and chemical properties, large surface area, fast exchange rate, high mechanicalstrength, strong anti-pollution ability and good thermal stability is selected, and the macroporous adsorptive resin is insoluble in acids, alkalis and organic enzymes, has good selectivity for organic substances, is not affected by the presence of inorganic salts and strong ionic low molecular compounds, can selectively adsorb the scopolamine from a solution by physical adsorption, and is fast inadsorption and desorption and large in adsorption capacity.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Novel method for extracting eleutheroside from radix acanthopanacis senticosi
InactiveCN108014153AHigh adsorption selectivityParsing fastPlant ingredientsEleutherococcus senticosusEleutheroside
Ultrasonic and microwave dual-assistance is applied to purification of eleutheroside, so that the adsorption selectivity for eleutheroside is good, adsorption and desorption are fast, and the adsorption capacity is larger. Extraction is convenient and fast, the production cost is low, the separation effect is obvious, the extraction purity is high, 90% or higher of eleutheroside can be obtained, and the defects of relatively low conventional extraction rate and low extraction purity are overcome. Polyamide resin adsorption chromatography with stable physical and chemical properties, larger surface area, higher exchange speed, high mechanical strength, high anti-pollution capacity and good thermal stability is adopted, selectivity to organic matter is better, influence of existence of inorganic salts and strong ionic low molecular compounds is avoided, and morin can be adsorbed selectively from the solution by physical adsorption. The method has the advantages of fast adsorption, fast desorption and larger adsorption capacity.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method for extracting atractylodes lancea ketone by using ultrahigh pressure technology
InactiveCN111217780AStable physical and chemical propertiesIncrease surface areaOrganic chemistryPlant cellKetone
The invention relates to an extraction method of atractylodes lancea ketone. According to the invention, an ultrahigh pressure technology is a treatment method for applying pressure of more than 100 MPa to raw materials under the conditions of normal temperature and near normal temperature, a solvent can enter plant cells under ultrahigh pressure, after pressure relief, the solvent can overflow along with effective components to achieve the high extraction efficiency of the effective components of the plants, and a macroporous resin is used for adsorbing and purifying atractylodes lancea ketone, wherein the adsorption selectivity on the atractylodes lancea ketone is good, the adsorption speed is high, the desorption speed is high, the adsorption capacity is large, and the defects of low extraction rate, low extraction purity and the like in the conventional technology are overcome.
Owner:南京西博恩生物科技有限公司
Ultrahigh-pressure extraction method of lentinan
InactiveCN111187364AHigh adsorption selectivityLarge adsorption capacityPhysical chemistryPlant cell
The invention relates to an extraction method of lentinan. According to the invention, an ultrahigh pressure technology is a treatment method for applying pressure of more than 100 MPa to raw materials under the conditions of normal temperature and near normal temperature, a solvent can enter plant cells under ultrahigh pressure, after pressure relief, the solvent can overflow along with effectivecomponents so as to achieve the high extraction efficiency of plant effective components, and lentinan is adsorbed and purified through a macroporous resin, so that the lentinan adsorption selectivity is good, adsorption and desorption are fast, the adsorption capacity is large, and the defects that in the conventional technology, the extraction rate is low, and the extraction purity is low are overcome.
Owner:南京萌源康德生物技术有限公司
Method for extracting tanshinone IIA from radix salviae miltiorrhizae
InactiveCN108033992AQuick selectionHigh selectivitySteroidsBulk chemical productionInorganic saltsPhysisorption
The invention belongs to the technical field of traditional Chinese medicine extraction, relates to a method for purifying tanshinone IIA, and particularly relates to a method for extracting tanshinone IIA from radix salviae miltiorrhizae. By applying supercritical CO2 fluid extraction, original color and flavor can not be damaged by heating, heat sensitivity can be better ensured, and substanceswhich are easy to oxidize can not be damaged; and extracts can also be simultaneously separated and purified in the extraction process. The method provided by the invention has the advantages that macroporous adsorption resin which is stable in physicochemical property, larger in surface area, higher in exchange speed, high in mechanical strength, high in anti-pollution capability and good in heatstability is selected, and the macroporous adsorption resin is insoluble in acids, alkalis and organic media, has better selectively to organic substances, is free from influence of inorganic salts and strong-ion low-molecular compounds, can selectively adsorb tanshinone IIA from the solution through physical absorption, and has the effects of high absorption speed, high desorption speed and larger adsorption capacity.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method for enriching and purifying veratric acid in globeflower
ActiveCN102070443BHigh adsorption selectivityParsing fastCarboxylic compound separation/purificationDesorptionVeratric acid
The invention belongs to the field of natural organic chemistry, and particularly relates to a method for enriching and purifying veratric acid in globeflower by using macroporous adsorbent resin. By using macroporous adsorption technology to separate and purify veratric acid, the invention has the characteristics of good adsorption selectivity for veratric acid, high adsorption and desorption speed, high adsorption capacity, abundant material sources, low production cost, obvious separation effect and high extraction purity, can be used for extracting veratric acid conveniently and quickly, can be used to obtain a semi-finished product of which the content of veratric acid is higher than 30% and a final product of which the content of veratric acid is higher than 90%, and can overcome the defects of low extraction yield and low extraction purity in the conventional method. The macroporous adsorbent resin, which has the advantages of stable physicochemical properties, large surface area, high exchange speed, high mechanical strength, high antipollution capability and high thermal stability, is used for selectively adsorbing veratric acid from the solution in a physical adsorption mode; and the invention has the advantages of high adsorption and desorption speed, and high adsorption capacity.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method for enriching and purifying folic acid in herba orostachyos by utilizing macroporous adsorption resin
InactiveCN111196810AHigh adsorption selectivityParsing fastOrganic chemistryPhysisorptionOrganic chemistry
The invention belongs to the field of natural organic chemistry, and relates to a method for enriching and purifying folic acid in herba orostachyos by utilizing macroporous adsorption resin. The method is characterized in that a macroporous adsorption technology is used for separating and purifying folic acid, the adsorption selectivity on folic acid is good, adsorption and desorption are fast, and the adsorption capacity is large; extraction is convenient and fast, raw material sources are rich, production cost is low, separation effect is obvious, extraction purity is high, a folic acid semi-finished product with the content of more than 35% and a folic acid final product with the content of more than 98% can be obtained, and the defects of relatively low conventional extraction rate and low extraction purity are overcome. Macroporous adsorption resin with stable physicochemical properties, large surface area, high exchange speed, high mechanical strength, strong anti-pollution ability and good thermal stability is selected, folic acid can be selectively adsorbed from a solution through physical adsorption, adsorption is fast, desorption is fast, and adsorption capacity is large.
Owner:HUANGGANG HUAYANG PHARMA
A method for extracting cistanche glucoside from Cistanche cistanche
InactiveCN103044504BHigh adsorption selectivityRich sourcesSugar derivativesSugar derivatives preparationChemical reactionCoupling
The invention belongs to the field of natural organic chemistry, and relates to a method for enriching and purifying boschniakia rossica glucoside in boschniakia rossica through supercritical CO2 fluid extraction and macroporous resin coupling. The method has the characteristics that effective components of a medical plant are kept in an extraction process by a supercritical CO2 fluid extraction technology; chemical reaction does not occur in the extraction process; the safety is good; the extraction efficiency is high; the energy consumption is less; the production efficiency is improved; and the cost is lowered. With the adoption of a macroporous adsorbing technology for separating and purifying boschniakia rossica glucoside, a separating effect is obvious; the extraction purity is high; semifinished boschniakia rossica glucoside with the content above 30%, and finished boschniakia rossica glucoside with the content above 95% can be obtained; and the defects that the conventional extraction yield is relatively lower and the extraction purity is low are overcome.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
A new method for purification of Lycium barbarum polysaccharide
The invention discloses a novel purification method of lycium chinense polyhexose, which comprises the steps that lycium chinense fruits are smashed into crude powder, 15 times of 85% methanol is added for reflux extraction for 120min and filtered; methanol is recovered from a filtrate; the filtrate is concentrated to 3 Be; hydrochloric acid and water at a volume ratio of 3:1 are used to regulate a pH value of a concentrated solution to 2.5; the concentrated solution is placed for 20 min and filtered; a broad-spectrum macroporous resin adsorption column is placed in the filtrate for collection of an eluent; methanol is recovered; the eluent is concentrated and dried to form a polysaccharide semifinished product; a silica gel chromatographic column is placed in the polysaccharide semifinished product; acetone and carbinol at a volume ratio of 3:1 are used to wash impurities; acetone and methanol at a volume ratio of 7:1 are used for elution; an eluent is collected; the collected polysaccharide eluent is refined to form the lycium chinense polysaccharide finished product; and the content is over 70%. The novel purification method has the greatest characteristics that with the adoption of a macroporous adsorption resin-silica gel chromatography coupled method, the novel purification method is quick and convenient; sources of raw materials are abundant; the manufacturing cost is low; the separating effect is obvious; and the extraction purity is high.
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
A kind of epoxy modified nitro enamel and preparation method thereof
ActiveCN103409050BGood color retentionImprove thermal stabilityAnti-corrosive paintsEpoxy resin coatingsEpoxySolvent
The invention provides a kind of epoxy modified nitro enamel and preparation method thereof, described epoxy modified nitro enamel is made of epoxy nitro varnish, pigment, talcum powder, precipitated barium sulfate, 10% bentonite pregel , dibutyl phthalate, anti-sedimentation agent CP-88, 1 / 2 second nitrocellulose solution, mixed dry material, 10% silicone oil butyl ester solution and mixed solvent, and the epoxy nitrocellulose paint is calculated in parts by weight 30‑45 parts of raw materials, 5‑20 parts of pigments, 5‑10 parts of talcum powder, 5‑20 parts of precipitated barium sulfate, 2‑6 parts of 10% bentonite pregel, 0.5‑1.5 parts of dibutyl phthalate, Anti-settling agent CP-880.1-0.3 parts, 1 / 2 second nitrocellulose liquid 25-40 parts, mixed dry material 1.0-2.5 parts, 10% silicone oil butyl ester liquid 0.1-0.3 parts, mixed solvent 1-5 parts, by stirring Prepared by mixing; has excellent adhesion, flexibility, gloss and fullness.
Owner:天津灯塔涂料工业发展有限公司
Method for enriching and purifying folic acid in houseleek by macroporous absorbent resin
ActiveCN101775016BHigh adsorption selectivityParsing fastOrganic chemistryAbsorption capacityDesorption
The invention relates to a method for enriching and purifying folic acid in houseleek by macroporous absorbent resin, which belongs to the field of natural organic chemistry. The invention is characterized in that the macroporous absorbent technology is used for separating and purifying the folic acid, the adsorption selectivity on the folic acid is good, both the adsorption and the desorption are fast, the adsorption capacity is large, the extraction is convenient and fast, the raw material sources are rich, the production cost is low, the separation effect is obvious, the extraction purity is high, the folic acid semi-finished products with the content higher than 35 percent and the folic acid finished products with the content higher than 98 percent can be obtained, and the defects of relatively low extraction rate and low extraction purity of the conventional method are overcome. The invention adopts the macroporous absorbent resin with the advantages of stable physicochemical property, large superficial area, high exchange speed, high mechanical strength, strong pollution resistance capability and good thermal stability, the folic acid can be selectively absorbed in the solution through physical absorption, and the invention has the advantages of fast absorption, fast desorption and large absorption capacity.
Owner:HEILONGJIANG DINGHENGSHENG PHARM CO LTD
Method for enriching and purifying fructooligosaccharide in witloof
ActiveCN102093437BHigh adsorption selectivityRich sourcesSugar derivativesOligosaccharidesHigh absorptionAbsorption capacity
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
Method for enriching and purifying common phellinus fungus general flavone in common phellinus fungus
ActiveCN102078339BHigh adsorption selectivityParsing fastFungi medical ingredientsImmunological disordersBiotechnologyCoupling
Owner:DAXINGANLING LINGOBERRY BOREAL BIOTECH CO LTD
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