33results about How to "Good chemical cross-linking" patented technology

The invention discloses waterborne polyurethane thermal-insulating sound-absorbing coating and a preparation method thereof. The waterborne polyurethane thermal-insulating sound-absorbing coating comprises a polyurethane prepolymer, N-hydroxymethyl acrylamide, phthalic acid dibutyl ester, a zirconium-aluminic acid ester coupling agent, rutile titanium dioxide, methylsilicone oil, a mixed solvent and a sound-absorbing material. The preparation method comprises the following steps: dissolving every 1 kg by weight of N-hydroxymethyl acrylamide in 2 kg of 50-70% ethanol in volume concentration, mixing with the polyurethane prepolymer in a reaction kettle, enabling the components to react for 1 hour at 80-150 DEG C, and adding the zirconium-aluminic acid ester coupling agent to continuously react for 2-5 hours; subsequently adding the phthalic acid dibutyl ester, rutile titanium dioxide, methylsilicone oil, mixed solvent and sound-absorbing material, and uniformly mixing, thereby obtaining a waterborne polyurethane thermal-insulating sound-absorbing coating product. The waterborne polyurethane thermal-insulating sound-absorbing coating can insulate heat and absorb sound, and is good in chemical resistance, good in temperature resistance, good in weather resistance, long in film service life, free of toxicity or smell, safe and environment-friendly and good in sound absorption effect.

The invention relates to a TPU thin film with light reflection and thermal insulation functions and a preparation method thereof. The TPU thin film is prepared from, by weight, 50-100 parts of polyester glycol, 15-30 parts of diisocyanate, 5-35 parts of a chain extender, 1-5 parts of molybdenum disulfide micro powder, 1-5 parts of white carbon black, 2-5 parts of metal oxide-modified diatomaceous earth powder, 2-5 parts of dibutyl phthalate, 0.5-1 parts of a titanate coupling agent, 1-5 parts of talcum powder and 1-5 parts of sepiolite. The TPU thin film has the excellent light reflection and thermal insulation functions.

The invention discloses a thermal insulation heat-preservation paint coating used for a building external wall. The thermal insulation heat-preservation paint coating is prepared from, by weight, 40-50 parts of emulsion, 1-2 parts of N-hydroxymethyl acrylamide, 6-9 parts of titanium dioxide, 4-6 parts of water, 1-2 parts of titanate coupling agent, 8-16 parts of auxiliary, 7-9 parts of mixed solvent, and 9-12 parts of thermal insulation heat-preservation material, wherein the emulsion is the mixed solution of A-102 silicone acrylic emulsion and A-99 pure acrylic emulsion in the weight ratio of 1.5:1, the auxiliary is composed of 1-2 parts of biocide mildewcide, 1-3 parts of flattening agent, 1-2 parts of pigment dispersing agent, 1-3 parts of thickening agent and 4-6 parts of film-forming agent, and the thermal insulation heat-preservation material is a mixture of hollow glass beads, expanded perlite and aluminum silicate fiber in the weight ratio of 1:1:1. The thermal insulation heat-preservation paint coating used for the building external wall is characterized by being strong in chemical resistance, good in weather resistance, good in thermal insulation heat-preservation effect, high in glossiness, long in service life of coating and the like.

The invention relates to a polyurethane anticorrosive thermal-insulation paint and a preparation method thereof. The paint comprises a polyurethane prepolymer, diacetone acrylamide, dipropanediol dibenzoate, an aluminate coupling agent LS-822, a dispersing agent triethanolamine, rutile titanium white, a defoaming agent OP-10, kaolin, a mixed solvent, expanded perlite and a preservative. The preparation method comprises the following steps: adding 2.4kg of 55-85 vol% ethanol into every kilo of diacetone acrylamide, dissolving, mixing with the polyurethane prepolymer in a reaction kettle, reacting at 80-140 DEG C for 1-2 hours, and adding the aluminate coupling agent LS-822 and dispersing agent triethanolamine; and continuing reacting for 3-5 hours, adding the dipropanediol dibenzoate, rutile titanium white, defoaming agent OP-10, kaolin, mixed solvent, expanded perlite and preservative, and evenly mixing to obtain the polyurethane anticorrosive thermal-insulation paint product.

The invention discloses a polyurethane waterproof flame-retardant paint and a preparation method thereof. The paint comprises polyurethane prepolymers, diacetone acryloamide, buty stearate, titanate coupling agent TMC-311 and titanium pigment. The paint further comprises polydimethyl siloxane, white carbon black, mixed solvent and flame-retardant materials. The preparation method comprises the following steps: dissolving the diacetone acrylamide by ethanol of which the volume concentration is 65-80%, wherein the adding amount of the ethanol is 1.5 kilograms in per kilogram of diacetone acrylamide on the basis of weight; mixing the dissolved diacetone acrylamide with the polyurethane prepolymers in a reaction kettle, wherein the reaction temperature is 75-119 DEG C and the reaction time is 1.2-1.5 hours; adding the titanate coupling agent TMC-311 into the mixture and further reacting for 3-6 hours; then adding buty stearate, the rutile-type titanium pigment, polydimethyl siloxane, the flame-retardant materials, the white carbon black and the mixed solvent into the mixture and uniformly mixing, so that the polyurethane waterproof flame-retardant paint product is obtained. The paint prepared by the preparation method is good in waterproof and flame-retardant effects, friendly to the environment and not easy to age.

The invention relates to a water-soluble polyurethane external-wall thermal-insulation waterproof paint and a preparation method thereof. The paint comprises a polyurethane prepolymer, N-hydroxymethyl acrylamide, dibutyl phthalate, vinyl trichlorosilane, titanium white, methyl silicone oil, superfine calcium carbonate and a mixed solvent. The preparation method comprises the following steps: adding 2 kilos of 50-70 vol% ethanol into every kilo of N-hydroxymethyl acrylamide for dissolution, mixing with the polyurethane prepolymer in a reaction kettle, reacting at 80-150 DEG C for 1 hour, and adding vinyl trichlorosilane; continuing reacting for 2-5 hours; and adding the dibutyl phthalate, rutile titanium white, methyl silicone oil, superfine calcium carbonate and mixed solvent, and uniformly mixing to obtain the water-soluble polyurethane external-wall thermal-insulation waterproof paint product. The water-soluble polyurethane external-wall thermal-insulation waterproof paint has the characteristics of high chemical resistance, high temperature resistance, favorable weather resistance favorable pollution resistance, high glossiness, long service life of the coated film and the like.

The invention relates to a polyurethane modified asphalt waterproof paint and a preparation method thereof. The paint is prepared from a polyurethane prepolymer, 90# petroleum asphalt, modified nano calcium carbonate, vinyl trichlorosilane, a tackifier, n-butyl acetate, citric acid, dibutyltin dilaurate, polyoxyethylene polyoxypropylene ether and fumed silica. The preparation method includes: modifying the 90# petroleum asphalt with the polyurethane prepolymer and modified nano calcium carbonate; then adding vinyl trichlorosilane, citric acid and n-butyl acetate into a reaction kettle, and stirring the substances evenly; then adding fumed silica, the tackifier and dibutyltin dilaurate, and stirring the substances evenly; then adding polyoxyethylene polyoxypropylene ether; further performing stirring till no powder flotation; shearing all the materials in the reaction kettle on a high speed shearing machine again until the 90# petroleum asphalt and other materials are evenly dispersed,thus obtaining the polyurethane modified asphalt waterproof paint. The product provided by the invention has the advantages of high bonding strength, high tensile strength and good dispersibility.

The invention relates to a water-soluble polyurethane external-wall thermal-insulation paint and a preparation method thereof. The paint comprises a polyurethane prepolymer, N-hydroxymethyl acrylamide, dibutyl phthalate, vinyl trichlorosilane, titanium white, methyl silicone oil, superfine calcium carbonate and a mixed solvent. The preparation method comprises the following steps: adding 2 kilos of 50-70 vol% ethanol into every kilo of N-hydroxymethyl acrylamide for dissolution, mixing with the polyurethane prepolymer in a reaction kettle, reacting at 80-150 DEG C for 1 hour, and adding vinyl trichlorosilane; continuing reacting for 2-5 hours; and adding the dibutyl phthalate, rutile titanium white, methyl silicone oil, superfine calcium carbonate and mixed solvent, and uniformly mixing to obtain the water-soluble polyurethane external-wall thermal-insulation paint product. The water-soluble polyurethane external-wall thermal-insulation paint has the characteristics of high chemical resistance, high temperature resistance, favorable weather resistance, favorable pollution resistance, high glossiness, long service life of the coated film and the like.

The invention discloses water-soluble polyurethane flame-retardant coating and a preparation method thereof. The water-soluble polyurethane flame-retardant coating comprises a polyurethane prepolymer, N-hydroxymethyl acrylamide, phthalic acid dibutyl ester, a titanate coupling agent, talcum powder, light calcium carbonate, tributyl phosphate, isopropanol, a mixed solvent and a flame-retardant material. The preparation method comprises the following steps: dissolving every 1 kg by weight of N-hydroxymethyl acrylamide in 2 kg of 50-70% ethanol in volume concentration, mixing with the polyurethane prepolymer in a reaction kettle, enabling the components to react for 1 hour at 80-150 DEG C, and adding a mixture of isopropanol and a titanate coupling agent in a weight ratio of 1:1 to continuously react for 2-5 hours; subsequently adding phthalic acid dibutyl ester, talcum powder, light calcium carbonate, tributyl phosphate, the mixed solvent and the flame-retardant material, and uniformly mixing, thereby obtaining a water-soluble polyurethane flame-retardant coating product. The water-soluble polyurethane flame-retardant coating has the characteristics of good chemical resistance, good temperature resistance, good weather resistance, good stain resistance, high glossiness, long film service life and the like.

The invention discloses a high-voltage transmission lead anti-corrosion paint prepared from modified nano-silicon dioxide and a preparation method of the anti-corrosion paint. The anti-corrosion paintcomprises, by weight, 80-90 parts of acrylic resin, 30-40 parts of styrene-acrylic emulsion, 25-30 parts of modified nano-silicon dioxide, 6-10 parts of graphene, 2-4 parts of sodium hexametaphosphate, 4-6 parts of sodium benzoate, 2-4 parts of carbon fluoride, 6-8 parts of zinc stearate, 2-4 parts of tributyl citrate, 7-9 parts of aluminum zirconate coupling agents, 3-5 parts of hydroxyethyl cellulose, 2-4 parts of polyvinyl alcohol and 100-120 parts of deionized water. Physical performances such as corrosion resistance, dispersity, weather resistance and barrier property of the paint are remarkably improved under synergistic effects of components, nano-silicon dioxide is modified, so that compatibility between the nano-silicon dioxide and an organic macromolecule is improved, rheological properties of a system are improved, and super-hydrophobicity and mechanical wear resistance of the paint are improved.

The invention provides a production method for a cement utility pole coated with weather-resistant artificial tree bark. The production method comprises the following steps: S1, producing a cement utility pole; S2, preparing weather-resistant artificial tree bark slurry; S3, applying the weather-resistant artificial tree bark slurry to produce the cement utility pole coated with the weather-resistant artificial tree bark. The cement utility pole coated with a weather-resistant artificial tree bark layer is attractive in appearance and is in harmony with the surroundings, visual enjoyment can be brought to a tourist attraction environment, and beauty elements can be added to a tourist attraction. The weather-resistant artificial tree bark slurry is prepared from the following raw materials: epoxy resin, polyaniline, carboxyl polysiloxane, heavy calcium carbonate powder, fumed silica, pigment printing paste, glass fibers, a curing agent, an antioxidant, an ultraviolet light absorber, dibutyl phthalate and a mixed solvent. Construction is simple and fast, and the applied bark is natural in texture and good in weather resistance and used for beautifying the cement utility pole and brings visual enjoyment.

The invention belongs to the field of water-based coating materials, and particularly relates to a water-based heavy anti-corrosion flame-retardant coating material for a metal base material, and a preparation method thereof. The water-based heavy anti-corrosion flame-retardant coating material comprises a component A and a component B according to a weight ratio of 100:(20-30), wherein the component A comprises 50-60 parts of a modified epoxy resin emulsion, 10-15 parts of functionalized modified graphene, 12-18 parts of a filler, 5-10 parts of a cosolvent, 0.5-1 part of an antifoaming agent,0.5-1 part of a leveling agent, 1-2 parts of an anti-settling agent, 0.5-1 part of an anti-freezing agent, 1-1.5 parts of a thickener, 1-2 parts of a wetting agent, 1-2 parts of a dispersant and 35-45 parts of deionized water, and the component B comprises 35 to 50 parts of a curing agent and 20 to 35 parts of a cosolvent. According to the invention, the water-based heavy anti-corrosion flame-retardant coating material has the advantages of good film-forming property, high coating adhesive force, good stability, greatly improved fire resistance limit, greatly improved bonding strength, greatly improved fire resistance time, good flame retardancy, good corrosion resistance, good water resistance, good weather resistance, low cost, safety and environmental protection; and the preparation method disclosed by the invention is simple, easy to operate, high in production efficiency, available in raw materials, low in energy consumption and capable of realizing large-scale production.

The invention provides a flame-retardant bark of an artificial tree and a making method thereof. The bark is prepared from the following raw materials: epoxy resin, polyaniline, carboxyl polysiloxane, heavy calcium carbonate powder, fumed silica, pigment printing paste, glass fiber, a curing agent, a fire retardant, dibutyl phthalate and a mixed solvent. The making method comprises the following steps: adding epoxy resin into a reaction vessel, then adding the mixed solvent for dissolving, adding polyaniline into the reaction vessel, mixing polyaniline with mixing under high-speed stirring, carrying out a reaction at 20 to 25 DEG C for 1 h with a pH value controlled to be 1 and then adding carboxyl polysiloxane; continuing the reaction at a temperature in a range of room temperature to 50 DEG C for 2 to 5 h; and then adding dibutyl phthalate, heavy calcium carbonate powder, fumed silica, pigment printing paste, glass fiber, the curing agent and the fire retardant, carrying out uniformly mixing under stirring, pouring the obtained mixture into a bark die placed in advance and carrying out micro-pressure standing so as to eventually obtain the flame-retardant bark of the artificial tree. The bark of the artificial tree has lifelike texture and flame retardation effect.

The invention provides an imitative landscape iron tower. The imitative landscape iron tower comprises a trunk, an imitative tree bark, imitative tree branches and a support, wherein the trunk is vertically and fixedly arranged on ground, the imitative tree bark coats the outside of the trunk; the imitative tree branches are fixedly arranged on the trunk, extend dendritically and are dispersedly distributed; the support is arranged at the top of the trunk, communication equipment is arranged on the support; an iron tower is simply treated, designed into a modelling of an imitative tree, beautiful in appearance and coordinated with a surrounding environment; and a beautiful element is added for a tourist area. The imitative tree bark is prepared from the following raw materials: epoxy resin, polyaniline, carboxyl polysiloxane, heavy calcium carbonate powder, gas phase white carbon black, coating pigment paste, glass fibers, aliphatic polyamine, ferric oxide, dibutyl phthalate and a mixed solvent, and the produced imitative tree bark is natural in texture, strong in weather resistance, simple and rapid in construction, long in anti-aging time and used for beautifying the iron tower and brings visual enjoyment to people.

A flame-retardant waterproof coating for building outer walls consists of 40 to 50 parts of emulsion, 1 to 2 parts of N-methylolacrylamide, 6 to 9 parts of fumed silica, 4 to 6 parts of water, 1 to 2parts of titanate coupling agent, 6 to 12 parts of auxiliary agent, 7 to 9 parts of n-butyl acetate, 6 to 9 parts of flame retardant mixture, and 5 to 10 parts of modified nano calcium carbonate, wherein the emulsion is a mixed solution of A-102 silicone-acrylic emulsion and A-99 pure acrylic emulsion with a weight ratio of 1.5:1, the auxiliary agent consists of 1 to 3 parts by weight of levelingagent, 1 to 3 parts by weight of thickening agent and 4 to 6 parts by weight of film forming aid, and the flame retardant mixture is a mixture of dimethyl methylphosphonate and microencapsulated red phosphorus with a weight ratio of 1:2. The coating of the invention has the characteristics of strong chemical resistance, good weather resistance, good flame retardant effect, high gloss, long servicelife of a formed film and the like.